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11.
12.
193nmLA-ICPMS对国际地质标准参考物质中42种主量和微量元素的分析 总被引:47,自引:16,他引:31
本文采用配备有 193nm Ar F准分子 (excimer)激光器的 Geo L as2 0 0 M剥蚀系统和 Elan6 10 0 DRC ICP- MS对 4个美国地质调查所 (USGS)玻璃标准参考物质以及 3个美国国家标准技术研究院 (NIST)人工合成硅酸盐玻璃标准参考物质中几乎覆盖整个质量数范围 (从 7L i到 2 38U)的 38个微量和 4个主量 (Na、Mg、Ti和 Mn)元素进行了分析。分析结果表明 ,无论是对 USGS还是 NIST玻璃 ,元素分析的相对标准偏差 RSDs和分析值与参考值之间的相对偏差 (RDs)一般优于 10 % ,RSD和RD较大的元素主要出现在含量很低或不均匀样品中。稀土元素的 RSD显示 ,除 AGV- 2 G可能存在不均匀现象外 ,其它所测样品在 6 0 μm尺度上 ,元素分布是均匀的。本研究证明 ,由于 ICP- MS具有 10 8cps(每秒计数 )的动态线性范围 ,本实验室的L A- ICPMS系统可定量分析含量在百分之几的主量元素及微量元素。分析精密度和准确度可与常规溶液雾化进样 ICP- MS方法相媲美 相似文献
13.
Maik Pertermann Alan G. Whittington Anne M. Hofmeister Frank J. Spera John Zayak 《Contributions to Mineralogy and Petrology》2008,155(6):689-702
Thermal diffusivity (D) was measured using laser-flash analysis from oriented single-crystal low-sanidine (K0.92Na0.08Al0.99Fe3+
0.005Si2.95O8), and three glasses near KAlSi3O8. Viscosity measurements of the three supercooled liquids, in the range 106.8 to 1012.3 Pa s, confirm near-Arrhenian behavior, varying subtly with composition. For crystal and glass, D decreases with T, approaching a constant near 1,000 K: D
sat ∼ 0.65 ± 0.3 mm2 s−1 for bulk crystal and ∼0.53 ± 0.03 mm2 s−1 for the glass. A rapid decrease near 1,400 K is consistent with crossing the glass transition. Melt behavior is approximated
by D = 0.475 ± 0.01 mm2 s−1. Thermal conductivity (k
lat) of glass, calculated using previous heat capacity (C
P) and new density data, increases with T because C
P strongly increases with T. For melt, k
lat reaches a plateau near 1.45 W m−1 K−1, and is always below k
lat of the crystal. Melting of potassium feldspars impedes heat transport, providing positive thermal feedback that may promote
further melting in continental crust. 相似文献
14.
玻璃幕墙防护侧击雷的施工方法 总被引:1,自引:1,他引:0
主要讲述了玻璃幕墙侧击雷防护施工方法、防雷措施及玻璃幕墙防雷接地的几种形式,是在玻璃幕墙防雷施工过程中的一些认识,供参考。 相似文献
15.
The natural environment of an environmental conflict site in Incheon, Korea was assessed with a focus on the hydrogeological
environment. Residents had made claims against a company because of health problems, including skin tumors. More specifically,
the residents suspected that their drinking groundwater had been contaminated by glass fibers which had caused the health
problems. Air, soil, and groundwater samples were analyzed to estimate whether environmental pollution could have caused the
problems claimed by the residents. No specific evidence was found from this study to support the groundwater contamination
by glass fibers, but groundwater contamination by leaked fuel oils was confirmed in the course of evaluating the glass fiber
problem.
Received: 16 May 1997 · Accepted: 18 August 1997 相似文献
16.
近年来,玻璃钢夹砂管在(管工程中的到越来越广泛的应用,以广州市某污水工程顶管施工为例,介绍了玻璃钢夹砂管在流砂地层的应用,以及在顶管施工中所要注意的事项和应对措施,以供工程技术人员和同类工程参考。 相似文献
17.
