中天山卡瓦布拉克杂岩带中闪长岩的锆石U-Pb年龄及Hf同位素特征

卡瓦布拉克杂岩带出露于中天山地块东段卡瓦布拉克—阿克塔格地区,沿卡瓦布拉克断裂呈东西向展布。笔者选择构成该杂岩带的中—基性岩石主体闪长岩,开展了LA-ICP-MS锆石U-Pb年代学和LA-MC-ICP-MS锆石Hf同位素研究。结果表明:闪长岩中锆石呈自形—半自形,发育典型的岩浆锆石振荡生长环带,Th/U值较高(均大于0.40),且Th、U含量呈现较好的正相关关系,为典型的岩浆成因锆石;这些锆石的206Pb/238 U年龄加权平均值为(375±1)Ma,MSWD=0.081,属晚泥盆世,可代表其结晶年龄;锆石具有较均一的Hf同位素组成,初始比值为0.282 655~0.282 747、εHf(t)值为4.0~7.2,其对应的亏损地幔模式年龄为714~842Ma。结合区域地质资料认为,卡瓦布拉克杂岩带中的闪长岩由亏损岩石圈地幔发生部分熔融而形成。     

末次冰盛期后黄河三角洲沉积物的磁性特征及其沉积环境

On the basis of measuring the magnetic parameters of sediment in Core YDZ1, combined with a grain size analysis and Carbon-14 dating, the magnetic properties of sediment and sedimentary environment in the Huanghe(Yellow River) Delta area after the last glacial maximum have been studied. The results show that the ferrimagnetic minerals of a pseudo single domain and multi domain particles dominate the magnetic properties of sediment in Core YDZ1. The imperfect anti ferrimagnetic minerals have more contribution on sediment in a depth of 24.0–22.1 m, and more stable-single domain and pseudo single domain particles exist. The susceptibility of anhysteretic remanent magnetization and the ratio of the susceptibility of anhysteretic remanent magnetization to saturation isothermal remanent magnetization show a decrease trend below depth of 24 m, a marked increase trend in a depth of 24.0–13.5 m, and a rapid decrease at depth of 13.5 m, then a fluctuation trend upward. The above two magnetic parameters and the ratio of the susceptibility of anhysteretic remanent magnetization to the mass susceptibility can be regarded as the proxy indicators for the content of clay(4 μm)and the fine-grained size(32 μm). The sedimentary environment after the last glacial maximum in the Huanghe Delta area has experienced the fluvial facies, the tidal flat facies, the neritic facies, the pro delta facies, the delta front facies and the floodplain facies. Thickness of the Holocene transgression layer is 10.5 m and the depth of substrate is about 24 m according to the YDZ1 core. The sedimentary dynamic has a variation trend with strongweak-strong, which has been proved by the Flemming triangular schema.     

陕西小秦岭华阳川韧性剪切带的特征 及其区域构造意义

陕西小秦岭华阳川韧性剪切带发育在新太古界太华群之中,野外调研和显微构造观察结果表明,该韧性剪切带是由构造片岩、眼球状片麻岩组成的深层次韧性剪切带,具有逆冲兼左行走滑的斜冲特征。对韧性剪切带构造片岩黑云母进行^40Ar／^39Ar同位素定年,获得坪年龄为419M±0．6Ma,反等时线年龄为417Ma±0．8Ma。认为华阳川韧性剪切带及其相应的小秦岭区域主导构造变形是发生于419Ma左右的秦岭加里东事件的结果。     

热释光断代技术测定断层活动时代可能性的研究

本文根据多年来研究断层活动所积累的热释光年龄资料和断层运动过程中各种温、压条件变化的模拟实验结果,阐述了断层运动所产生的摩擦升温有可能使断层面上乃至断层带内某些矿物原有的热释光“退火”,初步探讨了用热释光测年技术测定断层活动年代的可能性     

江西李公岭花岗闪长岩锆石U-Pb定年及找矿前景

为探究江西李公岭花岗闪长岩的成岩时代和成矿前景,对李公岭地区的花岗闪长岩及其中发育的隐爆角砾岩筒中的花岗闪长(斑)岩角砾岩块分别进行了锆石LA-ICP-MS U-Pb定年。测年结果表明,李公岭花岗闪长岩(150.6±1.1)Ma和隐爆角砾岩筒中的花岗闪长(斑)岩岩块(151.0±1.3)Ma基本为同时形成,时代为晚侏罗世。李公岭花岗闪长岩和李公岭角砾岩筒中的花岗闪长(斑)岩的形成时代与区内发育的阳储岭W-Mo矿的成岩成矿时代基本一致,以及隐爆角砾岩筒和周围的网脉状石英脉的存在,表明李公岭地区当时可能存在一个岩浆热液活动中心,且该热液活动可能与江南古陆东北缘燕山晚期大规模W-Mo成矿作用有关,暗示李公岭岩体周围具有较大的W-Mo找矿前景。     

