From geometry to dynamics of microstructure: using boundary lengths to quantify boundary misorientations and anisotropy

The microstructure of a quartzite experimentally deformed and partially recrystallised at 900 °C, 1.2 GPa confining pressure and strain rate 10⁻⁶/s was investigated using orientation contrast and electron backscatter diffraction (EBSD). Boundaries between misoriented domains (grains or subgrains) were determined by image analysis of orientation contrast images. In each domain, EBSD measurements gave the complete quartz lattice orientation and enabled calculation of misorientation angles across every domain boundary. Results are analysed in terms of the boundary density, which for any range of misorientations is the boundary length for that range divided by image area. This allows a more direct comparison of misorientation statistics between different parts of a sample than does a treatment in terms of boundary number.The strain in the quartzite sample is heterogeneous. A 100×150 μm low-strain partially recrystallised subarea C was compared with a high-strain completely recrystallised subarea E. The density of high-angle (>10°) boundaries in E is roughly double that in C, reflecting the greater degree of recrystallisation. Low-angle boundaries in C and E are produced by subgrain rotation. In the low-angle range 0–10° boundary densities in both C and E show an exponential decrease with increasing misorientation. The densities scale with exp(−θ/λ) where λ is approximately 2° in C and 1° in E; in other words, E has a comparative dearth of boundaries in the 8–10° range. We explain this dearth in terms of mobile high-angle boundaries sweeping through and consuming low-angle boundaries as the latter increase misorientation through time. In E, the density of high-angle boundaries is larger than in C, so this sweeping would have been more efficient and could explain the relative paucity of 8–10° boundaries.The boundary density can be generalised to a directional property that gives the degree of anisotropy of the boundary network and its preferred orientation. Despite the imposed strain, the analysed samples show that boundaries are not, on average, strongly aligned. This is a function of the strong sinuosity of high-angle boundaries, caused by grain boundary migration. Low-angle boundaries might be expected, on average, to be aligned in relation to imposed strain but this is not found.Boundary densities and their generalisation in terms of directional properties provide objective measures of microstructure. In this study the patterns they show are interpreted in terms of combined subgrain rotation and migration recrystallisation, but it may be that other microstructural processes give distinctive patterns when analysed in this fashion.     

西藏纳木错晚更新世以来湖面变化和藏北高原古大湖的演化

根据西藏纳木错及邻区发现的多处湖岸阶地和高位湖相沉积,确定了藏北高原古大湖的存在。水准测量表明,在纳木错沿岸发育了6级湖岸阶地,以及拔湖48～139.2m的高位湖相沉积;在拔湖26m以下,发育有8～30条湖岸堤;一条明显的湖蚀凹槽则集中出现在拔湖17.5～19.8m的高度上,与纳木错和仁错的分水垭口的高度相当。纳木错沿岸和邻区湖相或湖滨相沉积物的铀系年龄测定表明,高位湖相沉积形成于115.9～71.8kaB.P.的晚更新世早期;第6至第2级阶地形成于53.7～28.2kaB.P.的晚更新世中晚期;与湖蚀凹槽相当的湖滨相沉积则稍早于29.3kaB.P.;第2至第1级阶地,14C测定结果为2350～10390aB.P.。     

极隙区电子束流模电磁不稳定性

解析地研究了中高度（离他心3－4个地球半径）极隙区极低密度上行电子束流引起的沿磁力线传播的电磁个稳定性，上行电子束流和背景等离子体都考虑成冷等离子体．结果表明，上行电子引起的左旋和右旋圆偏振电磁来流模是不稳定的，当它与离子回旋模耦合时增长率达到最大值，频率色散关系仍为电子束流模特征这此结果对解释权隙区纬度地面站低频电磁波观测资料和理解极隙区动力学过程是很有益的．     

Geochronology of Middle and Upper Pleistocene Loess Sections in Hungary

The application of both thermoluminescence and infrared stimulated luminescence dating to the extensively studied “classical” Hungarian loess/paleosol sequences from Basaharc, Mende, and Paks provides a reliable chronological framework and climatostratigraphic reconstruction for the last interglacial/glacial cycle. Based on this combined luminescence dating study a new chronology is proposed for the “Young Loess” in Hungary. Luminescence dating suggests that the loess below the MF2 horizon formed during the penultimate glaciation. The MF1 horizon probably formed during an interstade within oxygen isotope stage 3. For the youngest loess, overlying MF1, a very high accumulation rate was determined. Large time gaps occur above MF2 and MF1, indicating that most of the record of the last glaciation is missing in the standard sections at Basaharc, Mende, and Paks. Either large discontinuities or a very low accumulation rate occurred in all three type sections during the soil-forming periods. High-resolution studies of climatic proxies using this combined luminescence dating approach provide a reliable chronological framework for loess and loess derivatives of the last glacial cycle in Hungary, although a precise and complete chronostratigraphic reconstruction cannot be achieved from the incomplete records found at these sites.     

