Slepian函数在月球局部重力场分析中的适用性分析

在分析Slepian函数数学性质的基础上,选取月球北极球冠区域为研究范围,结合CEGM02模型,研究Slepian函数在解算月球局部重力场和局部功率谱优缺点和适用范围。同时利用CEGM02、SGM150j、LP150Q、GRAIL660模型,分析不同模型的月球局部重力场-地形导纳及相关性。结果表明Slepian函数的局部正交特性在表达月球局部重力场方面有明显优势;由Slepian模型计算得到的局部重力场功率谱可信可靠带宽较大,但球冠边缘异常信号对谱分析结果高频部分带来较大不确定性;利用Slepian加窗的局部谱分析方法可以分析局部区域能量与全球的关系,但其谱分析结果可信可靠频段较窄,低阶段误差较大。4个重力场模型局部重力-地形导纳中低阶部分接近,高阶部分随阶次增大差距明显,可靠性降低。     

武汉地区建筑废弃泥浆泥水分离试验研究

针对武汉地区不同地层、不同工艺产生的建筑工程废弃泥浆,通过光谱仪分析了其主要化学成分,并通过过滤、真空抽滤、离心以及不同絮凝剂的正交试验,以上清液浊度和清液率为主要指标对废弃泥浆泥水分离效果进行评价。试验发现：废弃泥浆固相颗粒以有机质为主;采用过滤方式取得的清液浊度较低,但清液率较少;采用真空抽滤方式处理废弃泥浆可以获得较多的上清液;采用离心方式能处理除含特细颗粒外的多数废弃泥浆;正交试验表明阳离子絮凝剂（PAM）处理废弃泥浆效果较好。     

转炉高温熔渣显微结构研究

传统的炉渣岩相分析方法是在显微镜下观察其冷凝渣的岩相结构,并以此来推测该炉渣在高温下的行为。但炉渣在由熔融态逐渐冷却的过程中,会发生物理、化学变化,故用冷凝渣结构来反映炉渣高温状态是有缺陷的。为此,试用热台高温显微镜进行了炉渣高温显微结构研究,并与冷凝渣进行了对比。１　研究方法１－１　试验设备采用英国１２Ｄ型热台高温显微镜,进行了高温熔渣研究。该高温显微镜是以热电偶、发热体和样品支架为一体的微型高温炉为主体,ＰｔＲｈ热丝炉可迅速将约０－１ｍｇ试样加热到１６５０℃以上,并可利用放大５０倍的显微镜…     

河北山前平原地下水^32Si年龄初探

＾３２Ｓｉ是放射性同位素,半衰期约１４０ａ可以测定５０～１０００ａ地下水的年龄,本文用Ｆｅ（ＯＨ）３共沉淀法从天然水中提取ＳｉＯ２回收率可达３０％～９８％,然后提取和纯化＾３２Ｐ,将Ｈ３ＰＯ４溶液和Ｐｉｃｏ－ｆｌｏｕｒ＾ＴＭＬＬＴ混合制备计数溶液,用液体闪烁计数法测量中＾３２Ｐ的放射性,本底计数为４．８０ｃｐｈ,仪器效率为４５．３４％,然后用公式计算样品的＾３２Ｓｉ放射性浓度和地下水的＾３２Ｓｉ年     

浙江十种经济海藻的氨基酸含量分析

采用以异硫氰酸苯脂（ＰＩＴＣ）为柱前衍生化的ＰＩＣＯ－ＴＡＧ反相高效液相色谱法对浙江沿岸１０种经济海藻的氨基酸含量进行测定,得出以上海藻的氨基酸色谱图。发现１０种海藻的氨基酸组成基本相同。氨基酸总含量达１０．５７％～３３．５１％,其中必需氨基酸占总量的２８．２８％～４５．２２％。该测定结果可以为海藻经济开发提供参考。     

