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91.
氢化物发生—原子荧光光谱法测定煤样中的硒 总被引:6,自引:2,他引:6
采用氢化物发生原子荧光光谱法测定了煤样中的总Se。煤样选用高压闷罐强酸消解的方法进行处理,所得消解液经6mol/L HCl将Se(Ⅵ)还原为Se(Ⅳ),然后进行测定。标准工作曲线的线性范围为0-400μg/L Se,检测限为0.4μg/L Se。用标准参考物质煤飞灰对方法进行了验证,所得总Se含量与标准值相符,对ω为10^-6级Se的4次测定,RSD≤4.5%。 相似文献
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Luo Yan Liu Yongsheng Hu Shenghong Gao Shan Open Laboratory of Constitution Interaction Dynamics of the Crust Mantle System Ministry of National Lands Resources China University of Geosciences Wuhan Lin Shoulin Faculty of Material Sc 《中国地质大学学报(英文版)》2001,12(3)
INTRODUCTIONLaserablationinductivelycoupledplasmamassspectrome tryisanincreasinglydevelopedanalyticaltechniqueforsolidsampleanalysis.LA ICP MSoffersattractivecharacteristicsofhighsensitivity ,lowdetectionlimits,minimalsampleprepara tion ,lessoxidesinterfe… 相似文献
94.
本文论述用地面伽玛能谱资料估计地层(体)含铀性和资源量方法,并提出富铀富集体、铀源富集体、尤其富铀源富集体是最有利于成矿的结论。 相似文献
95.
作者对激光热透镜光谱法测定微量钼进行了研究.试验表明,在丙酮介质中,Mo6+能被还原成Mo5+并形成钼蓝同多酸,最大吸收彼长在670um处,利用He-Ne激光器输出的632.8um的激光作光源,进行微量钼的热透镜法分析测定.两酮的存在能增强热透镜信号强度。钼含量在0.01—2.0μg/mL范围内与激光热透镜信号强度呈良好的线性关系,方法检出限为0.005μg/mL钼,已用于地质样品中微量钼的高灵敏度测定.结果满意. 相似文献
96.
王建民 《紫金山天文台台刊》1999,18(3):271-273
频繁的超新星爆发可用以解释活动星系核与类星体的超高金属丰度。星团中的恒星与吸积盘相互作用导致致密天体中子星和黑洞的形成率很高,这些致密天体与红巨星很容易形成双星系统,而后形成(NS/BH,NS/BH) 双星由于引力辐射最终导致并合而形成伽玛射线爆发。我们估计了伽玛射线爆的爆发频率,发现与观测相符。 相似文献
97.
X射线荧光光谱分析检出限问题的探讨与建议 总被引:12,自引:5,他引:7
对有关X射线荧光光谱分析低含量元素的检出限问题进行了多方面的探讨。从检出限的定义及其定义下的相对标准偏差到各种不同测量、校准与校正方法的检出限及其相对应的相对标准偏差进行计算。提出了以定义检出限的相对标准偏差为基准,对各种测量方法计算出的检出限进行重新界定,从而确认一个具有可比性的、精度一致的检出限。同时还讨论了仪器与X光管固有杂质元素谱线对该元素检出限的影响;测量仪器、测量条件与测量时间对检出限的影响;不同岩性试样对检出限的影响;检出限与测定限等问题。 相似文献
98.
Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) has been applied to determine the elemental composition of the surface layer, as well as of the first interior layer, of quartz grains from the mine tailings from Kristineberg (northern Sweden) in order to determine concentration gradients between these two layers. The quartz grains were collected from the oxidized and unoxidized zones within the tailings. The aim of this study is to assess the role of quartz surfaces as sites for the attenuation of solutes from the mine-tailings porewater. Concentrations of Cu, Ag, Sb, Pb and Bi are highest near the surface of each grain and decrease towards the interior. The surface concentration of Cu, Zn and Pb is more pronounced within the unoxidized than within the oxidized zone of the tailings. Cu exhibits a distinct concentration peak at the surface of the quartz grains below the pre-remediation oxidation front. For Zn and Ce the trend of high surface concentration is less pronounced than for Cu or Pb. Silver, Bi and As are preferably adsorbed within the uppermost layers of the oxidized zone where the pH is as high as 6.2. The conversion of intensity signals of the elements to concentration values in ppm was done by using external standards (NIST silicate glass). 相似文献
99.
Statistical Properties of the Highest Pulses in Gamma-Ray Bursts 总被引:1,自引:0,他引:1
Yi-Ping Qin En-Wei Liang Guang-Zhong Xie Cheng-Yue SuNational Astronomical Observatories Yunnan Observatory Chinese Academy of Sciences Kunming qinyp@public.km.yn.cnDepartment of Physics Guangxi University Nanning eloy@iaa.esDepartment of Physics Guangdong Industry University Guangzhou 《中国天文和天体物理学报》2003,3(1):38-48
We study the statistical properties of the highest pulses within individual gamma-ray bursts (GRBs). A wavelet package analysis technique and a developed pulse-finding algorithm have been applied to identify the highest pulses from burst profiles observed by BATSE on board CGRO from 1991 April 21 to 1999 January 26. The statistical light curves of the highest pulses in four energy channels have been derived by an aligning method, which illustrate the temporal evolution of the pulse emission. Our result that narrower pulses go with higher energies is consistent with previous findings. By normalizing both the pulse durations and counts to unity, “characteristic” profiles of the highest pulses in the four channels are also derived. The four characteristic profiles are turned out to be almost the same, thus strongly support the previous conclusion that the temporal profiles in different energy channels are self-similar and the previous conjecture on GRB pulses, implying that the emission process is similar at different energies. The cosmological time dilation effect is examined by investigating the relationship between the pulse flux and pulse duration. An anti-correlation between the two was found, which agrees with the expectation of the cosmological time dilation effect. Also, the evolution of the pulse duration with the observational epoch is studied. The result shows that the pulse duration tends to be shorter in later epochs. This trend cannot be explained by the present theoretical models, and may represent a great challenge to current theories. 相似文献
100.