标志沉积层磁组构特征及其古环境意义研究

通过对长江三角洲及其邻近区域埋藏古土壤、潮坪、长江下游河道浸滩、舟山滨岸风成沙丘、南京黄土古土壤序列沉积体的磁组构测量统计分析，取得了各自的标志特征。该２特征揭示出，舟山滨岸风成沙丘与南京黄土吉土壤序列沉积的搬运介质能量位相基本一致，其物源来向却显示出巨大差异；上述两类沉积体与上述现今潮坪、河道漫滩沉积体地搬运介质能量位相及物源来向均显示出绝然不同的标志特征。然而浸滩物源来民南京黄土的物尖兵为向却     

海水中砷标准物质的研制

本文介绍了海水中砷标准物质的研制过程，其中包括溶液的配制、均匀性和稳定性检验，标样的分析方法。并对标准物质的定值数据进行统计处理，两种浓度的定值结果分别为：１．００μｇ／ｃｍ３±０．０４μｇ／ｃｍ３和５１．０μｇ／ｄｍ３±２．６μｇ／ｄｍ３。两种浓度砷标准物质的稳定期均为一年     

Multi-bioindicator study of a small estuary in Vendée (France)

Surficial sediment (about 5 mm) was scraped off in 15 stations selected in the Vie Estuary, a small estuary on the French Atlantic coast. The samples, prepared using the suitable methods, were used for comparing the behaviour of periphytic algae, sporopollinic and other palynologic material, ostracoda and foraminifera for proposing a synthetic evaluation of the information provided by each of them. Dinoflagellate cysts, which are found in an almost monospecific assemblage in low-salinity water, are dispersed by tidal currents, but the location of tintinnids in only the lower reaches shows a limited inward transport. Sporopollinic material is clearly related to the adjacent vegetation, indicating a local origin, and then little influence of transport on the microbenthos, even if fragments of freshwater crustaceans and of Pediastrum alga are found down to the mouth in the sporopollinic deposits. This limited transport of microbenthos allows the use of periphytic algae, benthic ostracoda and benthic foraminifera as indicators of local environmental conditions. It was then possible to determine the extent of marine influence in the estuary, to discriminate between the main channel and adjacent basins, and between different stages of evolution of the basins, from a recently dug basin to a eutrophicated one.     

A community-wide intercomparison exercise for the determination of dissolved iron in seawater

The first large-scale international intercomparison of analytical methods for the determination of dissolved iron in seawater was carried out between October 2000 and December 2002. The exercise was conducted as a rigorously “blind” comparison of 7 analytical techniques by 24 international laboratories. The comparison was based on a large volume (700 L), filtered surface seawater sample collected from the South Atlantic Ocean (the “IRONAGES” sample), which was acidified, mixed and bottled at sea. Two 1-L sample bottles were sent to each participant. Integrity and blindness were achieved by having the experiment designed and carried out by a small team, and overseen by an independent data manager. Storage, homogeneity and time-series stability experiments conducted over 2.5 years showed that inter-bottle variability of the IRONAGES sample was good (< 7%), although there was a decrease in iron concentration in the bottles over time (0.8–0.5 nM) before a stable value was observed. This raises questions over the suitability of sample acidification and storage.     

Kohonen网络与BP网络的集成应用研究

本文介绍了 Kohonen神经网络对输入数据进行聚类方法在卷烟配方中的应用 ,提出了从核心样本动态搜索 BP网络训练样本的新探索 ,摒弃了过去 BP算法中训练样本固定不变 ,互不相交的方法 ,实现了 BP网络和 Kohonen网络动态无缝集成。     

六溴苯的合成研究

对直接溴化法合成六溴苯作了系统的研究,并对文献方法进行了一系列的改进。包括选择适当的摧化剂及其用量,使反应基本上在室温下进行;利用水汽蒸馏法驱除残余溴,可直接得到无色或近乎无色的纯净产物,而勿需进行还原脱溴,且得率较高。提出一种以溴化物形式回收副产物的方法。     

Sample Disturbance in Soft and Sensitive Clays: Analysis and Assessment

Despite the sophisticated methods employed to obtain high quality samples, they are prone to disturbance, due to stress release, let apart, due to sampling tools and techniques adopted. Critical reappraisal of different methods suggest that any method of sample quality assessment involving strength and deformation parameters would enable easier implementation and correct other engineering parameters for estimated sample disturbance. In this technical paper, sample disturbance index, using merely the slopes of compression paths, (representing mechanical response), in the pre- and post-yield stress regimes under odeometric loading conditions is proposed. This method is based on single oedometer test results on samples of unknown degrees of disturbance during sampling and handling. The unique feature of this approach is that the ideal rigid plastic material behavior is taken as reference. This eliminates the need for any additional experimental data or any calculations from the relationships formulated with any set of assumptions.     

大窑湾疏浚物倾倒区环境调查研究

本文以1989年8月调查资料为基础,论述了大窑湾疏浚物倾倒区的水化学要素(pH、盐度、DO、COD、浊度)、营养盐(NO_2-N、NO_3-N、NH_4-N、PO_4-P、SiO_3-Si)和重金属(Cu、Zn、Pb、Cd)等污染物分布特征;分析了水质、底质的环境状况及潮流的影响。从环境地球化学观点探讨了该疏浚物倾倒区选择的科学性。     

离子色谱分析在黄土和粉尘研究中的应用

黄土中存在着大量的碱金属及碱土金属，以往的测试方法多为原子吸收和ICP—MS，离子色谱法在测试黄土样品的碱金属和碱土金属元素含量中应用不多。将黄土地质标准样品进行消解后用离子色谱进行测试，测试效果良好，重复测试的相对标准偏差小于5％，与推荐值的相对误差小于5％，准确度和精密度符舍相关的质量控制要求。本实验方法测试的离子含量都在仪器响应呈线性的最佳测试范围之内，标准曲线经回归后相关系数均达到0．9999。黄土样品的分析结果与粉尘气溶胶样品的离子分析结果对比表明，此方法对于探讨粉尘起源以及沙尘暴天气的研究具有重要意义。     

廉州湾南部海域泥沙来源及运移趋势分析

重矿物组合、含量变化和特征矿物的分布及变化规律是沿海泥沙来源和运移趋势判断的重要手段之一。通过对廉州湾南部海域海底表层沉积物的重矿物分析 ,发现该区重矿物分布以北海地角为界 ,其百分含量和特征矿物南北有别 ,可能分别代表不同的物质来源区。其中廉州湾北部南流江流域来沙是该区主要物源 ,运移趋势为自 NE向 SW;地角西南岸段、岭南侧海岸侵蚀及银滩来沙也为该区提供了部分物源 ,运移趋势为绕过冠头岭沿海岸向 N方向运移。由于缺乏北海陆域陆相地层重矿物含量等相关资料 ,暂未做物质来源区的具体判断