山地温性积雪内液体水含量的测定方法

通过在北欧ＡｕｓｔｒｅＯｋｓｔｉｎｄｂｒｅｅｎ冰川积雪内的实际测定结果,证明野外测量积雪内液体水含量的新方法－酒精量热法是可行和适用的,解决了过去测定积雪内液体水含量时遇到困难。５个雪坑剖面的测定结果清楚地显示雪内液体水含量的区带性和随高度的变化,积雪内液体水含量的垂直变化与雪层中物理结构,温度和密度的分布有关。     

窗函数对地基阻尼比测试的影响

根据某块体基础的实测数据,讨论了常见平滑方法对时域对数衰减法和频域点峰法竖向阻尼比测试的影响。结果表明,无论采用时域方法还是频域方法,分别对测试曲线进行相邻三点的滑动平均、汉宁窗、哈明窗平滑,阻尼比计算数值差别很小。平滑次数对时域阻尼比结果有影响,平滑次数越多,时域阻尼比有减少的趋势,而频域阻尼比有增大的趋势。滑动平均方法和平滑次数的合理选取,应通过理论和试验方法的研究进一步确定。     

山东地区尾波衰减特性（Qc）研究

基于单次散射模型,利用山东数字地震台网数字地震波形资料,计算了山东地区13个频段的Qc值。结果表明,在1．0—20Hz（短周期）或0．05—20HIz（宽频带）频率范围内,Qc随频率的变化近似服从幂函数关系Qc^mQ0f^q,拟合得到山东地区尾波Qc值随频率的变化关系为Qc（f）=118．7±26．8f^0.94±0.14,并且选取的流逝时间越长,即时间窗越靠后,Q值一般也越大。     

Chemical constituents and antioxidant activities of waste liquid extract from Apostichopus japonicus Selenka processing

Apos tichopus japonicus Selenka is an ideal tonic food that is used traditionally in many Asian countries, and it contains many bioactive substances, such as antioxidant, antimicrobial, and anticancer materials. To convert waste liquid generated during production into a useful resource, extract from waste liquid was isolated by column chromatography and studied by the pyrogallol autoxidation and 1,10-phenanthroline-Fe²⁺ oxidation methods. Results show that the extract scavenged about 91% of the superoxide anion radical at a concentration of 1.4 mg/mL and 24% of the hydroxyl radical at 3.3 mg/mL. Four compounds were isolated and identified from the extract: 2,4-dihydroxy-5-methyl-1,3-azine; 2,4-dihydroxy-1,3-diazine; 3-O-[β-D-quinovopranosyl-(1→2)-4-O-sodium sulfate-β-D-xylopranosyl]-holosta-9(11)-ene-3β,12α,17α-triol; and 24-ethyl-5α-cholesta-7-ene-3β-O-β-D-xylopyranoside. All of these compounds are known in A. japonicus, and were found in the waste liquid for the first time.     

Stability and changes in astaxanthin ester composition from Haematococcus pluvialis during storage

In this paper, we investigated the effects of temperature, oxygen, antioxidants, and corn germ oil on the stability of astaxanthin from Haematococcus pluvialis under different storage conditions, and changes in the composition of astaxanthin esters during storage using high performance liquid chromatography and spectrophotometry. Oxygen and high temperatures （22-25~C） significantly reduced the stability of astaxanthin esters. Corn germ oil and antioxidants （ascorbic acid and vitamin E） failed to protect astaxanthin from oxidation, and actually significantly increased the instability of astaxanthin. A change in the relative composition of astaxanthin esters was observed after 96 weeks of long-term storage. During storage, the relative amounts of free astaxanthin and astaxanthin monoesters declined, while the relative amount of astaxanthin diesters increased. Thus, the ratio of astaxanthin diester to monoester increased, and this ratio could be used to indicate if astaxanthin esters have been properly preserved. If the ratio is greater than 0.2, it suggests that the decrease in astaxanthin content could be higher than 20%. Our results show that storing algal powder from H. pluvialis or other natural astaxanthin products under vacuum and in the dark below 4~C is the most economical and applicable storage method for the large-scale production of astaxanthin from H. pluvialis. This storage method can produce an astaxanthin preservation rate of at least 80% after 96 weeks of storage.