新型磁选装置的研制及其应用于分离超贫磁铁矿中的磁性铁

磁性铁是超贫磁铁矿勘查中的基本分析项目之一,为准确测定磁性铁的含量,首先需要实现磁性铁的定量分离。目前常用的手工内磁选法由于所用磁铁的有效磁场强度难以保证,而且受人为操作的影响较大,导致分析结果的重现性差。本文应用50 m L滴定管、电磁铁和三相异步电动机,研制了一种新型磁选装置——电磁式磁性铁分选装置,实现了超贫磁铁矿中磁性铁与非磁性铁的定量分离,结合重铬酸钾容量法建立了超贫磁铁矿中磁性铁的分析方法。在选定的磁选条件下(电流2.5 A,磁选管运动频率40 r/min,磁选时间5 min)分析铁矿石标准物质,磁性铁的测定值与标准值的相对误差小于1.0%;分析采自实际矿区的超贫磁铁矿样品,磁性铁的测定结果与手工内磁选法一致,且相对标准偏差(RSD,n=5)小于1.0%,优于手工内磁选法的精密度。本方法采用的电磁式磁性铁分选装置有效地控制了磁场强度的强弱,避免永磁铁出现磁损失,同时可以量化磁性铁分离的参数,提高了磁性铁的分析精度。     

载炭泡塑吸附-电感耦合等离子体发射光谱法测定金矿石的金量

载炭泡塑吸附法对金有良好的吸附性能,但只能用于抽滤吸附不能振荡吸附,分析手续繁杂。本文以载炭泡塑振荡吸附-电感耦合等离子体发射光谱法测定金矿石的金量。样品在650℃高温灼烧2 h,用50%王水和10%氯化铁加热溶解,溶液冷却后加入5%高锰酸钾氧化,用中密度规格的载炭泡塑两次振荡吸附溶液中的金,然后于580℃高温灼烧后以50%王水溶解灰分,直接用ICP-OES测定金量。方法检出限(3σ)为0.002μg/g,精密度(RSD,n=11)小于3.7%。本方法对金的吸附率大于99.9%,测定范围为0.01~90μg/g,对不同类型金矿石的适应性强,解决了以往泡塑吸附法吸附率较低、标准系列与样品需同时预处理的问题,对低含量和高含量样品均有较高的准确度。     

云南昭通铅锌矿pH-logfo_2和pH-loga相图对铅锌共生分异的制约

云南昭通大型铅锌矿是滇东北矿集区乃至川滇黔铅锌成矿域铅锌矿床的典型代表。矿床具有明显的矿物组合分带性的特点,区别于典型的MVT型铅锌矿床。根据矿物组合特征构建、计算、绘制了该矿床的p H-logfo2、p Hloga相图,剖析了铅锌矿共生分异的形成机理。研究表明p H、氧逸度、组分浓度的协同作用造成了铅、锌的共生分异,对矿物组合分带起控制作用,且温度下降、氧逸度升高和p H升高有利于金属硫化物的沉淀,成功解释了昭通铅锌矿床独具特色的矿物分带地质特征。     

空气（泡沫）潜孔锤钻进工艺在王家岭煤矿紧急避险孔中的应用

空气（泡沫）潜孔锤钻进工艺在王家岭煤矿紧急避险孔钻进中,有效解决了钻孔垂直度要求高、地层漏失等施工难点,实现了高质量快速成孔。该工艺平均机械钻速高达7.99 m/h,终孔水平位移仅为0.48 m,二开孔段每米综合成本504.8元。邻孔SW1水文补勘孔以泥浆作为循环介质、采用牙轮回转正循环钻进工艺,平均机械钻速为0.86 m/h,二开孔段每米综合成本为820.5元。前者平均机械钻速约是后者的9倍,较后者节约成本38.5%。与邻孔泥浆正循环牙轮回转钻进工艺相比,该工艺不仅解决了紧急避险孔施工难点,还提高了孔身质量、节约了工期、降低了成本,达到降本增效的目的,值得类似工程借鉴。     