Thrusting of the North Lhasa Block in the Tibetan Plateau

A huge thrust system, the North Lhasa Thrust (NLT), was discovered in the northern Lhasa block of the Tibetan Plateau based on geological mapping of the Damxung region and its vicinity, the Deqen-Lunpola traverse and the Amdo-Bam Co profile. The NLT consists of the Dongqiao-Lunpola thrust (DLT), the west Namco thrust (WNT) and the south Damxung thrust (SDT) and ductile shear zones, ophiolite slices and folds extending in a WNW direction. Major thrust faults of the NLT seem to merge into a single deep-seated detachment of the upper-crust and totally displaced southward as far as 100-120 km. Chronological analyses with 39Ar-40Ar of plagioclase and hornblende, Rb-Sr isochron of minerals and fission-tracks of apatite from mylonite within the WNT yield ages of 174-173 Ma, 109 Ma and 44 Ma, showing 3 periods of thrusting in the north Lhasa block caused by subduction of the Tethys oceanic plate and the India-Eurasia continental collision respectively.     

北苏鲁超高压变质带中斜长角闪岩的成因

在北苏鲁超高压变质带的威海地区的正片麻岩中,存在大量规模不一的含石榴石斜长角闪岩的透镜体或不规则团块。锆石中矿物包体的激光拉曼测试、阴极发光图像分析、稀土元素和微量元素以及Lu-Hf同位素的LA-(MC)-ICP-MS测试等综合研究结果表明,含石榴石斜长角闪岩 (WH17) 只存在一种成因类型的锆石,即变质锆石。该类锆石自核部到边部均保存了典型的超高压包体矿物组合：柯石英 (Coe)+石榴石 (Grt)+绿辉石 (Omp)+多硅白云母 (Phe)+金红石 (Rt)+磷灰石 (Ap),相应的阴极发光图像自核部到边部十分均匀,具有典型变质锆石的特点。锆石核部和边部的稀土元素含量特征和配分模式也十分相似,主要表现为轻稀土元素相对亏损,而重稀土元素相对平坦,无Eu异常 (Eu/Eu^*=0.94~1.04), 具较明显的正Ce异常 (Ce/Ce^*=83.4~111.0),低的Th/U (<0.02) 和 Lu/Hf (<0.00010) 比值以及极低的 Th (1×10^-6~4×10^-6) 含量。锆石核部到边缘的重稀土元素亏损与石榴石稳定有关,而无Eu异常则与斜长石分解关系密切。上述特征表明,含石榴石斜长角闪岩中的锆石均是在超高压变质阶段形成的变质锆石,而研究样品中继承性岩浆结晶锆石的缺乏,是由于含石榴石斜长角闪岩在原岩形成时Zr的成分明显匮乏所致。SHRIMP U-Pb定年结果表明,含柯石英锆石自核部到边部记录了十分一致的²⁰⁶Pb/²³⁸U 年龄,变化于 240.2±3.3Ma 到220.2±2.8Ma 之间,加权平均年龄为229.8±2.0Ma, 这组年龄与前人对苏鲁超高压变质带中榴辉岩、正片麻岩、副片麻岩和大理岩等含柯石英锆石微区记录的年龄完全吻合,应代表苏鲁地体超高压变质时代。Lu-Hf同位素研究结果表明,含石榴石斜长角闪岩中变质锆石的Hf同位素特征与苏鲁超高压变质带中榴辉岩的继承性岩浆锆石和变质锆石均存在本质差别,其中¹⁷⁶Hf/¹⁷⁷Hf=0.00001~0.00003, ¹⁷⁶Hf/¹⁷⁷Hf (_t)=0.282052~0.282107, 相应的ε_Hf(t)=-21.1~-18.8, 模式年龄t_DM2=2.14~2.24Ga,这些Lu-Hf同位素特征与围岩正片麻岩含柯石英锆石微区的Hf同位素性质十分相似, 充分表明了北苏鲁含石榴石斜长角闪岩在超高压变质阶段形成的变质锆石所必须的Zr和Hf成分不是来自体系本身,而是来源于围岩正片麻岩。     

Strain partitioning and preservation of Ar/Ar ages during Variscan exhumation of a subducted crust (Malpica–Tui complex, NW Spain)

The Malpica–Tui complex (NW Iberian Massif) consists of a Lower Continental Unit of variably deformed and recrystallized granitoids, metasediments and sparse metabasites, overridden by an upper unit with rocks of oceanic affinities. Metamorphic minerals dated by the ⁴⁰Ar/³⁹Ar method record a coherent temporal history of progressive deformation during Variscan metamorphism and exhumation. The earliest stages of deformation (D1) under high-pressure conditions are recorded in phengitic white micas from eclogite-facies rocks at 365–370 Ma. Following this eclogite-facies peak-metamorphism, the continental slab became attached to the overriding plate at deep-crustal levels at ca. 340–350 Ma (D2). Exhumation was accompanied by pervasive deformation (D3) within the continental slab at ca. 330 Ma and major deformation (D4) in the underlying para-autochthon at 315–325 Ma. Final tectonothermal evolution included late folding, localized shearing and granitic intrusions at 280–310 Ma.

