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51.
以微晶白云母为载体,钛酸丁酯为钛源,采用溶胶-凝胶法合成制备微晶白云母负载纳米TiO2光催化剂,然后用X射线衍射,扫描电镜等对微晶白云母负载TiO2光催化剂进行表征。再以微晶白云母负载纳米TiO2光催化剂对亚甲基蓝进行了光催化降解研究,特别针对有无紫外光照射条件下微晶白云母、纳米TiO2、微晶白云母/纳米TiO2等在亚甲基蓝溶液中的行为进行研究,结果表明:所制备的微晶白云母负载TiO2光催化剂对亚甲基蓝具有较好的光催化降解能力,1250目微晶白云母负载TiO2在紫外光照射下光催化反应4h,其降解率可达99%以上。 相似文献
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内蒙古红花尔基钨钼矿云英岩化白云母Ar-Ar定年及其地质意义 总被引:2,自引:2,他引:0
红花尔基钨多金属矿是近年在大兴安岭中北部地区发现的一处大型钨多金属矿床,主要矿化蚀变为云英岩化、绢英岩化,主要有用金属矿物为白钨矿和辉钼矿,岩体内辉钼矿与白钨矿有上钼下钨的带状分布特点,地质特征显示该矿床为一高温热液型钨(钼)矿床。为准确限定成矿热液活动时间,本文对矿区典型蚀变矿物——云英岩化蚀变带白云母进行Ar-Ar同位素定年,获得Ar-Ar坪年龄为174.4±1.2 Ma,等时线年龄为173.2±4.3 Ma。根据矿区云英岩化带与钨钼矿化带空间上重合和密切共生的关系,可知白云母的形成是与白钨矿、辉钼矿形成同源、同时,且辉钼矿Re-Os年龄(176.8±2.2 Ma)与Ar-Ar年龄在误差范围内具有一致性,该年龄代表了钨钼矿热液成矿时代。结合野外地质特征及锆石U-Pb、辉钼矿Re-Os年龄,进一步限定该矿床成矿时代为早中侏罗世,属燕山期构造岩浆活动的产物。 相似文献
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铁格隆南矿床产出了西藏班公湖- 怒江成矿带多龙矿集区最大的斑岩- 高硫型铜(金银)成矿系统。由于高硫型矿化与蚀变对斑岩型矿化和蚀变的广泛叠加,导致其成矿系统结构和成矿作用机制变得十分复杂,一定程度阻碍了其精细成矿模型的构建。本文基于铁格隆南矿床现有的勘查和研究成果,从矿物学的角度,以白云母为典型蚀变矿物,通过详细的镜下鉴定、扫描电镜和电子探针分析,详细揭示不同空间位置、不同产状白云母的矿物学特征和成因,探究其对铁格隆南矿床成矿机制的指示意义。结果显示,铁格隆南矿床的热液白云母主要由白云母端元、伊利石端元、绿鳞石端元以及少量钠云母端元组成。矿体中白云母与铜矿物具有成因联系。在深部的早期水岩反应中,白云母主要与黄铜矿伴生,热液蚀变斑岩形成的白云母呈现高Si低Al的特征,而热液蚀变砂岩呈高Al低Si的特征。随着流体向浅部继续运移,白云母共生的金属矿化转换为斑铜矿和铜蓝,多形成高Al低Si的白云母。相对于在侵入岩中产出的白云母,在砂岩中形成的白云母的FeT、Fe3+、Na+含量更高。侵入岩中形成富Fe2+白云母,指示热液还原性较强。此外,在黄铁绢英岩化带较中—浅部产出的白云母常与较多高岭石和铜蓝、斑铜矿伴生,指示了热液中的SO2发生聚集、温度降低、酸性增强并导致水岩反应增强和矿质沉淀的过程。综上,白云母与不同矿物组合及其地球化学特征,对成矿流体环境及勘查评价有良好的指示意义。 相似文献
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针对市场上出现的一种外观酷似和田玉的微晶化玻璃,利用常规宝石学测试手段、扫描电镜分析、X射线粉末衍射分析以及红外光谱分析等测试方法,对该材料样品的宝石学特征、表面微观形貌特征、光谱学特征等进行了研究。结果显示,样品为一种含氟的硅碱钙石微晶化玻璃,它是由以二氧化硅为主要成分的基础玻璃在特定的温度条件下逐渐析晶而成的,其微观结构与和田玉的有一定的差异,可以通过红外光谱和XRD对其进行结论性鉴定与区别。 相似文献
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Chemical and physical weathering of primary minerals during the formation of laterite profiles in the Darling Range has formed distinct secondary mineral and morphological zones in the regolith. Erosion and human activity such as mining have exposed large areas of lateritic regolith, and its classification is important for land management, especially for mine rehabilitation. Preserved rock fabrics within regolith may enable the identification of parent rock type and degree of weathering, thus providing explanations for variations in important physical properties such as the strength and water retention of regolith. Feldspar, quartz, biotite and muscovite in porphyritic and fine-grained monzogranite in lateritic profiles have weathered via a series of gradational changes to form saprolite and pedolith consisting of kaolin, quartz, iron oxides, muscovite and gibbsite. Local reorganisation in the upper regolith or pedoplasmation zone has included illuviation of kaolin, which may be iron oxide-stained and which has disrupted the preserved rock fabric of saprock and saprolite. Quartz grain- or matrix-supported fabrics have developed, with greater pedoplasmation resulting in a quartz-grain-supported fabric. The recognition of these processes enables the use of gibbsite grainsize and distribution in regolith to infer original feldspar grainsize. Muscovite-rich or muscovite-deficient kaolin matrix indicates where plagioclase or alkali feldspar, respectively, was present in the parent rock. In some regolith, cementing by iron oxides has faithfully preserved rock fabric. The recognition of these various regolith types provides a basis for identifying