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51.
The application of X-ray photoelectron spectroscopy (XPS) to coal surface characterisation for preparation research is described. Progress towards the acquisition of complementary surface chemical information by time-of-flight secondary ion mass spectrometry (ToF-SIMS) is also discussed. Surface-based beneficiation techniques such as flotation are assuming greater importance as the proportion of fines in raw coal increases due to the proliferation of high capacity mining methods. A necessary condition for the floatability of a coal particle is adequate hydrophobicity, and the degree of hydrophobicity of the flotation concentrate is one factor influencing the ease with which its dewatering can be affected. The hydrophobicity of a coal is very difficult to measure directly because of microporosity, and it is often necessary to deduce the degree of hydrophobicity from a knowledge of the surface chemistry. XPS is able to provide sufficient analytical data to allow relative levels of hydrophobicity to be estimated. In principle, ToF-SIMS should be able to supply additional information enabling refinement of such estimates; however, there are insufficient data at present to allow the ionic fragments detected to be related to specific functional groups at the coal surface. 相似文献
52.
超灵敏加速器质谱计测定^32Si样品制备新技术 总被引:1,自引:0,他引:1
介绍了制备元素硅的一种化学方法,它可用于AMS装置的离子源。含硅的物质溶解在HF中,用LiAlH4把SiF4还原成SiH4,再将SiH4加热分解成元素硅,并且沉淀在石墨盘上,用AMS测定w32Si/wSi总比值,其灵敏度可达10^-13。 相似文献
53.
Seepage driving effect on deformations of San Fernando dams 总被引:2,自引:0,他引:2
In the process of flow deformation of an earth dam, the seepage force inside the dam plays a role as a driving force. The seepage force acts just like the gravitational force in terms of pushing soils away from their original locations after liquefaction is triggered. This paper draws attention to this seepage driving effect by presenting a set of fully coupled finite element analyses on the well-known San Fernando dams, with the objective of evaluating the impact of this seepage effect. The results indicate that while this effect is always there, its practical significance depends on a number of factors. In the case of the upper San Fernando dam, which experienced a significant, but restricted, downstream movement during the 1971 earthquake, the seepage driving effect was indeed significant. On the contrary, for the lower dam, which failed and slid into the upstream reservoir during the same earthquake, this seepage effect was relatively less pronounced. The detailed results of the analyses reveal the likely mechanisms of failure and deformation of the two dams and the likely cause behind the difference between their responses during the earthquake. 相似文献
54.
文中重点分析了中国科学院大气物理研究所LASG最新发展的全球大气环流谱模式(R42L9)与一全球海洋环流模式(T63L30)耦合形成的全球海洋-大气-陆面气候系统模式(GOALS/LASG)新版本已积分30 a的模拟结果,通过与多种观测资料的对比分析,讨论了赤道太平洋海表温度(SST)的年际变化及其纬向传播、赤道东太平洋SST异常与其他洋面SST变化之间的遥相关关系、赤道太平洋浅表层海温的年际变化特征等研究内容.结果表明,COALS模式模拟出了赤道太平洋SST异常出现不规则的年际变化特点;赤道东太平洋SST异常的向西传播过程;赤道太平洋混合层海温变化由西向东、由深层向浅层的传播过程;同时也模拟出了赤道东太平洋SST变化与赤道西太平洋以及与西南太平洋海温之间的反相关关系,与南印度洋和副热带大西洋SST之间的正遥相关关系等实际观测现象.但COALS模式也存在明显的不足,如对赤道东、中太平洋SST异常的年际变化幅度明显偏小,没能模拟出赤道东太平洋的SST变化比赤道中太平洋强的特点;赤道太平洋SST从东向西的传播速度明显比实际观测慢得多,但混合层海温极值变化由西向东的传播速度明显比实际情况快得多;没能模拟出赤道东太平洋SST变化同西北太平洋SST的负相关和北印度洋海温变化的正相关现象,因此也影响了对南亚、东南亚降水年际变化的模拟能力. 相似文献
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58.
Numerical simulations for coupled rock deformation and gas leak flow in parallel coal seams 总被引:3,自引:0,他引:3
Peide Sun> 《Geotechnical and Geological Engineering》2004,22(1):1-17
Based on the new viewpoint of interaction mechanics for solid and gas, gas leakage in parallel deformable coal seams can be
understood. That is, under the action of varied geophysical fields, the methane gas flow in a double deformable coal seam
can be essentially considered to be compressible with time-dependent and mixed permeation and diffusion through a pore-cleat
deformable, heterogeneous and anisotropic medium. From this new viewpoint, coupled mathematical models for coal seam deformation
and gas leak flow in parallel coal seams were formulated and the numerical simulations for slow gas emission from the parallel
coal seams are presented. It is found that coupled models might be close to reality. Meanwhile, a coupled model for solid
deformation and gas leak flow can be applied to the problems of gas leak flow including mining engineering, gas drainage engineering
and mining safety engineering in particular the prediction of the safe range using protective layer mining where coal and
gas outbursts can efficiently be prevented.
This revised version was published online in July 2006 with corrections to the Cover Date. 相似文献
59.
In this study, a capillary barrier system was designed and tested for an arid land environment. To simulate arid land conditions
of high temperature and sub-irrigation systems, the barrier was subjected to thermal and hydraulic gradients in opposite directions;
to test the barrier system under these severe conditions, an experimental apparatus was designed and fabricated. The multilayer
capillary barrier consisted of three layers made of silica sand, a mixture of sand and bentonite in equal portions, and a
mixture of clay (25%) and aggregate (75%). Several one dimensional coupled heat and moisture tests were performed. Temperature
variations along the thickness of the barrier were recorded as a function of time, and at the end of each test, the barrier
was sliced into small sections, for the determination of volumetric water content as a function of distance from the heat
source. The experimental results were discussed in view of the barrier's intended purpose of its ability to store moisture
for long time durations.
Coupled heat and moisture flow equations were developed and solved numerically via a finite difference method. Diffusivity
parameters were calculated by using experimental results, a numerical model, and Powell's conjugate directions method of nonlinear
optimization. The model was calibrated and the results were discussed. Good agreement between calculated and experimental
results was obtained.
This revised version was published online in July 2006 with corrections to the Cover Date. 相似文献
60.
A coupled hydro-chemo-mechanical numerical model is developed for these coupled phenomena in many engineering fields. The
model has been applied to predicting the response of a stressed rockmass column to an injected reactive fluid (reagent) flow.
The response includes evolutions of porosity, permeability, reagent and mineral concentrations during dissolution. In the
model, the progress of dissolution is defined by the change in porosity ratio and the porosity increases with dissolution
assuming there is no precipitation. The numerical evolutions of porosity, permeability, reagent and mineral concentrations
during dissolution are validated against steady state solutions. The model results show that these evolutions are regulated
to a certain extent by the applied external loadings: an applied extensional stress enhances the progress of the dissolution
process while an applied compression stress slows the progress of the dissolution process.
This revised version was published online in July 2006 with corrections to the Cover Date. 相似文献