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91.
High-pressure and high-temperature experiments using a laser-heated diamond anvil cell (LHDAC) and synchrotron X-ray diffraction have revealed a phase transition in MgAl2O4. CaTi2O4-type MgAl2O4 was found to be stable at pressures between 45 and at least 117 GPa. The transition pressure of CaTi2O4-type phase in MgAl2O4 is much lower than that in the natural N-type mid-oceanic ridge basalt composition. The Birch–Murnaghan equation of state for CaTi2O4-type MgAl2O4 was determined from the experimental unit cell parameters with K
0=219(±6) GPa, K
0′=4(constrained value), and V
0=238.9(±9) Å3. The observed compressibility was in agreement with the theoretical compressibility calculated in a previous study. ε-MgAl2O4 was observed at pressures between 40 and 45 GPa, which has not been reported in natural rock compositions. The gradient (dP/dT slope) of the transition from the ε-type to CaTi2O4-type MgAl2O4 had a positive value. These results should resolve the dispute regarding the stable high-pressure phase of MgAl2O4, which has been reported in earlier studies using both the multi-anvil press and the diamond anvil cell. 相似文献
92.
N. V. Chalapathi Rao Rajesh K. Srivastava 《Contributions to Mineralogy and Petrology》2009,157(2):245-265
The petrology and geochemistry of some new occurrences of Mesoproterozoic diamondiferous hypabyssal-facies kimberlites from
the Chigicherla, Wajrakarur-Lattavaram and Kalyandurg clusters of the Wajrakarur kimberlite field (WKF), Eastern Dharwar craton
(EDC), southern India, are reported. The kimberlites contain two generations of olivine, and multiple groundmass phases including
phlogopite, spinel, calcite, dolomite, apatite, perovskite, apatite and rare titanite, and xenocrysts of eclogitic garnet
and picro-ilmenite. Since many of the silicate minerals in these kimberlites have been subjected to carbonisation and alteration,
the compositions of the groundmass oxide minerals play a crucial role in their characterisation and in understanding melt
compositions. While there is no evidence for significant crustal contamination in these kimberlites, some limited effects
of ilmenite entrainment are evident in samples from the Kalyandurg cluster. Geochemical studies reveal that the WKF kimberlites
are less differentiated and more primitive than those from the Narayanpet kimberlite field (NKF), Eastern Dharwar craton.
Highly fractionated (La/Yb = 108–145) chondrite-normalised distribution patterns with La abundances of 500–1,000 × chondrite
and low heavy rare earth elements (HREE) abundances of 5–10 × chondrite are characteristic of these rocks. Metasomatism by
percolating melts from the convecting mantle, rather than by subduction-related processes, is inferred to have occurred in
their source regions based on incompatible element signatures. While the majority of the Eastern Dharwar craton kimberlites
are similar to the Group I kimberlites of southern Africa in terms of petrology, geochemistry and Sr–Nd isotope systematics,
others show the geochemical traits of Group II kimberlites or an overlap between Group I and II kimberlites. Rare earth element
(REE)-based semi-quantitative forward modelling of batch melting of southern African Group I and II kimberlite source compositions
involving a metasomatised garnet lherzolite and very low degrees of partial melting demonstrate that (1) WKF and NKF kimberlites
display a relatively far greater range in the degree of melting than those from the on-craton occurrences from southern Africa
and are similar to that of world-wide melilitites, (2) different degrees of partial melting of a common source cannot account
for the genesis of all the EDC kimberlites, (3) multiple and highly heterogeneous kimberlite sources involve in the sub-continental
lithospheric mantle (SCLM) in the Eastern Dharwar craton and (4) WKF and NKF kimberlites generation is a resultant of complex
interplay between the heterogeneous sources and their different degrees of partial melting. These observations are consistent
with the recent results obtained from inversion modelling of REE concentrations from EDC kimberlites in that both the forward
as wells as inverse melting models necessitate a dominantly lithospheric, and not asthenospheric, mantle source regions. The
invading metasomatic (enriching) melts percolating from the convecting (asthenosphere) mantle impart an OIB-like isotopic
signature to the final melt products. 相似文献
93.