甘肃巴谢剖面黄土-古土壤的光释光测年研究

光释光（OSL）测年是测定第四纪沉积物年龄的一种新技术。它通过单色光束激发使晶体中储存的电离辐射能释放出来。与热释光（TL）测年相比，OSL测年可以不考虑残留的OSL信号，而且测量具有简便、迅速且准确等优点。本文用细颗粒光释光技术对甘肃巴谢剖面的黄土-古土壤进行了测定，其测年结果与14C测年结果相吻合。这表明，光释光是一项极潜力的年代学技术。     

现代沉积的210Pb计年

²¹⁰Pb具有百年时间尺度沉积计年的重要价值。²¹⁰Pb_ex计年假设：沉积物是封闭系统；进入水体的²¹⁰Pb能有效地转移到沉积物中并不发生沉积后迁移；非过剩²¹⁰Pb与其母体²²⁶Ra保持平衡。²¹⁰Pb_ex计年可用稳定输入通量-稳定沉积物堆积速率模式、常量初始浓度模式或恒定补给速率模式。沉积物柱芯必须保持原态并以0．5～1cm间隔分截；用相应层节²²⁶Ra校正。沉积物表层混合作用及²²²Rn的丢失可能导致顶部²¹⁰Pb_ex异常。季节性缺氧湖泊沉积物顶部可能存在²¹⁰Pb及²¹⁰Po的再迁移。²¹⁰Pb与¹³⁷Cs两种计年方法原理上具有根本差别。²¹⁰Pb，¹³⁷Cs与沉积纹理方法对比是准确计年的重要保证。     

九甸峡工程区断层测年结果研究与讨论

断层的年代测定是研究断层活动性的重要内容之一。然而, 一个工程同一条断层会出现不同的测年结果, 从而引起争议和难予决断。近年来我们通过几个大型工程区域稳定性研究, 对此获得了一些认识。本文以洮河九甸峡地区几条主干断层为研究对象, 采用同位素年龄测定与野外地质调查和显微构造分析相结合的方法, 对断层测年问题作一分析和讨论, 也许对岩土工程断层活动性研究有一定参考价值。     

大别山超高压石榴多硅白云母片岩中钻石U－Pb年龄

大别山超高压石榴多硅白云母片岩中钻石Ｕ－Ｐｂ年龄刘晓春（中国地质科学院地质力学研究所，北京１０００８１）李惠民，左义成（地质矿产部天津地质矿产研究所，天津３００１７０）关键词石榴多硅白云母片岩，Ｕ－Ｐｈ年龄，早元古代表壳岩，印支期超高压变质，大别山高...     

Thorium and uranium isotopes in a manganese nodule from the Peru basin determined by alpha spectrometry and thermal ionization mass spectrometry (TIMS): Are manganese supply and growth related to climate?

Thorium- and uranium isotopes were measured in a diagenetic manganese nodule from the Peru basin applying alpha- and thermal ionization mass spectrometry (TIMS). Alpha-counting of 62 samples was carried out with a depth resolution of 0.4 mm to gain a high-resolution²³⁰Th_excess profile. In addition, 17 samples were measured with TIMS to obtain precise isotope concentrations and isotope ratios. We got values of 0.06–0.59 ppb (²³⁰Th), 0.43–1.40 ppm (²³²Th), 0.09–0.49 ppb (²³⁴U) and 1.66–8.24 ppm (²³⁸U). The uranium activity ratio in the uppermost samples (1–6 mm) and in two further sections in the nodule at 12.5±1.0 mm and 27.3–33.5 mm comes close to the present ocean water value of 1.144±0.004. In two other sections of the nodule, this ratio is significantly higher, probably reflecting incorporation of diagenetic uranium. The upper 25 mm section of the Mn nodule shows a relatively smooth exponential decrease in the²³⁰Th_excess concentration (TIMS). The slope of the best fit yields a growth rate of 110 mm/Ma up to 24.5 mm depth. The section from 25 to 30.3 mm depth shows constant²³⁰Th_excess concentrations probably due to growth rates even faster than those in the top section of the nodule. From 33 to 50 mm depth, the growth rate is approximately 60 mm/Ma. Two layers in the nodule with distinct laminations (11–15 and 28–33 mm depth) probably formed during the transition from isotopic stage 8 to 7 and in stage 5e, respectively. The Mn/Fe ratio shows higher values during interglacials 5 and 7, and lower ones during glacials 4 and 6. A comparison of our data with data from adjacent sediment cores suggests (a) a variable supply of hydrothermal Mn to sediments and Mn nodules of the Peru basin or (b) suboxic conditions at the water sediment interface during periods with lower Mn/Fe ratios.     

U—Series Dating of Fossil Bones：Results from Chinese Sites and Discussions on Its Reliability

Calculations,according to some open-system models,point out that while a statistically significant discrepancy between the results of two U-series methods,^230Th/^234U and ^227Th/^220Th(or ^231Pa/^235U),attests a relatively recent and important uranium migration,concordant dates cannot guarantee closes-system behavior of sample.The results of 20 fossil bones from 10 Chinese sites,19 of which are determined by two U-series methods,are given,Judging from independent age controls,8 out of the 11 concordant age sets are unacceptable,The results in this paper suggest that uranium may cycle into or out of fossil bones,such geochemical events may take place at any time and no known preserving condition may securely protect them from being affected.So for the sitew we have studied,the U-series dating of fossil bones is of limited reliability.