Sarah E. Mouring 《Ocean Engineering》1999,26(8):793
The U.S. shipbuilding industry recently has started incorporating composite materials in the construction of both military and commercial ships due to the advantages of composite construction. These advantages include the reduction in total life costs, corrosion resistance, high strength- and stiffness-to-weight ratios, and improved stealth for military applications. One disadvantage is the higher costs of composites compared to steel and other conventional materials. Therefore, new higher quality materials with lower costs and new fabrication methods need to be developed before composite materials will be fully accepted for the construction of large ships. A new composite preform framing technology shows promise in the reduction of fabrication costs for large ship construction. There already has been significant cost savings using this framing technology in the construction of small recreational boats and large yachts. This framing technology involves casting a dry glass fiber-reinforced plastic (GRP) fabric into shape in a closed mold with a foam core. One unresolved issue using this framing technology is the orientation of the fiber for the frames. This paper summarizes experimental results of the testing of composite panels stiffened with preform frames under in-plane uniaxial compressive loads. Biaxial (0,90), quadaxial (0,90,+45,−45), and triaxial (+45,−45,0) laminates were used in the frames. 相似文献
18.
19.
Discontinuous tephra layers were discovered at Burney Spring Mountain, northern California. Stratigraphic relationships suggest that they are two distinct tephras. Binary plots and standard similarity coefficients of electron probe microanalysis data have been supplemented with principal component analysis to correlate the two tephra layers to known regional tephras. Using principal component analysis, we are furthermore able to bound our uncertainty in the correlation of the two tephra layers. After removal of outliers, within the 95% prediction interval, we can say that one tephra layer is likely the Rockland tephra, aged 565–610 ka, and the second layer is likely from Mt. Mazama, the Trego Hot Springs tephra, aged ~ 29 ka. In the case of the Rockland tephra, the new findings suggest that dispersal to the north was highly restricted. For Trego Hot Springs ash, the new findings extend the distribution to the southwest, with a rapid thinning in that direction. Coupled with considerations of regular tephra dispersal patterns, the results suggest that the primary dispersal direction for both tephras was to the south, and that occurrences in other directions are unlikely or otherwise anomalous. 相似文献
20.
Pyroclastic materials dispersed in recent volcanic eruptions in Northern Patagonia were analysed in order to characterize the volcanic provenance by the geochemical fingerprint. The volcanic products studied were dispersed by eruptions of volcanoes Calbuco in 1961, Chaitén in 2008, and Cordón Caulle Volcanic Complex (CCVC) in 1960 and 2011. The geochemical characterization was based on the determination of 35 major and trace elements by Instrumental Neutron Activation Analysis, including geochemical tracer such as Rare Earth Elements (REE). The study of the pyroclastic products also included the morphological analysis by petrographic and scanning electron microscopy, and the mineralogical characterization by X-ray diffraction.Geochemical tracers determined in the glass fraction of the dispersed pyroclastic materials allowed a clear discrimination of the three volcanoes that gave origin to the tephras, the three of them with different evolution degree. Tephras from 1960 and 2011 CCVC eruptions showed the same geochemical signature. The geochemical parameters providing the differential characterization are the normalized REE and multi-element patterns, the Eu anomaly, the heavy to light and medium to light REE normalized ratios, and the Cs, Sc, Rb, Ta and Th concentrations. The bulk glassy fraction showed the same composition for each volcanic eruption in samples collected even in distant sites (from 100 to 220 km in Chaitén, 2008, and from 80 to 650 km in CCVC 2011), attesting to be the most reliable material for correlation purposes.According to the mineralogy, cristobalite was found in volcano Chaitén tephra as an indicator of such origin. Arsenic, an element of environmental interest, exhibited concentrations ranging from 6 to 16 μg g−1, with the highest values corresponding to Puyehue–Cordón Caulle and Chaitén products. 相似文献