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41.
42.
对于变质岩 Sm-Nd 和 Rh-Sr 同位素年代学来说,其中一个重要问题是等时线矿物之间在一特定的变质事件过程中是否达到并在随后保持同位素平衡。矿物 O 同位素地质测温也是如此。由于许多情况下 Nd、Sr 和 O 在变质矿物中的扩散速率具有可比性,变质矿物之间 O 同位素平衡状况能够为矿物 Sm-Nd 和 Rb-Sr 内部等时线定年结果的有效性提供制约。为了验证其适用性,本文对大别造山带双河超高压榴辉岩和片麻岩 Sm-Nd 和 Rh-Sr 等时线矿物进行了 O 同位素地质测温。尽管Sm-Nd 等时线给出一致的三叠纪年龄(213~238Ma),同一样品 Rb-Sr 等时线却给出侏罗纪年龄(171~174Ma)。片麻岩、榴辉岩和榴闪岩矿物对 O 同位素测温得到600~720℃和420~550℃两组温度,分别对应于约225±5Ma 榴辉岩相变质和约 175±5Ma 角闪岩相退变质条件下停止同位素扩散交换的温度。同一样品三叠纪 Sm-Nd 等时线年龄的保存、侏罗纪 Rh-Sr 等时线年龄的出现以及有规律的 O 同位素温度,表明在角闪岩相退变质过程中,Sr 和 O 在含水矿物(如黑云母和角闪石)中的扩散速率在手标本尺度上比石榴石 Nd 和多硅白云母 Sr 的扩散速率快。在退变质作用过程中,等时线矿物之间的初始同位素比值均一化速率主要受扩散速率慢的矿物控制,而矿物等时线时钟的启动主要受具有高母/子体比值的矿物控制。只有当高母/子体比值矿物具有快的放射成因同位素扩散速率时,才能够应用合理的矿物等时线确定变质再造的时间。 相似文献
43.
在矿床地质研究的基础上,将五龙金矿的内生成矿作用从早到晚划分为5个成矿阶段,分别为纯石英阶段(Ⅰ)、黄铁矿—石英阶段(Ⅱ)、黄铁矿—辉铋矿—石英阶段(Ⅲ)、多金属硫化物—灰色石英阶段(Ⅳ)、碳酸盐阶段(Ⅴ)。对其中具有工业矿化的第二(Ⅱ)和第四(Ⅳ)主成矿阶段进行了石英流体包裹体Rb-Sr法测年,上述两个阶段年龄值分别为120±3Ma和112±1Ma,说明一个中、大型金矿的形成,其主成矿阶段可能要持续8Ma左右。Sr同位素的初始值(Ⅱ:I_(Sr)=0.71541±0.00008,Ⅳ:I_(sr)=0.71603±0.00006)表明,不同成矿阶段的成矿物质来自同一源区,且以壳源为主。 相似文献
44.
铜山岭铅锌多金属矿床位于扬子地块湘南-桂东北坳陷与华夏地块粤北坳陷的拼贴部位,是中国南岭多金属成矿区代表性矿床之一。为确定矿床成矿时代,挑选铜山岭铅锌多金属矿床中含矿矽卡岩的石榴子石进行Sm-Nd同位素定年,获得的等时线年龄为173±3Ma,指示成矿作用发生于燕山早期。对金属硫化物矿物进行了Pb同位素分析,其~(206)Pb/~(204)Pb、~(207)Pb/~(204)Pb、~(208)Pb/~(204)Pb平均值分别为18.602、15.701、38.729,表明成矿物质来源于相对富集铀铅、略微亏损钍铅的上地壳源区。从(~(207)Pb/~(204)Pb)i-(~(206)Pb/~(204)Pb)i铅同位素演化模式图可知,寄主花岗闪长岩是铜山岭铅锌多金属矿床的重要物质来源,且成矿物质中可能含有寄存在花岗闪长岩中的地幔组分。 相似文献
45.
Calculations of isochrons by different methods are compared for the case when both variables are subject to error. Least-squares operations of the kind given by York (1969) and linear methods are compared. The advantage of the linear methods is demonstrated for the case of data reported by Housner and Brennan (1948), which we have modified for nonreplicated sampling. The sampling distribution of the slope is obtained and confidence intervals for it are given. The confidence intervals for the intercept on the ordinate and its distribution are obtained for fixed values of the slope. Examples of application of the method are given, based on data from the literature compiled in Appendix A. 相似文献
46.