the parent materials of lateritic regolith developed from granitic and doleritic rocks. Rock fabric is sometimes preserved in iron oxide-cemented bauxite mine floor regolith (Zh) due to the pseudomorphic gibbsite grains and iron oxide cement which forms a porous, rigid fabric. Plagioclase-rich granitoid is more likely to have weathered to dense clay-rich regolith (Zp), whereas albite and alkali feldspar have weathered to quartz-rich regolith (Zm) with the random orientation of quartz grains indicating that substantial reorganisation of rock fabric has occurred. It is possible to predict the response of regolith materials exposed in mine floors to management practices including ripping and re-vegetation, thus allowing targeted use of deep-ripping and planting density based on regolith type. 相似文献
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Herbert W. Fournier James K. W. Lee Alfredo Camacho 《Journal of Metamorphic Geology》2019,37(6):769-793
The determination of the thermal (temperature–time) histories of high‐P metamorphic terranes has been commonly based on the concepts of slow cooling and closure temperatures. In this paper, we find that this approach cannot reconcile a geochronological data set obtained from the amphibolite‐facies allochthonous Leknes Group of the Lofoten islands, Norway, which reveals an extremely complex thermal history. Using detailed results from several different geochronometers such as 40Ar/39Ar, Rb–Sr and U–Pb, we show that a model invoking multiple, short‐lived thermal pulses related to hot‐fluid infiltration channelized by shear zones can reconcile this complicated data set. This model suggests that hot fluids infiltrated throughout basement shear zones and affected the overlying cold allochthon, partially resetting U/Pb rutile and titanite ages, crystallizing new zircon and produced identical 40Ar/39Ar and Rb/Sr ages in muscovite, biotite and amphibole in various rocks throughout the region. This paper shows the enormous potential of coupling laser Ar‐spot data with thermal modelling to identify and constrain the duration of short‐lived events. An optimal P–T–t history has been derived by modelling the age data from a previously dated large muscovite crystal (Hames & Andresen, 1996, Geology, 24 :1005) and using Zr‐in‐rutile thermometry which is consistent with all geochronological data and geological constraints from the basement zones and allochthon cover. This tectonothermal model history suggests that there have been three episodic hot‐fluid and 40Ar‐free infiltration events, resulting in the total resetting of Ar ages during the Scandian (425 Ma) for 1 Ma at 650°C and two reheating events at 415 Ma for 400 ka at 650°C and at 365 Ma for 50 ka at 600°C, which are modelled as thermal spikes above an ambient temperature of 300°C. Independent confirmation of these parameters was provided by Pb‐diffusion modelling in rutile and titanite. The model suggests that the amphibolite facies rocks of the Leknes Group probably remained cold before being exhumed for at least 60 Ma (425–365 Ma) and successfully explains the presence of different minerals that crystallized or were totally/partially reset in the allochthon and in the basement. The migration of hot fluids for short periods of times within conduits extending through the basement and allochthon rock units is likely associated with episodic seismic activity during the Caledonian orogeny. 相似文献