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241.
242.
243.
The crystal structures, lattice dynamics and magnetic properties of synthetic Co-cordierite, Co2Al4Si5O18, and Mn-cordierite, Mn2Al4Si5O18 have been studied by neutron powder diffraction, infrared spectroscopy and magnetisation measurements. Due to different synthesis
conditions, the Co-cordierite used here crystallised in the hexagonal α-cordierite structure with a disordered Si/Al distribution
in the framework, while for the Mn-cordierite the orthorhombic β-structure has been determined. The experimentally determined
paramagnetic moments,
exp
(Mn) = 5.47(6)
B
and
exp
(Co) = 3.88(4)
B
, are in good agreement with theoretical predictions for octahedrally coordinated Mn2+ and Co2+, respectively. In both compounds there is no magnetic long-range order down to at least 1.5 K. However, the onset of an anti-ferromagnetic
short-range correlation of magnetic moments along [001] has been observed for Mn-cordierite by magnetisation and neutron diffraction
measurements. This short-range magnetic correlation becomes evident from diffuse scattering observed at 2 K. The diffuse scattering
has been interpreted in terms of a Blech-Averbach function.
Received: 30 June 1998 / Revised, accepted: 3 March 1999 相似文献
244.
Bond critical point properties of electron density distributions calculated for representative Si5O16 moieties of the structure of coesite are compared with those observed and calculated for the bulk crystal. The values calculated
for the moieties agree with those observed to within ∼5%, on average, whereas those calculated for the crystal agree to within
∼10%. As the SiOSi angles increase and the SiO bonds shorten, there is a progressive build-up in the calculated electron density
along the bonds. This is accompanied by an increase in both the curvatures of the electron density, both perpendicular and
parallel to each bond, and the Laplacian of the electron density distribution at the bond critical points. The cross sections
of the bonds at the critical points become more circular as the angle approaches 180o. Also, the bonded radius of the oxide
anion decreases about twice as much as that of the Si cation as the SiO bond length decreases and the fraction of s-character of the bond is indicated to increase. A knowledge of electron density distributions is central to our understanding
of the forces that govern the structure, properties, solid state reactions, surface reactions and phase transformations of
minerals. The software (CRYSTAL95 and TOPOND) used in this study to calculate the bond critical properties of the electron
density and Laplacian distributions is bound to promote a deeper understanding of crystal chemistry and properties.
Received: 23 February 1998 / Revised, accepted: 16 July 1998 相似文献
245.
大洋多金属结核矿区沉积物土工性质 总被引:16,自引:0,他引:16
利用1994年大洋多金属结核调查所获得的土工资料,结合以往有关资料进行了综合分析。研究了大洋沉积物类型、沉积物土工性质、土质强度等,为未来海底工程设施和多金属结核开采设备的设计与制造提供依据。 相似文献
246.
We examine results from a cruise in May 1997. CTD casts to near the bottom were made south of the Aleutian Islands, across Amchitka Pass, and north of the islands. We computed a westward geostrophic speed of 123 cm s–1 at 173.5°W in the Alaskan Stream. The computed volume transport there, referred to the bottom, was 25×106m3s–1. On other similar sections, transports were 8–15 × 106 m3s–1. Various complex variations in geopotential height along the Stream apparently altered the cross-stream gradients, and hence the transports. Rotational tendencies were also present. Northward inflow through Amchitka Pass was quite strong (6 × 106 m3s–1). Data north of the islands supported the existence of a zero-velocity reference level of variable depth. 相似文献
247.
248.
An understanding of the behavior of cohesive sediment is required to solve various engineering problems such as scour around bridge elements, mitigation of soil erosion, pavement design, river bed degradation,stable channel design. Pavement foundation designers principally use the California bearing ratio(CBR)to describe the subgrade and subbase materials and their strength. Several laboratory experiments were done to study the variation in the CBR of cohesive mixtures comprised of clay-gravel m... 相似文献
249.
安徽省地震宏观异常日报集成系统是由Android的App、MySQL数据库和PHP网站组合而成的应用管理系统。从设计思路、框架及主要技术实现出发,介绍集成系统的应用成效。 相似文献
250.
卫星遥感器中的CO21.6μm弱吸收带通道测量信号可以反映CO2的近地层浓度分布,是温室气体卫星反演的重要通道之一。HITRAN数据库是建立卫星遥感CO2浓度算法依赖的重要分子光谱参数数据库,目前已经更新到了2012版,不同版本中大气分子谱线参数存在差异。本文利用逐线积分模式LBLRTM,研究了最近3个版本HITRAN数据库(04、08、12版)在CO2的弱吸收带通道上大气光学厚度、透过率的差异,发现04版计算的气体光学厚度普遍偏高,可对CO2造成约38 ppm的低估;08版本得到的气体光学厚度与12版本接近,反演相差2 ppm以内。在此基础上,分析了不同HITRAN数据库对整层CO2变化和近地层CO2变化的敏感性,结果表明:04版对整层和近地面大气的变化敏感性最强,并且放大了近地层信号;08版与12版对整层或近地层CO2的敏感度接近,两者经过卷积后得到的信号无差异。 相似文献