Andrea De Stefano M. G. Kopylova P. Cartigny V. Afanasiev 《Contributions to Mineralogy and Petrology》2009,158(3):295-315
We studied diamonds and barren and diamondiferous eclogite xenoliths from the Jericho kimberlite (Northern Slave craton).
The majority of the diamonds are non-resorbed octahedral crystals, with moderately aggregated N (IaB < 50%, N < 300 ppm) and δ13C = −5 to −41‰. The diamonds belong to “eclogitic” (90% of the studied samples), “websteritic” (7%) and “peridotitic” (3%)
assemblages. The Jericho diamonds differ from the majority of “eclogitic” diamonds worldwide in magnesian compositions of
associated minerals and extremely light C isotopic compositions (δ13C = −24 to −41‰). We propose that metasomatism triggered by H2O fluids may have been involved in the diamond formation. Multiple episodes of the metasomatism and associated melt extraction
of various ages are evident in Jericho eclogite xenoliths where primary garnet and clinopyroxene have been recrystallized
to more magnesian minerals with higher contents of some incompatible trace elements and to hydrous secondary phases. The model
is supported by the general similarity of mineral compositions in diamondiferous eclogites to those in diamond inclusions
and to secondary magnesian garnet and clinopyroxene in recrystallized barren eclogites. The ultimate products of the metasomatism
could be “websteritic” diamond assemblages sourced from magnesian eclogites.
Electronic supplementary material The online version of this article (doi:) contains supplementary material, which is available to authorized users. 相似文献
94.
《International Geology Review》2012,54(4):504-519
ABSTRACTThe preservation of metastable diamond in ultrahigh-pressure metamorphic (UHPM) complexes challenges our understanding of the processes taking place during exhumation of these subduction zone complexes. The presence of diamonds in UHPM rocks implies that diamonds remained metastable during exhumation, and within thermodynamic stability of graphite for an extended period. This work studies the influence of pressure on the surface graphitization rate of diamond monocrystals in carbonate systems to understand the preservation of microdiamond during exhumation of UHP subduction complexes. Experiments were performed with 2–3 mm synthetic diamond monocrystals at 2–4 GPa in СаСО3 (1550°С) and К2СО3 (1450°С) melts using a high-pressure multi-anvil apparatus. The highest rate of surface graphitization took place at 2 GPa; diamond crystals were almost completely enveloped by a graphite coating. At 4 GPa, only octahedron-shaped pits formed on flat {111} diamond crystal faces. Our results demonstrate that the surface graphitization rate of diamonds in the presence of carbonate melts at 1450–1550°C increases with decreasing pressure. Decreased pressure alone can graphitize diamond regardless of exhumation rate. Metastable diamond inclusions survive exhumation with little or no graphitization because of excess pressure up to 2 GPa acting on them, and because inclusions are protected from interaction with C-O-H fluid. 相似文献
95.
Yusuke Seto Daisuke Hamane Takaya Nagai Kiyoshi Fujino 《Physics and Chemistry of Minerals》2008,35(4):223-229
We report on high-pressure and high-temperature experiments involving carbonates and silicates at 30–80 GPa and 1,600–3,200 K,
corresponding to depths within the Earth of approximately 800–2,200 km. The experiments are intended to represent the decomposition
process of carbonates contained within oceanic plates subducted into the lower mantle. In basaltic composition, CaCO3 (calcite and aragonite), the major carbonate phase in marine sediments, is altered into MgCO3 (magnesite) via reactions with Mg-bearing silicates under conditions that are 200–300°C colder than the mantle geotherm.
With increasing temperature and pressure, the magnesite decomposes into an assemblage of CO2 + perovskite via reactions with SiO2. Magnesite is not the only host phase for subducted carbon—solid CO2 also carries carbon in the lower mantle. Furthermore, CO2 itself breaks down to diamond and oxygen under geotherm conditions over 70 GPa, which might imply a possible mechanism for
diamond formation in the lower mantle. 相似文献
96.