Dating of high-pressure rocks by the ⁴⁰Ar/³⁹Ar method yields ages that are synchronous with published Rb–Sr and Sm–Nd ages obtained for both the Malpica–Tui complex and its correlative, the Champtoceaux complex in the French Armorican Massif. The results indicate that phengitic white mica retains its radiogenic argon despite been subjected to relatively high temperatures (500–600 °C) for a period of 20–30 My corresponding to the time-span from the static, eclogite-facies M1 peak-metamorphism through D1-M2 eclogite-facies deformation to amphibolite-facies D2-M3. Our study provides additional evidence that under certain geological conditions (i.e., strain partitioning, fluid deficiency) argon isotope mobility is limited at high temperatures, and that ⁴⁰Ar/³⁹Ar geochronology can be a reliable method for dating high pressure metamorphism.     

LA-ICP-MS石榴子石U-Pb定年方法在异剥钙榴岩和矽卡岩年代学研究中的应用

本文利用Coherent GeoLasHD型193 nm ArF准分子激光剥蚀系统和Agilent 7900型四极杆电感耦合等离子体质谱仪, 建立了LA-ICP-MS石榴子石U-Pb定年方法。利用该方法, 对采自冀北地区晚古生代镁铁质-超镁铁质混杂岩体中的异剥钙榴岩和闽西南马坑式铁矿含矿石榴子石矽卡岩这两种岩石中的石榴子石开展U-Pb定年研究。在冀北地区晚古生代镁铁质-超镁铁质混杂岩体中的异剥钙榴岩中, 获得石榴子石下交点年龄为(387.6±5.4) Ma (D496-1, MSWD=1.1, N=30)和(409.3±7.8) Ma (D493-1, MSWD=2.0, N=60), 在马坑铁矿石榴子石矽卡岩中, 获得石榴子石下交点年龄为(128.6±2.1) Ma (ZK7921-b24, MSWD=2.0, N=60)和(128.7±3.2) Ma (ZK7922-b1, 用锆石91500校正, MSWD=1.8, N=42); 在潘田铁矿的石榴子石矽卡岩中, 获得石榴子石的下交点年龄为(128.7±1.7) Ma (PT-b1, MSWD=1.7, N=30)和(132.1±1.3) Ma (PT-b1样品, 用锆石91500校正, MSWD=1.6, N=30)(除了指明使用锆石标样91500校正石榴子石未知样品外, 其他皆用石榴子石标样Willsboro校正石榴子石未知样品的U/Pb分馏)。以上结果与Sm-Nd等时线年龄及前人报道的锆石U-Pb年龄在误差范围内一致。对马坑式铁矿石榴子石矽卡岩U-Pb定年结果表明, 利用石榴子石标样Willsboro和锆石标样91500作为外标样校正同一样品中石榴子石U/Pb同位素分馏, 获得的下交点年龄一致, 206Pb/238U年龄的加权平均值也一致, 说明石榴子石与锆石之间的基体效应较小, 在缺乏石榴子石标样时, 可用锆石标样91500代替。在上述研究基础上分析了石榴子石U-Pb定年方法在矽卡岩型矿床成矿时代研究及异剥钙榴岩年代学研究中的应用潜力, 认为石榴子石U-Pb定年方法在矽卡岩型矿床及异剥钙榴岩年代学研究中具有巨大的应用推广前景, 具有重要的理论指导和实际应用意义。     

中国东北完达山地区早白垩世同构造岩浆侵位——对晚中生代左行走滑作用的响应

分布于中国东北完达山地区的饶河花岗岩岩体中暗色矿物和斑晶钾长石定向排列,呈北北东走向,其中透镜状闪长质捕掳体近水平排列,局部具有左行剪切的特点。岩体中发育石香肠状石英脉,表明岩体在侵位过程中受到左行剪切作用的影响或制约。对出露的花岗岩进行LA-ICP-MS锆石U-Pb定年,获得年龄121±1Ma和119±1Ma,表明该岩浆流动形成于早白垩世。同时对围岩辉长岩、侵入岩体中的正长岩脉和辉绿岩脉进行锆石U-Pb年龄分析,分别获得160±1Ma、109±2Ma、124±1Ma的年龄结果。根据各样品中继承锆石的特征,围岩辉长岩的年龄数据很集中,不存在古老锆石的年龄信息。岩浆流动岩体及岩脉中都有太古宙、元古宙等各时代的锆石年龄数据,可能表明完达山地区在约120Ma之前已完成古太平洋板块的俯冲拼贴,饶河岩体形成于走滑环境下的陆内变形,为同构造侵入岩。