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71.
本法采用氯酸钾-王水分解样品,选用硝酸镍作基体改进剂,提高了灰化温度。使用石墨杯原子化器,Zeeman效应扣除背景,实现了用石墨炉原子吸收法直接测定硅酸盐中微量砷。快速、简便,其绝对灵敏度达5.7×10~(-11)(g/l%),变动系数小于8%。 相似文献
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在伊朗卡尔赫水电站坝址工程勘察中,采用金刚石双管单动钻具和SM胶冲洗液进行取样钻探,用清水钻进压水试验,由于钻探工艺合理,钻探质量均达到了设计要求。 相似文献
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P. S. A. Jones 《地球表面变化过程与地形》1984,9(5):479-484
The oxygen plasma furnace enables small samples of clastic sediment to be separated from filter papers at low temperatures without physical or chemical alteration of the sediment. This technique provides a suitable treatment for processing very small samples of alpine eolian sediment, enabling their grain size distribution, mineralogy, and origin to be determined. 相似文献
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Fire has long been recognized as an agent of rock weathering. Our understanding of the impact of fire on stone comes either from early anecdotal evidence, or from more recent laboratory simulation studies, using furnaces to simulate the effects of fire. This paper suggests that knowledge derived from simulated heating experiments is based on the pre‐conceptions of the experiment designer – when using a furnace to simulate fire, the operator decides on the maximum temperature and the duration of the experiment. These are key factors in determining the response of the stone to fire, and if these are removed from real‐world observations then knowledge based on these simulations must be questioned. To explore the differences between heating sandstone in a furnace and a real fire, sample blocks of Peakmoor Sandstone were subjected to different stress histories in combination (lime rendering and removal, furnace heating or fire, frost and salt weathering). Block response to furnace heating and fire is discussed, with emphasis placed on the non‐uniformity of the fire and of block response to fire in contrast to the uniform response to surface heating in a furnace. Subsequent response to salt weathering (by a 10% solution of sodium chloride and magnesium sulphate) was then monitored by weight loss. Blocks that had experienced fire showed a more unpredictable response to salt weathering than those that had undergone furnace heating – spalling of corners and rapid catastrophic weight loss were evidenced in blocks that had been subjected to fire, after periods of relative quiescence. An important physical side‐effect of the fire was soot accumulation, which created a waxy, relatively impermeable layer on some blocks. This layer repelled water and hindered salt ingress, but eventually detached when salt, able to enter the substrate through more permeable areas, concentrated and crystallized behind it, resulting in rapid weight loss and accelerated decay. Copyright © 2007 John Wiley & Sons, Ltd. 相似文献
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正交实验法在测绘仪器检定中的应用 总被引:2,自引:0,他引:2
在测绘生产和科研项目中,为了改革旧工艺或对新仪器,新产品,经常需要做多因素实验,如何安排多因素实验,是一个很值得研究的问题,文中以数字水准仪及标尺综合精度的检定为例,介绍了正交实验法在测绘仪器检定中的应用。 相似文献