《地学前缘(英文版)》2022,13(6):101455
Although the diamond potential of cratons is linked mainly to thick and depleted Archean lithospheric keels, there are examples of craton-edge locations and circum-cratonic Proterozoic terranes underlain by diamondiferous mantle. Here, we use the results of comprehensive major and trace-element studies of detrital garnets from diamond-rich Late Triassic (Carnian) sedimentary rocks in the northeastern Siberia to constrain the thermal and chemical state of the pre-Triassic mantle and its ability to sustain the diamond storage. The studied detrital mantle-derived garnets are dominated by low- to medium-Cr lherzolitic (~45%) and low-Cr megacrystic (~39%) chemistries, with a significant proportion of eclogitic garnets (~11%), and only subordinate contribution from harzburgitic garnets (~5%) with variable Cr2O3 contents (1.2–8.4 wt.%). Low-Cr megacrysts display uniform, “normal” rare-earth element (REE) patterns with no Eu/Eu* anomalies, systematic Zr and Ti enrichment (mainly within 2.5–5), which are evidence of their crystallization from deep metasomatic melts. Lherzolitic (G9) garnets exhibit normal or humped to MREE-depleted sinusoidal REE patterns and elevated Nd/Y (up to 0.33–0.41) and Zr/Y ratios (up to 7.62). Rare low- to high-Cr harzburgitic (G10) garnets have primarily “depleted”, sinusoidal REE-patterns, low Ti, Y and HREE, but vary significantly in Zr-Hf, Ti and MREE-HREE contents, Nd/Y (within 0.1–2.4) and Zr/Y (1.53–19.9) ratios. The observed trends of chemical enrichment from the most depleted, harzburgitic garnets towards lherzolitic (including high-Ti high-Cr G11-type) garnets and megacrysts result from either voluminous high-temperature metasomatism by plume-derived silicate melts or recurrent mobilization of less voluminous kimberlitic or related carbonated mantle melts, rather than the initially primitive, fertile nature of the Proterozoic SCLM. Calculated Ni-in-garnet temperatures (primarily within ~1150–1250 °C) indicate their derivation from at least ~220 km thick Cr-undersaturated lithosphere at the relevant Devonian to Triassic thermal flow of ~45 mW/m2 or cooler. We suggest the existence of rare harzburgitic domains in the primarily lherzolitic diamond-facies SCLM beneath the northeastern Siberian craton at least by Triassic, whereas the abundance of eclogitic garnets, predominance of E-type inclusions in placer diamonds and specific morphologies argue for diamondiferous eclogites occurring within a ~50–65 kbar diamond window of the Olenek province by the same time. 相似文献
97.
Lutz Nasdala Ronald Miletich Katja Ruschel Tamás Váczi 《Physics and Chemistry of Minerals》2008,35(10):597-602
Pressure-induced changes of Raman band parameters of four natural, gem-quality zircon samples with different degrees of self-irradiation
damage, and synthetic ZrSiO4 without radiation damage, have been studied under hydrostatic compression in a diamond anvil cell up to ~10 GPa. Radiation-damaged
zircon shows similar up-shifts of internal SiO4 stretching modes at elevated pressures as non-damaged ZrSiO4. Only minor changes of band-widths were observed in all cases. This makes it possible to estimate the degree of radiation
damage from the width of the ν3(SiO4) band of zircon inclusions in situ, almost independent from potential “fossilized pressures” or compressive strain acting
on the inclusions. An application is the non-destructive analysis of gemstones such as corundum or spinel: broadened Raman
bands are a reliable indicator of self-irradiation damage in zircon inclusions, whose presence allows one to exclude artificial
color enhancement by high-temperature treatment of the specimen. 相似文献
98.
99.
Based on the earthquake activity characteristics of the diamond block in the Sichuan-Yunnan region and by using the method of the meso-scope damage dynamics and damage evolution,we studied the damage evolution process for moderately strong earthquakes along two seismicbelts.The original combination patterns of all the units which illuminate the changes from stable state to destroyed state are given.All these patterns can direct the earthquake prediction practice in this region 相似文献
100.