古交矿区8号煤的实验室热解脱硫

介绍了古交矿区8号煤在不加催化剂和加催化剂两种条件下的实验室热解脱硫试验情况．结果表明，在不加催化剂时，升温速度为5～10℃／min脱硫效果最好，脱硫率大于40％；当在原煤中添加催化剂AlCl3和NH4Cl时，有较好的脱硫作用，焦炭中灰分也没有明显提高，而当添加催化剂CuCl2和CaO时，不能脱除煤中硫。并据此提出了建议脱硫方案。     

尽快建立煤炭地质单位信用管理制度

煤炭地质单位尚未建立有效地信用管理制度，威胁了煤炭地质经济的持续健康发展。煤炭地质单位领导要高度重视信用管理，尽快设立专门的信用管理机构，规范内部管理，防范经营风险。     

开滦林南仓井田岩浆岩侵入规律及找煤方向探讨

通 过地 面钻孔 、井下 开采和 磁法 勘探,发现 井 田内 赋存 有 大量 的岩 浆 岩体 ,特 别是 西二 采 区发 育岩 床 ,使该 区可采 储量 急 剧减 少,严重 影 响了 井田 采 掘 工 程的 衔 接 ,使 矿 井 生产 处 于 被 动局 面 。 通过 对 岩 浆 岩侵 入 规 律 的深 入 研究,预 测了井 田岩 床的分 布范 围和面 积,对 区域找 煤以 及为矿 井生 产和可 持续 发展具 有现 实的指 导意 义。     

急倾斜煤层开采地表沉陷的渐近灰色预测

煤层开采所引起的地表沉陷是一种严重的矿区地质灾害。煤层的倾角、厚度等物理条件是地表沉陷的主要影响因素。在水平煤层或缓倾斜煤的开采过程中，由于地层倾角小，地表沉陷具有较完整的规律性，其预测效果也比较理想。但是，在急倾斜煤层的开采中，由于地层倾角较大，赋存条件和地质体物理力学性质的差异，增强了地表下沉的非线性特征，使地表沉陷具有不确定的表现规律。文章对重庆市南桐矿区东林矿的地表沉陷非线性特征进行了探讨，得到了东林煤矿地表下沉曲线的分形维数是1．07。在岩层移动这个系统当中，既含有已知的又含有未知的或非确定的信息，可以作为一个灰色系统来研究。岩层控制系统的状态、结构和边界条件难以精确描述，属本征性灰色系统。文章针对东林煤矿地表下沉曲线非线性较弱的性质，提出用一种基于GM(1，1)的渐近预测模型对东林煤矿42个月的地表下沉量时间序列进行探讨。结果表明，这种模型对急倾斜层开采地表沉陷的预测是一种行之有效的方法。通过对其他工程实例的应用分析，进一步证明这种渐近的灰色预测方法具有相对较高的精度，是一种比较实用的地表沉陷预测方法，具有广泛的工程实用空间。     

高密度电阻率法在探测煤层露头中的应用

新 疆 含 煤 地 层 具 有 地 层 倾 角 大 、煤 层 厚 度 较 大 、上 覆 第 四 系 厚 度 薄 等 特 点 ,适 宜 用 高 密 度 电 阻 率 法 追 踪 煤层 露 头 。新 疆 煤 田 地 质 局 物 测 队 使 用 复 合 对 称 四 极 剖 面 法 、联 合 剖 面 法 和 中 间 梯 度 法 等 方 法 ,在 拜 城 县 梅 斯 布 拉 克矿 区 探 测 煤 层 露 头 的 隐 伏 位 置 ,收 到 了 很 好 的 效 果 。     

测试超细煤粉粒度的实验研究

利用激光粒度仪测试超细煤粉的粒度。对测试超细煤粉试样粒度时的试样浓度、测试温度、分散时间、分散剂的种类及浓度等方面的影响进行了实验研究，给出了激光粒度仪测试超细煤粉粒度的最佳实验条件。     

