氰化液中Ag的现场测定

已往测定氰化液中Ag的方法只适用于化学成分简单的样品，对于成分较复杂，尤其是Cu，Pb，Zn浓度较高的氰化液，其测定Ag的重现性较差。现场测定氰化液中Ag的方法是基于采用HNO3 H2O2(过氧化氢)破坏氰化液中的[CN]-，在10％HNO3介质中以CCX富集分离Ag。吸附在CCX上的Ag经灰化法解脱后在pH值为3．3的CH3COOH(乙酸)-CH3COONa(乙酸钠)缓冲溶液中，以Au试剂液珠萃取比色法进行测定。选择一个已知含量的氰化液进行10次测定，方法的测定下限为0．1μg／mL，RSD为5．8％，分析结果能满足选冶生产工艺的需要。     

Experimental research on reservoir sensitivity to stress and impacts on productivity in Kela 2 Gas Field

Kela 2 Gas Field, with high formation pressure (74.35MPa), high pressure coefficient (2.022) and difficulty of potential test and evaluation, is the largest integrated proved dry gas reservoir in China so far and the principal source for West-East Gas Development Project. In order to correctly evaluate the elastic-plastic deformation of rocks caused by the pressure decline during production, some researches, as the experiment on reservoir sensitivity to stress of gas filed with abnormal high pressure, are made. By testing the rock mechanic properties, porosities and permeabilities at different temperature and pressure of 342 core samples from 5 wells in this area, the variations of petro-physical properties at changing pressure are analyzed, and the applicable inspection relationship is concluded. The average productivity curve with the reservoir sensitivity to stress is plotted on the basis of the research, integrated with the field-wide productivity equation. The knowledge lays a foundation for the gas well productivity evaluation in the field and the gas field development plan, and provides effective techniques and measures for basic research on the development of similar gas fields.     

Measurement of the spatial distribution of fluvial bedload transport velocity in both sand and gravel

Maps are presented of the spatial distribution of two‐dimensional bedload transport velocity vectors. Bedload velocity data were collected using the bottom tracking feature of an acoustic Doppler current pro?ler (aDcp) in both a gravel‐bed reach and a sand‐bed reach of Fraser River, British Columbia. Block‐averaged bedload velocity vectors, and bedload velocity vectors interpolated onto a uniform grid, revealed coherent patterns in the bedload velocity distribution. Concurrent Helley‐Smith bedload sampling in the sand‐bed reach corroborated the trends observed in the bedload velocity map. Contemporaneous 2D vector maps of near‐bed water velocity (velocity in bins centered between 25 cm and 50 cm from the bottom) and depth‐averaged water velocity were also generated from the aDcp data. Using a vector correlation coef?cient, which is independent of the choice of coordinate system, the bedload velocity distribution was signi?cantly correlated to the near‐bed and depth‐averaged water velocity distributions. The bedload velocity distribution also compared favorably with variations in depth and estimates of the spatial distribution of shear stress. Published in 2004 by John Wiley & Sons, Ltd.     

A comparative study on the illite crystallinity and the clay mineral reflectance spectral index for subdividing the very low-grade metamorphic belt along the Lizhou-Hekou geological section in the Youjiang sedimentary basin, Guangxi, China

To examine the application potential of hyperspectral remote sensing techniques in classifying very low-grade metamorphic belts, the composition of clay minerals and the cyrstallinity of illite from mudstones were measured using XRD and VIS-SWIR (400-2500 nm) reflectance spectroscopy. Based on the illite cyrstallinity, Kubler Index (KI), the Early Triassic LuoLou Group and the Middle Triassic lower Baifeng Formation were classified as the lower Epizone with KI△2θ° ranging from 0.22 to 0.25, the upper Baifeng Formation as upper anchizone with KI△2θ°ranging from 0.26 to 0.33, and the Hekou Formation as lower anchizone with KI△2θ° ranging from 0.38 to 0.40. According to a KI△2θ° value of 0.43, it is possible that there may exist a local diagenetic zone in the upper strata. The illite cyrstallinity Kubler index and the metamorphic grade increase from the bottom to the top of the stratigraphic sequence. The metamorphic grade boundaries nearly match the stratigraphic boundaries, indicating a burial metamorphism nature for the stratigraphic sequence. From the bottom to the top of the sequence, the spectral absorption band center of clay minerals from fresh rocks is around 2200 nm. The absorption band centers change towards shorter wavelengths: the Luolou Group being at 2220 nm, the Baifeng Formation at 2217-2213 nm, the lower member of the Hekou Formation at 2214-2206 nm, and the upper member of the Hekou Formation at 2205-2197 nm. The spectral absorption band center of illite shows the same change pattern. These results indicate that very low-grade metamorphic belts can be subdivided using spectral indices of clay minerals, which are measured by using field portable spectroradiometers. However, it may not work well with satellite and airborne sensors.     

