基于孔压静力触探试验的水运工程土分类方法研究

土的工程分类是工程勘察和设计应用的关键问题之一。基于孔压静力触探测试（piezocone penetration test,简称CPTU）原位测试参数进行土分类是高效实用的方法。国内外现有分类方法的名称及标准与我国《水运工程岩土勘察规范》（JTS 133－2013）不符合。因此,建立基于CPTU原位测试参数、符合我国行业标准的土工程分类方法具有重要工程意义。在收集大量国内外水运工程CPTU测试资料的基础上,对比分析了616个间距小于5 m的CPTU测试孔和相应钻孔取样与室内土工试验成果。选择国内外7种常用的CPTU土分类图进行应用比较,发现这些土分类图所采用的应力修正计算方法在考虑浅层土体的有效上覆应力修正时存在一定的缺陷,通过引入新的应力修正方法和修正土分类边界线,建立了适合我国水运工程的CPTU土分类方法。对比应用分析表明,该分类图能够准确地进行水运工程土类划分,尤其适合于软土、粉细砂和中粗砂的划分,可作为我国水运工程的土工程分类方法。     

致密砂岩气藏可动流体赋存特征的微观地质因素: 以苏里格气田东部盒8段储层为例

以苏里格气田东部盒8段典型的致密砂岩气藏为例,运用核磁共振、恒速压汞、铸体薄片、物性、X-衍射等实验资料,探讨了影响可动流体赋存差异的微观地质 因素。结果表明,盒8段储层可动流体饱和度低,T₂谱分布均为左高峰右低峰的双峰态;黏土矿物的充填与孔隙类型是孔隙结构复杂的重要因素,孔隙结构是影响可动流体赋存特征的关键;面孔率、喉道 半径、孔喉半径比是影响可动流体饱和度的主要因素,有效孔隙体积、分选系数对可动流体饱和度影响明显,储层物性、黏土矿物、有效喉道体积、孔隙半径对可动流体饱和度影响较弱。     

黄土高原中东部沙尘与非沙尘天气花粉组成及来源范围

通过黄土高原两个不同地区(浑源、洛川)沙尘与非沙尘天气花粉组合的对比来探讨主要花粉类型最大传播距离。结果表明：沙尘天气花粉汇集量明显高于非沙尘天气,特别是蒿属和藜科花粉,沙尘天气平均是非沙尘天气的3倍以上。随风速增大,花粉可能的最大源区范围明显增大。风速低于3.3 m/s时,蒿属和藜科花粉多来自100 km范围内,其他类型花粉来源范围不超过20 km;风速大于5.9 m/s时,蒿属和藜科花粉源区范围增至300 km以上;其他类型花粉不超过100 km。风速达到12.5 m/s时,蒿属及藜科最大花粉源区范围可达1000 km,其他类型花粉不超过300 km。浑源地区不论平均风速还是最大风速均明显高于洛川地区,因此,主要花粉类型可能的最大源区范围达200 km,大于洛川地区(低于100 km)。     

A cavity expansion–based solution for interpretation of CPTu data in soils under partially drained conditions

A cavity expansion–based solution is proposed in this paper for the interpretation of CPTu data under a partially drained condition. Variations of the normalized cone tip resistance, cone factor, and undrained-drained resistance ratio are examined with different initial specific volume and overconsolidation ratio, based on the exact solutions of both undrained and drained cavity expansion in CASM, which is a unified state parameter model for clay and sand. A drainage index is proposed to represent the partially drained condition, and the critical state after expansion and stress paths of cavity expansion are therefore predicted by estimating a virtual plastic region and assuming a drainage-index–based mapping technique. The stress paths and distributions of stresses and specific volume are investigated for different values of drainage index, which are also related to the penetration velocity with comparisons of experimental data and numerical results. The subsequent consolidation after penetration is thus predicted with the assumption of constant deviatoric stress during dissipation of the excess pore pressure. Both spherical and cylindrical consolidations are compared for dissipation around the cone tip and the probe shaft, respectively. The effects of overconsolidation ratio on the stress paths and the distributions of excess pore pressure and specific volume are then thoroughly investigated. The proposed solution and the findings would contribute to the interpretation of CPTu tests under a random drained condition, as well as the analysis of pile installation and the subsequent consolidation.     

赤道东北太平洋表层沉积物间隙水中营养盐的剖面分布及其海底扩散通量

对赤道东北太平洋海域表层沉积物间隙水中硅酸盐、磷酸盐和硝酸盐等营养盐的剖面分布三个航次的研究表明,研究区在采样深度内沉积物中有机质的分解以硝化作用为主.在水-沉积物界面附近硅酸盐、磷酸盐和硝酸盐都存在着极陡的浓度梯度, Fick扩散定理的计算结果表明,研究区内硅酸盐、磷酸盐和硝酸盐的海底扩散通量分别为- 886.45～ 42.62 μ mol/(m2· d)、- 3.04～ 5.83 μ mol/(m2· d)和- 189.43～ 21.05 μ mol/(m2· d),且硅酸盐和硝酸盐主要是从沉积物向底层水体扩散,是底层水体营养盐的来源之一;研究区内硅酸盐、磷酸盐和硝酸盐的海底扩散通量存在着一定的时间和空间变化, 这可能与因全球气候变化而导致的沉积环境的改变有关.     