含煤盆地煤储层后期改造形式及对煤层气选区影响--以华北克拉通选区为例

阐述了改造型含煤盆地煤储层被改造的两种形式；煤体结构的改造及构造煤的形成原因；后生充填物对煤层孔隙的改造及形成原因。提出了以构造煤发育程度作为改造型含煤盆地改造强度的一个指标。概述了华北克拉通盆地由中生代剪压应力转化为新生代剪张应力和拉张应力，而在盆地内形成以挤压构造为主到伸展构造为主的演化历程，及不同构造类型的区域分布，指出这种演化极易形成构造煤和后生充填物。提出将华北克拉通含煤盆地分为3种改造类型及其分布区域，分析了各自区域的煤储层物性及对煤层气开发选区的影响。提出应重视鄂尔多斯盆地侏罗纪煤层的煤层气．研究与开发．     

Numerical simulations for coupled rock deformation and gas leak flow in parallel coal seams

Based on the new viewpoint of interaction mechanics for solid and gas, gas leakage in parallel deformable coal seams can be understood. That is, under the action of varied geophysical fields, the methane gas flow in a double deformable coal seam can be essentially considered to be compressible with time-dependent and mixed permeation and diffusion through a pore-cleat deformable, heterogeneous and anisotropic medium. From this new viewpoint, coupled mathematical models for coal seam deformation and gas leak flow in parallel coal seams were formulated and the numerical simulations for slow gas emission from the parallel coal seams are presented. It is found that coupled models might be close to reality. Meanwhile, a coupled model for solid deformation and gas leak flow can be applied to the problems of gas leak flow including mining engineering, gas drainage engineering and mining safety engineering in particular the prediction of the safe range using protective layer mining where coal and gas outbursts can efficiently be prevented. This revised version was published online in July 2006 with corrections to the Cover Date.     

Design of backfilled thin-seam coal pillars using earth pressure theory

In underground coal mining any increase in coal recovery rate is dependent on a decrease in pillar size. Backfilling is one way of reducing the required size of pillars and hence the volume of coal left underground. Therefore any comparisons made between a self-supported mine layout and backfill supported mine layout are based directly on pillar design. The most effective way to examine the effect of backfill on pillar support, and subsequently the rate of recovery, would be to incorporate the mechanisms of backfill support directly into the current design procedure for coal pillars. This paper presents a review of the mechanics of backfill support, a method of estimating the magnitude of that support based on earth pressure theory, and an example that incorporates backfill support into current coal pillar design.     

Direct Current Plasma Emission Spectrometric Determination of Major, Minor and Trace Elements in Microwave Oven Acid Leachates of Powdered Whole Coal Samples

Major concentrations of Al₂O₃, Fe₂O₃, MgO, CaO, Na₂O and K₂O, minor levels of TiO₂, P₂O₅ and thirty petrologically, geochemically and environmentally significant trace elements have been determined in microwave oven acid leachates of whole powdered coal samples by direct current plasma‐atomic emission spectrometry (DCP‐AES). A single sample preparation procedure was suitable for all the determinations with no additional dilution step for major elements solution. Dried samples (0.5 g) were treated in low‐pressure PFA digestion vessels with HF/HCl/HNO₃/HClO₄ acids to quantitatively extract the analytes from the bulk material, while leaving the major part of organic matrix as a residue. The major constituents of geological samples, in particular the easily ionised elements (EIEs) such as alkali and alkaline earths, may complicate the instrumental determinations in DCP‐AES because of differential enhancements of elemental emission intensities and stray light interferences. Taking account of these factors, the coal matrix is considered to have very low major oxide totals as compared to many other common geo‐environmental and related materials (rocks, sediments, soil, ashes etc.). The sample size employed here, while yielding a relatively concentrated solution to cover a wide range of elemental determinations, provided a sample matrix that significantly diminished interferences for DCP measurements. The need for closely matching the unknowns and calibrators was eliminated except for overall acidity and an excess quantity of caesium for EIE buffering. Calibration of the spectrometer was accomplished by simple aqueous single element solutions as high concentration calibrators in addition to a reagent blank as a low concentration calibrator. Two point working curves were established to allow for the maximum concentrations of each element expected in the unknowns. The precision of determinations under routine conditions as well as the reproducibility of the leaching and precision of instrumental measurements have been evaluated. Relative standard deviations (RSD) were of 1–2% for those elements whose concentrations in solid samples were well above the limits of quantification. Method detection limits in the buffered solutions were also evaluated. To evaluate the accuracy of the microwave oven‐DCP method a suite of eight certified coal reference materials of differing rank, were analysed with good agreement with the certified and/or available published data. Results are presented for the uncertified major oxides in the AR series reference materials.