http://www.sciencedirect.com/science/article/pii/S167498711300162X

Seismic observations have shown structural variation near the base of the mantle transition zone(MTZ)where subducted cold slabs,as visualized with high seismic speed anomalies(HSSAs),flatten to form stagnant slabs or sink further into the lower mantle.The different slab behaviors were also accompanied by variation of the "660 km" discontinuity depths and low viscosity layers(LVLs) beneath the MTZ that are suggested by geoid inversion studies.We address that deep water transport by subducted slabs and dehydration from hydrous slabs could affect the physical properties of mantle minerals and govern slab dynamics.A systematic series of three-dimensional numerical simulation has been conducted to examine the effects of viscosity reduction or contrast between slab materials on slab behaviors near the base of the MTZ.We found that the viscosity reduction of subducted crustal material leads to a separation of crustal material from the slab main body and its transient stagnation in the MTZ.The once trapped crustal materials in the MTZ eventually sink into the lower mantle within 20-30 My from the start of the plate subduction.The results suggest crustal material recycle in the whole mantle that is consistent with evidence from mantle geochemistry as opposed to a two-layer mantle convection model.Because of the smaller capacity of water content in lower mantle minerals than in MTZ minerals,dehydration should occur at the phase transformation depth,~660 km.The variation of the discontinuity depths and highly localized low seismic speed anomaly(LSSA) zones observed from seismic P waveforms in a relatively high frequency band(~1 Hz) support the hypothesis of dehydration from hydrous slabs at the phase boundary.The LSSAs which correspond to dehydration induced fluids are likely to be very local,given very small hydrogen(H~+) diffusivity associated with subducted slabs.The image of such local LSSA zones embedded in HSSAs may not be necessarily captured in tomography studies.The high electrical conductivity in the MTZ beneath the northwestern Pacific subduction zone does not necessarily require a broad range of high water content homogeneously.     

北京土地利用混合度对居民职住分离的影响

市场经济体制改革以来,中国城市土地利用方式发生巨大变化,深刻影响居民日常生活。尽管国内外学者关注土地利用方式对居民通勤行为的影响,然而其研究方法均采用简单的单层模型,未能将数据的多层嵌套关系纳入模型中。为解决这一问题,本文采用多层线性模型(Multilevel Models),以北京为例,同时分析了在居住地和工作地层级上的街道土地利用混合度对居民职住分离的影响,以及居民住房情况和社会经济属性对其职住分离的影响。研究结果表明,微观层面的土地利用混合度的提升的确有利于减轻个体的职住分离;个体所在的工作地土地利用方式也对其职住分离产生影响,而且工作地对个体的影响要比居住地的影响更大;居民的社会经济属性、住房情况等对其职住分离程度存在显著的影响;交叉分类多层线性模型适用于解决存在复杂嵌套关系的影响因素分析。     

Parameters affect foaming and foam stability during foam drilling

The authors presented indoor practice experiments of parameters affect on foaming and foam stability. Experiments were carried out and special equipments were used to determine foaming and foam stability; tests were tabulated and charted. The effects of chemical and physical parameters on foaming and foam stability have been conducted.     

致密对称源OQ208自行的研究

利用美国甚长基线阵,在5GHz和8GHz波段观测致密对称源(CSO)OQ208,由获得的总流量图均显示OQ208是由2个主要的射电结构组成。5GHz波段在该源西南(SW)部分和东北(NE)部分都探测到2个子源。8GHz波段在该源(SW)部分探测到2个子源,而在(NE)部分探测到3个子源。在5GHz波段,根据子源A和D自1993年到2001年间的5个时段VLBI观测成图结果,拟合出它们的分离速度为0.037±0.006mas/a(年)。在8GHz波段,根据1994年到2002年间的9个时段观测数据,获得子源A和C的分离速度为0.046±0.009mas/a。     

Towards identifying sources of subsurface flow: A comparison of components identified by a physically based runoff model and those determined by chemical mixing techniques

A physically-based semidistributed model, TOPMODEL, is applied to a 340 hectare spruce forested catchment in mid-Wales. the model is calibrated to runoff and the subsurface flow is divided into components of flow identified by depth of origin. in addition, chemical mixing techniques are used to provide a hydrograph separation between acidic soil waters and well buffered deep waters. the short-term variations in the components of flow identified by these two approaches compare well.     

北京夏季日最大电力负荷预报模型建立方法探讨

为了探索夏季(6～8月)日气象负荷的最佳分离方式和引起日最大电力负荷波动的主要因子,以及建立预报模型最佳个数,基于北京市2005～2010年逐日最大电力负荷和同期的气象资料,分析了北京地区日最大电力负荷的变化规律,采用不同方法将气象负荷从夏季日最大电力负荷中分离出来,分析北京夏季气象负荷与气温、相对湿度、降水及炎热指数、高温持续日数、炎热日数持续时间、前一日气象负荷等因子之间的关系,并基于2005～2009年夏季逐日气象负荷和其主要影响因子采用逐步回归方法建立日最大电力负荷的预报模型,将2010年夏季北京日最大电力负荷作为预报效果的独立样本检验。结果显示:2005～2010年,北京逐日最大电力负荷具有明显的线性增长趋势,夏季日最大电力负荷具有显著的星期效应;与去掉逐年夏季日最大电力负荷趋势和夏季平均日最大电力负荷趋势相比,去掉全年逐日最大电力负荷变化趋势的夏季日气象负荷预报模型的拟合能力更优;北京夏季日气象负荷与当日气温的相关系数最高,与前一日气象负荷也关系密切;利用前一日相对气象负荷和当日气象要素一周逐日分别建立预报模型的拟合和预测效果较好。