构造煤结构与煤层气赋存研究进展

碎软煤的完整原样制取困难,需要加工制成重塑煤体,为了研究不同压制荷载对煤体物性特征的影响,以重塑煤体为研究对象,基于低温液氮的孔隙测试实验和高压容量法的甲烷吸附实验,探讨不同成型荷载而成的重塑煤体的微小孔结构及其吸附特性的差异。结果表明：不同成型荷载压制而成的重塑煤体,其微孔和小孔的孔容随着成型荷载的增大而略微减少,孔比表面积随着成型荷载的增大而略微增加,总孔体积减少和孔比表面积增加的幅度不大;通过分形理论发现无论高压段还是低压段,孔隙结构具有明显的分形特征,且在高压段的分形维数普遍低于低压段,不同荷载压制而成的重塑煤体的分形维数差别不大;等温吸附线均符合第Ⅰ类等温吸附曲线,Langmuir模型适用于描述重塑煤体的等温吸附,成型荷载对煤的吸附常数有一定的影响,其对吸附常数b值的影响大于对a值的影响。研究不同成型荷载下重塑煤体的吸附特性,为不同条件下型煤制作及冷冻取心实验提供参考。     

Effect of Shale Reservoir Characteristics on Shale Oil Movability in the Lower Third Member of the Shahejie Formation,Zhanhua Sag

To reveal the effect of shale reservoir characteristics on the movability of shale oil and its action mechanism in the lower third member of the Shahejie Formation(Es3l), samples with different features were selected and analyzed using N2 adsorption, high-pressure mercury injection capillary pressure(MICP), nuclear magnetic resonance(NMR), high-speed centrifugation, and displacement image techniques. The results show that shale pore structure characteristics control shale oil movability directly. Movable oil saturation has a positive relationship with pore volume for radius > 2 μm, as larger pores often have higher movable oil saturation, indicating that movable oil is present in relatively larger pores. The main reasons for this are as follows. The relatively smaller pores often have oil-wetting properties because of organic matter, which has an unfavorable effect on the flow of oil, while the relatively larger pores are often wetted by water, which is helpful to shale oil movability. The rich surface provided by the relatively smaller pores is beneficial to the adsorption of immovable oil. Meanwhile, the relatively larger pores create significant pore volume for movable oil. Moreover, the larger pores often have good pore connectivity. Pores and fractures are interconnected to form a complex fracture network, which provides a good permeability channel for shale oil flow. The smaller pores are mostly distributed separately;thus, they are not conducive to the flow of shale oil. The mineral composition and fabric macroscopically affect the movability of shale oil. Calcite plays an active role in shale oil movability by increasing the brittleness of shale and is more likely to form micro-cracks under the same stress background. Clay does not utilize shale oil flow because of its large specific surface area and its block effect. The bedding structure increases the large-scale storage space and improves the connectivity of pores at different scales, which is conducive to the movability of shale oil.     

脱气温度和样品粒径对致密砂岩低温氮气吸附实验结果的影响

基于静态体积法的低温氮气吸附实验已广泛用于分析致密储集层的孔隙结构。本文探索了脱气温度和样品粒径对松辽盆地高台子致密砂岩低温氮气吸附实验结果的影响。结果显示,110℃的脱气条件并不能清除束缚水而使得孔隙体积、比表面积均偏低,300℃的脱气条件容易破坏样品中黏土矿物的结构令孔隙体积、比表面积减小,200℃是比较合适的脱气温度,既能去除束缚水又不破坏黏土矿物结构。样品粒径从5～10目减小至10～30目,氮气探测的孔隙数量增多使比表面积、孔体积增大。从10～30目减小至180～200目,黏土矿物相对含量降低令比表面积、孔体积显著减小;小于200目的样品中减少的黏土矿物主要集中在大于200目的岩样中,因此大于200目岩样的测定结果最高。因此,10～30目是利用低温氮气吸附实验寻求分析致密砂岩储集层特征的最佳粒径范围。     

基于分形理论探究砂岩最小孔隙半径的最优区间

渗透率是评价多孔介质导水性能的主要参数,是导水介质微观孔隙结构在宏观上的表现特征。通过扫描电镜实验和图像处理技术,统计出砂岩微观孔隙几何参数,并结合分形理论探究了砂岩微观孔隙结构对渗透率的影响。同时,以实测渗透率为约束条件,确定了对渗流起作用的最小孔隙半径r_min区间,该区间可作为渗透率预测时最小孔隙半径r_min的最优取值区间,并获取了与之对应的孔隙半径累积百分数区间。结果表明：砂岩最小孔隙半径r_min的取值对渗透率影响较大,随着砂岩最小孔隙半径r_min取值的增大,其渗透率先急剧下降,后渐渐地趋于稳定,并伴有上升趋势。在致密砂岩中,理论渗透率与实测渗透率相等时,对应的最小孔隙半径r_min落在孔隙半径累积百分数为15%~25%内,该孔隙半径累积百分数区间对应的孔隙半径区间可作为计算砂岩理论渗透率时最小孔隙半径r_min的最优取值区间,并且随着砂岩渗透率的增大,最小孔隙半径r_min对应下的孔隙半径累积百分数逐渐增加。     

剪切-体积应变耦合的孔压增量模型试验

以南京细砂为对象,通过共振柱试验及应变控制的排水/不排水分级和单级加载循环三轴试验的系统性研究,建立了能够描述饱和砂土孔压增长规律的新模型。该模型遵循Martin和Byrne提出的基本理论框架,孔压的增长是由循环剪切作用下体积改变所引起的。提出的孔压模型属于应变控制的孔压增量模型。基于排水循环单级加载试验,通过引入体积门槛剪应变γ_(tv)的概念,以具有代表性的15周体应变(ξ_(vd))15为基准点,归准化体应变发展与循环剪应变之间的关系,建立了三参数的体应变增量模型及其参数标定方法。基于排水和不排水循环单级加载试验结果,揭示了体应变与孔压比之间的内在联系,进而导出回弹模量表达式。通过耦合新的体应变增量模型及回弹模量公式,建立了新的剪应变-体应变耦合的孔压增量模型。验证性试验表明,新的孔压增量模型的预测值与试验结果的吻合度较高。