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71.
Stem wood of the Angiosperm Calluna vulgaris (Scotch heather), isolated at different depths from a selection of raised bog peat deposits, was chemically characterized using in-source pyrolysis mass spectrometry (Py-MS) and Curie-point pyrolysis gas chromatography mass spectrometry (Py-GC-MS). Light microscopy was performed to relate mass spectrometric characteristics with anatomical features. Peatified wood samples, isolated from increasing depth show a gradual decrease in carbohydrate content. This decrease in anatomically reflected in a selective removal of secondary cell wall material from the fibre-tracheids and wood parenchyma. During prolonged peatification a selective removal of hemicellulose sugars is observed, while a part of the cellulose fraction is preserved. This highly resistant cellulose is mainly located in the secondary cell walls of the vessels. The lignin macromolecule is preserved, but a gradual decrease in syringyl to guaiacyl ratio (S/G) is observed during peatification. Because no increase in catechol and phenolic compounds is observed, we conclude that S/G shifts are due to removal the of syringyl-rich secondary cell wall material and the retention of guaiacyl-rich compound middle lamella. Small chemical changes in the lignin macromolecule involve shifts in oxygen substitutions on the aliphatic side chains of the methoxyphenolics and the occurrence of aromatic acids. 相似文献
72.
J. P. McGreevy 《地球表面变化过程与地形》1985,10(5):509-518
Honeycomb weathering has been observed in a Carboniferous sandstone at a coastal location near Ballycastle on the north coast of Northern Ireland. Specimens of this sandstone have been analysed by X-ray diffraction, scanning electron microscopy, and energy dispersive spectrometry. Results reveal that calcium sulphate (gypsum) is the only salt present and is found only at and immediately below the rock surface. SEM observations suggest that crystallization of salts in pores could easily dislodge quartz grains to promote granular disintegration, whilst etching of quartz grain surfaces attests to chemical weathering activity within the rock However, the reason for the development of the honeycomb pattern is not known. 相似文献
73.
A sequential fractionation procedure employing a series of selected mild organic solvents of different polarity has been applied for the isolation of chemically different organic fractions from a brown coal humic acid. Elemental composition, molecular weight distribution, i.r. and electron spin resonance analysis were carried out on the isolated humic fractions. They were characterized by: (a) a low polydispersity, (b) a decreasing aliphatic and increasing aromatic character along the series, (c) very different molecular weight which significantly correlated with E4/E6 ratios (particle aggregation and molecular association) and free radical concentrations (chemical and biochemical activity). Significant correlations were found between physico-chemical parameters of the isolated humic fractions, i.e. Mn, Mw, E4/E6 ratios, spins/g contents and the dielectric constants of the solvents used. This suggested the efficiency of the applied procedure in isolating chemically different organic fractions from the bulk, original humic acid. 相似文献
74.
Electron microscope analysis of sixty samples taken from six colluvium sites in Swaziland has shown that the quartz grains exhibit marked edge abrasion in the uppermost beds of exposures. This edge abrasion is lacking in the lower beds in all sections examined and indicates slope process change during colluvium deposition. A model of slope evolution is provided, in which slope erosion progressively brings about more channelling and causes greater surface roughness because of the exhumation of more core stones and differentially weathered rock. This roughness causes increased edge abrasion. 相似文献
75.
Results from long term microerosion meter (MEM) studies indicate that microenvironments are characterized by different erosion rates. A complementary study, carried out on the same sites, examines the microscale morphology in each environment. Optical and scanning electron microscopy were used to identify a range of features thought to reflect different processes. Under subaerial conditions micromorphology is dominated by biological weathering features owing to the presence of microflora. Sites permanently covered by soil or stream water have only dissolution etch features, though stream sites may exhibit microfractures. Sites with periodic exposure exhibit both dissolution and biological etch features. The natural environment is more accurately reflected by allowing some microflora colonization of MEM sites rather than preventing colonization by artificial means. 相似文献
76.
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78.
Rayleigh’s method of approximation is employed to find out the reflection and transmission coefficients due to an incident
plane SH wave at a corrugated interface between a laterally and vertically inhomogeneous anisotropic elastic solid half-space
and a laterally and vertically inhomogeneous isotropic visco-elastic solid half-space. The lateral and vertical inhomogeneities
are described by the exponential variations of elastic parameters. The formulae of reflection and transmission coefficients
are derived in closed form for the first-order approximation of the corrugation. The effects of the corrugation of the interface,
the inhomogeneity, the anisotropy, the visco-elasticity and the frequency of the incident wave on these coefficients are studied
analytically and numerically for a specific model containing a periodic interface. The results of earlier workers have been
reduced as particular cases from the present formulation. 相似文献
79.
80.
E. L. Afraimovich E. A. Kosogorov N. P. Perevalova A. V. Plotnikov 《Journal of Atmospheric and Solar》2001,63(18)
This paper is concerned with the parameters of shock-acoustic waves (SAW) generated during rocket launchings. We have developed the interferometric method for determining SAW parameters (including angular characteristics of the wave vector, and the SAW phase velocity, as well as the direction towards the source) using GPS-arrays. Contrary to the conventional radio-probing techniques, the proposed method provides an estimate of SAW parameters without a priori information about the site and time of a rocket launching. The application of the method is illustrated by a case study of ionospheric effects from launchings of rockets PROTON, SOYUZ and SPACE SHUTTLE from Baikonur and Kennedy Space Center cosmodromes in 1998–2000. In spite of a difference of rocket characteristics, the ionospheric response for all launchings had the character of an N-wave corresponding to the form of a shock wave. The SAW period T is 270–360 s, and the amplitude exceeds the standard deviation of total electron content background fluctuations in this range of periods under quiet and moderate geomagnetic conditions by factors of 2–5 as a minimum. The angle of elevation of the SAW wave vector varies from 30° to 60°, and the SAW phase velocity (900–1200 m/s) approaches the sound velocity at heights of the ionospheric F-region maximum. The position of the SAW source, inferred by neglecting refraction corrections, corresponds to the segment of the rockets path at a distance no less than 200–900 km from the launch pad, and to the rocket flying altitude no less than 100 km. Our data are consistent with the existing view that SAW are generated during a nearly horizontal flight of the rocket with its engine in operation in the acceleration segment of the path at 100–130 km altitudes in the lower atmosphere. 相似文献