TRMM卫星微波成像仪分级产品及其反演降水算法

文章叙述了获取定量降水信息的意义，简要介绍了对热带测雨卫星TRMM(Tropical Rainfall Measurement Mission)的仪器、美国国家宇航局提供的微波成像仪TMI(TRMM Microwave Imager)分级产品。对比了物理方法和经验方法反演降水的特点，并对一些经验方法以及倾斜对流系统对反演降水的影响、动态聚类分析、神经网络反演方法的研究成果进行了介绍。     

安塞油田杏河地区长6油层沉积微相研究

在岩心描述的基础上，对杏河地区长6油层沉积相进行了分析，提出了该区主要沉积相为湖泊环境的河控三角洲体系，主要为三角洲前缘亚相沉积，主要沉积微相有水下分流河道、分流河口砂坝、前缘砂席和分流间等，分流河道和河口砂坝是本区占主导地位的骨架砂体。该区长6油层的三角洲体系是安塞三角洲体系最早发育的一支，早期分流来自于北部，后期分流转由东北方向进入，由于各期分流河道迁移、袭夺、决口以及因压实的均衡调整等，从而形成三角洲复合体内部各分流三角洲砂体的相互叠置交错。根据岩心微相分析、小层砂体形态和测井剖面对比分析，对该区长6油层砂组及小层的沉积微相进行了研究，掌握了沉积微相的时空展布和变化规律。     

测试超细煤粉粒度的实验研究

利用激光粒度仪测试超细煤粉的粒度。对测试超细煤粉试样粒度时的试样浓度、测试温度、分散时间、分散剂的种类及浓度等方面的影响进行了实验研究，给出了激光粒度仪测试超细煤粉粒度的最佳实验条件。     

裂变径迹长度测量标准化研究——锆石蚀刻标准探讨

通过不同时间蚀刻的锆石径迹长度测量,确定海南迅速冷却火山型锆石的水平封闭径迹(HCT)平均长度L＝10.93 μm,标准偏差为0.93 μm,可作为锆石长度测量的参照标准.对锆石的蚀刻标准进行了探讨,确立垂直C轴的表面径迹宽度Dpar为(1.0±0.5)μm的蚀刻标准,要求Dpar>1 μm和Dpar<1 μm的颗粒数应大致相当,以及封闭径迹宽度DHCT<1.0 μm的测量标准.     

利用VB编程完成基点网联测中的各项计算

整套重力计算程序包括了除“地改”以外的所有项目的计算，在这篇文章中我们先仅介绍了“测区参数初始化”及“基点网联测”(采用三程小循环方式)的计算方法。“测区参数初始化”功能可生成gdw．csh初始化文件(该套程序的各项功能都要读取该文件中的相关参量)；“基点网联测”功能可计算基点网联测的各项精度，对联测进行平差，求出各分基点绝对重力值。     

渤南油田中部古近系沙河街组低渗透储层岩石学和成岩作用

该区储层岩石类型主要为岩屑质长石砂岩，溶解作用是主要的建设性成岩作用，压实、自生矿物充填和胶结作用是主要的破坏性成岩作用，成岩阶段处于晚成岩A亚期。该区储层较高的孔隙度是晚成岩期强烈的溶解作用形成次生溶孔的结果，而储层砂岩较低渗透率的主要成因机理是成岩期各种自生矿物的充填和胶结作用；此外，溶蚀作用形成的孤立、互不连通的粒间孔也是形成低渗微细喉道储层的主要原因。有利孔隙组合为粒间溶蚀孔-原生粒间孔-粒内破碎缝，有利储层的分布受砂体分布、构造配置及成岩作用的联合控制。