47.
Dipankar Pathak 《Geostandards and Geoanalytical Research》2023,47(1):185-197
Isotope dilution (ID) is a widely used analytical technique to determine elemental abundance to a high degree of accuracy and precision, using a spiked isotope tracer. This technique also enables efficient correction of the inevitable phenomenon of analytical mass fractionation during mass spectrometric analysis. It is also used to determine stable isotope variations of an element in a sample relative to a reference material, using tracers enriched in two isotopes (popularly known as the double spike method). Isotope dilution data reduction can be performed in Microsoft® Excel™ using different algorithmic approaches. Additional software such as iolite and MATLAB® offer algorithm implementations to perform these calculations. These are however limited to use within particular laboratories/research groups, or either require additional cost-bound software or some degree of knowledge in computer programming languages for use, or all of these. To ease this situation, a graphical user interface-based software is proposed (here named Parmanu-Gunak, meaning Atom-Calculator in Sanskrit text) to invert both single and double spiked isotope data, with the aim of making it a standard tool for ID data reduction. Examples of Nd and Mo isotopes are used to demonstrate the robustness of the program. 相似文献
48.
49.
Takamoto Okudaira Yasutaka Hayasaka Osamu Himeno Koichiro Watanabe Yasuhiro Sakurai Yukiko Ohtomo 《Island Arc》2001,10(2):98-115
Abstract The Ryoke metamorphic belt in south-west Japan consists mainly of I-type granitoids and associated low-pressure/high-temperature metamorphic rocks. In the Yanai district, it has been divided into three structural units: northern, central and southern units. In this study, we measured the Rb–Sr whole-rock–mineral isochron ages and fission-track ages of the gneissose granodiorite in the central structural unit. Four Rb–Sr ages fall in a range of ca 89–87 Ma. The fission-track ages of zircon and apatite are 68.9 ± 2.6 Ma and 57.4 ± 2.5 Ma (1σ error), respectively. Combining the newly obtained ages with previously reported (Th–)U–Pb ages from the same unit, thermochronologic study revealed two distinctive cooling stages; 1) a rapid cooling (> 40°C/Myr) for a period (~7 Myr) soon after the peak metamorphism (~ 95 Ma) and 2) the subsequent slow cooling stage (~ 5°C/Myr) after ca 88 Ma. The first rapid cooling stage corresponds to thermal relaxation of the intruded granodiorite magma and its associated metamorphic rocks, and to the uplift by a displacement along low-angle faults which initiated soon after the intrusion of the magma. Uplift by the later stage deformation having formed large-scale upright folds resulted in progress of the exhumation during the first stage. The average exhumation velocity of the stage is ≥ 2 mm/yr. During the second stage, the rocks were not accompanied by ductile deformation and were exhumed with the rate of 0.1–0.2 mm/yr. The difference in the exhumation velocity between the first and second cooling stages resulted from the difference in the thickness of the crust and in the activity of ductile deformation between the early and later stages of the orogenesis. 相似文献
50.
激光质谱测定南极乔治王岛北海岸A635玄武岩微区~(40)Ar-~(39)Ar的等时年龄 总被引:1,自引:0,他引:1
采用连续激光直接对岩石光片样品微区熔样,以高灵敏度、高精确度的质谱计测试,对南极乔治王岛玄武岩样品进行(40)Ar-(39)Ar法定年,取得了成功。样品置反应堆中心E-5孔道,以1.8×10(18)n/cm2的快中子总通量照射,时间为50h,放射性冷却后进行测定。样品的加热源为自行设计的Nd:YAG固体激光器,以He-Ne准激光器导光。测定中对4个250μm直径的微区分别在1500℃高温熔融,经Zr-Al泵纯化的气体用MM1200质谱计测量氩同位素各峰值。经计算得到该样品的等时年龄为52.4±1.1Ma,远远低于江个点的视年龄值,而((40)Ar/(36)Ar)>>295.5。这不仅证明该样品含有过剩氩,同时也证明了由K-Ar稀释法得到的偏高年龄值亦是样品中存在过剩氩造成的。激光微区等时年龄的获得进一步厘定了南极乔治王岛北海岸火山岩时代为第三纪,同时证明了我们建立的激光质谱微区、微粒熔样和测定技术是可行的和成功的。 相似文献