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361.
A cryogenic system for the airborne and ground based sampling of ambient radicals by matrix isolation is described. The trapped radicals, e.g., NO2 and RO2, are analyzed by ESR. The technique has been improved, mainly by addition of water vapor to the sampled air, to yield a collection efficiency of (90±10)% and a lower detection limit of about 20 ppt, but it still does not distinguish between the different RO2. Careful calibration reduced the measurement error (1 ) to ±10% for NO2 and ±15% for HO2. Two diurnal variations of RO2 and NO2 at ground level and vertical profiles in the lower troposphere are presented. 相似文献
362.
A study has been made of solid and solution electron paramagnetic resonance (EPR) spectra of humic acids from different horizons in a podzolic soil. Hyperfine splitting was observed in the solution spectra of humic acids from all horizons and depended on the strength of alkali and the period of dissolution. The upper organic horizons L, F and O1 contained humic acids with some spectral characteristics in common with lignin. Humic acid from the lower horizons showed different spectra. At least 5 different radical signals were present. 相似文献
363.
364.
Miryam Glikson 《Organic Geochemistry》1984,7(2):151-160
Transmission electron microscopy of torbanites from various localities in eastern Australia has revealed micro-organisms of possible methanogenic affinity. Botryococcus remains in the torbanites displayed close resemblance to the rubbery B. braunii accumulations deposited in recent bodies of freshwater origin. Compaction and collapse of structure seem to be the major visible alteration to the algal colonies. C-isotope compositions of the torbanites favour methanogenic activity. Comparison with recent botroyococcal accumulations support diagenetic alteration at a very early stage of deposition. 相似文献
365.
D. Mihelcic D. Klemp P. Müsgen H. W. Pätz A. Volz-Thomas 《Journal of Atmospheric Chemistry》1993,16(4):313-335
We present simultaneous field measurements of NO3 and peroxy radicals made at night in a forested area (Schauinsland, Black Forest, 48° N, 8° N, 1150 ASL), together with measurements of CO, O3, NO
x
, NO
y
, and hydrocarbons, as well as meteorological parameters. NO2, NO3, HO2, and (RO2) radicals are detected with matrix isolation/electron spin resonance (MIESR). NO3 and HO2 were found to be present in the range of 0–10 ppt, whilst organic peroxy radicals reached concentrations of 40 ppt. NO3, RO2, and HO2 exhibited strong variations, in contrast to the almost constant values of the longer lived trace gases. The data suggest anticorrelation between NO3 and RO2 radical concentrations at night.The measured trace gas set allows the calculation of NO3 and peroxy radical concentrations, using a chemical box model. From these simulations, it is concluded that the observed anthropogenic hydrocarbons are not sufficient to explain the observed RO2 concentrations. The chemical budget of both NO3 and RO2 radicals can be understood if emissions of monoterpenes are included. The measured HO2 can only be explained by the model, when NO concentrations at night of around 5 ppt are assumed to be present. The presence of HO2 radicals implies the presence of hydroxyl radicals at night in concentrations of up to 105 cm–3. 相似文献
366.
It has been known for many years that depositional method plays an important part in the results of laboratory testing of clean sands. In this paper, undrained triaxial compression tests were performed on specimens composed of Nevada sand with 20% non-plastic silt content using a variety of depositional methods that include slurry deposition, water sedimentation, air pluviation, mixed dry deposition, and dry funnel deposition. It was found that there was a marked difference in the undrained behavior even though the density and stress conditions were identical. The conclusion was that the soil fabric was responsible for this result. Using the scanning electron microscope, a method was developed to examine and quantify the microstructure of silty sand. These results appear to indicate that there are internal particle structures in sand with silt and their relative quantities correlate with the observed macroscopic undrained behavior. 相似文献
367.
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369.
LIU Fulai SHEN Qihan Institute of Geology Chinese Academy of Geological Sciences Beijing 《《地质学报》英文版》2003,77(1):28-35
The early Precambrian khondalite series is widely distributed in the Jining-Zhuozi-Fengzhen-Liangcheng area, southeastern Inner Mongolia. The khondalite series mainly consists of sillimanite garnet potash feldspar (or two-feldspar) gneiss and garnet biotite plagioclase gneiss. These gneissic rocks have commonly experienced granulite-facies metamorphism. In zircons separated from sillimanite garnet potash feldspar gneisses, many mineral inclusions, including Sil, Grt, Ky, Kfs, Qtz and Ap, have been identified by the Laser Raman spectroscopy. Generally, prograde metamorphic mineral inclusion assemblages such as Ky + Kfs + Qtz + Ap and Ky + Grt + Kfs + Qtz are preserved in the core of zircon, while peak granulite-facies metamorphic minerals including Sil + Grt + Kfs + Qtz and Sil + Grt + Kfs + Qtz + Ap are identified in the mantle and rim of the same zircon. However, in some zircons are only preserved the peak metamorphic minerals such as Sil + Grt + Kfs + Qtz and Sil + Grt + Kfs + Qtz + Ap from core to ri 相似文献
370.
矿山防治水工作是矿山开发的基础性工作,对煤炭工业的可持续性发展有越来越重要的意义。今后,煤矿防治水应引入新的观念,拓展新的领域,满足新的需求。文章对今后防治水领域中的一些关键性问题,如深部岩溶。弱合水层和隔水层的合理利用,延迟突水、环境、防治水工作的协调发展等问题做了讨论。 相似文献