离子色谱分析在黄土和粉尘研究中的应用

黄土中存在着大量的碱金属及碱土金属，以往的测试方法多为原子吸收和ICP—MS，离子色谱法在测试黄土样品的碱金属和碱土金属元素含量中应用不多。将黄土地质标准样品进行消解后用离子色谱进行测试，测试效果良好，重复测试的相对标准偏差小于5％，与推荐值的相对误差小于5％，准确度和精密度符舍相关的质量控制要求。本实验方法测试的离子含量都在仪器响应呈线性的最佳测试范围之内，标准曲线经回归后相关系数均达到0．9999。黄土样品的分析结果与粉尘气溶胶样品的离子分析结果对比表明，此方法对于探讨粉尘起源以及沙尘暴天气的研究具有重要意义。     

面对水产饲料标准的思考

水产饲料标准的颁布，规范了市场行为，但数量偏少，不利于对水产饲料质量的全面管理.我国实行推荐性饲料标准，有助于生产适销对路产品，但在卫生安全指标上仍应加以规范.     

Growth and reproduction of the bivalve Spisula subtruncata (da Costa) in Dutch coastal waters

The bivalve Spisula subtruncata is usually abundant in shallow coastal waters along the Dutch coast. However, its biomass has been decreasing since 1995. In order to assess whether reproductive failure may be the cause of the observed decline over the last decades, the energy investment in reproduction of a population of S. subtruncata from central Dutch coastal waters was studied. The population studied consisted of individuals of up to four years old. Shell length reached maximum values of around 32 mm and individual total body, somatic and gonadal ash-free dry mass reached maximum values of about 278 mg AFDM, 252 mg AFDM and 76 mg AFDM, respectively. A clear seasonal cycle in somatic and gonadal mass was observed. Somatic and gonadal mass indices increased in early spring and reached maximum values during summer, followed by a decrease to minimum values at the beginning of the following year. Spawning was in June–July and settlement of spat seems to have occurred in July–August. Mean oocyte diameter was 57.43 ± 0.03 μm, corresponding to a volume of 98972 μm³. These results suggested that reproductive failure was not the cause of the current population decline. Most likely, unsuccessful settlement of spat and/or severe predation during the first months of life were responsible for the observed patterns.     

对虾体内氯霉素含量测定方法的研究

应用ＨＰＬＣ技术建立常用药物氯霉素的虾体动力学研究方法。该方法的特点是：与微生物法、比色法、气相色谱法、荧光法及免疫法比较．测试准确、快速且灵敏度高。应用该方法可以从虾体内的血液、肌肉、肝胰脏、肠胃中分离出被虾吸收的氯霉素，并定量测定。在１—５０μｇ／ｍｌ范围内线性关系相关系数为０．９９９５。     

深层搅拌法在超软弱港口地基上的工程应用

某港口堆场地基上部5．0m系吹填而成，地表下18m范围均属软土，经真空预压初级加固后地基承载力仅在80—90kPa，局部区域上部淤泥土层土性指标较差，含水量大于50％，地基承载力不足60kPa。为了使地基达到230kPa的承载要求，设计采用深层搅拌法加固超软弱地基。通过现场成桩工艺试验和检测表明，桩身水泥土强度在90d龄期时大于1．80MPa，单桩承载力标准值大于150kN，以φ600桩径、桩长13．5m、置换率为0．308和φ500桩径、桩长13．5m、置换率为0．267两种方案布置的复合地基承载力标准值均超过了230kPa的设计要求。试验结果表明，深层搅拌法在港口超软弱地基土应用只要施工工艺适当，完全可以使地基承载力提高2—3．5倍以土，从而节省大量的工程投资。     

单中继星单低轨卫星的联合定轨精度分析

针对由单中继星和单低轨卫星组成的联合定轨系统,给出了系统内不同轨道卫星摄动项的选取方案和卫星间的可见性判别模型。在模拟出含有白噪声的四程测距观测数据文件的基础上,研究了测距精度和采样弧段对联合定轨中高、低轨卫星定轨精度的影响。得出如下结论:联合定轨更有利于对低轨卫星的轨道改进;同样的采样时间条件下,测距噪声越小定轨精度越高,并且采样时间越短它的影响越明显;同样的测距噪声条件下,所用资料的采样时间越长精度越高,但当测距精度很高时,TDRS达到最好定轨精度所需的采样时间相应有所缩短。并在定出轨道后进行了轨道预报,分析了轨道预报的趋势及精度。     

GPS单点测速的误差分析及精度评价 (英文)

Error sources which decrease the accuracy of GPS in absolute velocity determination have been changed since SA was turned off. Firstly, quantities of all kinds of error sources that influence velocity determination are analyzed. The potential accuracy of GPS absolute velocity determination is derived from both theory and field GPS data simulation. After that, two tests were carried out to evaluate the performance of GPS absolute velocity determination in the case of a static and an airborne GPS receiver and INS （Inertial Navigation System） instrument in kinematic mode. In static mode, the receiver velocity has been estimated to be several mm/s with the carrier-phase derived Doppler measurements, and several cm/s with the receiver generated Doppler measurements. In kinematic mode, GPS absolute velocity estimates are compared with the synchronized measurements from the high accuracy INS. The root mean square statistics of the velocity discrepancies between GPS and INS come up to dm/s. Moreover, it has a strong correlation with the acceleration or jerk of the aircraft.     

一种新型非线性滤波理论及其应用

研究一种新型的非线性滤波理论,即Unscented卡尔曼滤波（UKF）,同时为了获得更高的计算效率和确保协方差阵的非负定性,研究了平方根UKF。将UKF和平方根UKF应用到星载GPS卫星定轨中,实际算例表明UKF和平方根UKF的性能要优于常用的推广卡尔曼滤波的性能。     

构建基于GIS的房产管理

阐述了基于GIS房产管理的关键是建立统一的数据分类与编码标准,核心是建立房屋的空间地理属性信息、自然属性信息、社会人文属性信息的链接,基础是建立房产地理信息数据库。并提出了建立房产地理信息数据库的方法、设计思路和方式。     

重要找矿指示元素的野外快速分析法——金的野外快速分析

近年来,作者发展了七种以上重要找矿指示元素的野外快速分析法,此乃其一。文中提出一种新的金样冷浸技术,引进了新的光导光度检测方法,样品经溴化钠—硫酸—过氧化氢冷浸,用经丙酮—MIBK处理的泡沫塑料富集金,经混合解脱剂解脱并直接取解脱液用改进的微珠析出法或用光导光度法测定。取10g样品,可测定0.0005-50g/t范围内的金。方法简便、快速,可在普查分队驻地进行,每一工作日可测定80多个样品,由于废弃了王水分解样品和泡沫塑料的灰化,具有广阔的应用前景。