悬浮液原子荧光光谱法测定化探样品中的痕量汞

拟定了将悬浮液技术与汞蒸气原子荧光光谱法相结合测定化探样品中痕量Ｈｇ的分析方法。控制悬浮液中试样粒度在２００目，试样质量浓度１５ｇ／Ｌ，用电磁搅拌和载气搅拌保证悬浮液分散稳定，水溶液标准作校正曲线，方法的检出限为６ｎｇ／ｇＨｇ。对水系沉积物国家标准物质中痕量Ｈｇ进行测定，结果与标准值相符，对含Ｈｇ０１０μｇ／ｇ的ＧＢＷ０７３０５（ＧＳＤ５）测定１１次，ｘ为０１０５μｇ／ｇ，ＲＳＤ为５４％。     

3≈6 Months Variation of Sea Surface Height in the South China Sea and Its Adjacent Ocean

Sea surface height (SSH) variations with a period of 36 months (SSH36 variations) in the South China Sea (SCS) and its adjacent ocean are intensively investigated using six years of TOPEX/POSEIDON-derived SSH data. The results show that there appears higher energy of SSH36 variations in the east of the Luzon Strait and in some areas of the SCS, both of which are correlated with each other. The SSH36 variations usually propagate westward in the subtropical region of the northern Pacific Ocean and turn northward in the east of the Luzon Strait while they sometimes propagate into the SCS through the Luzon Strait with the phase speed of about 11–12 cm/s, which may be considered as Rossby waves. It can be inferred that the SSH36 variations are strongly associated with current structures and eddies in the SCS because of their significant intensiveness. The SSH variations with the period of 6 months are more dominant than those with the other periods in the SCS.     

用6－甲氨基嘌呤诱导贻贝四倍体胚胎

在滤过海水中以４×１０（－４）ｍｏｌ·Ｌ（－１）６－甲氨基Ｃ嘌呤（６－ＤＭＡＰ）处理贻贝Ｍｙｔｉｌｕｓｅｄｕｌｉｓ受精卵或胚胎，受精激活后５０或１２０ｍｉｎ处理２０—３０ｍｉｎ，分别抑制第一或第二次有丝分裂，以诱导四倍体胚胎。顶荧光显微观察表明，６－ＤＭＡＰ有效地抑制了第一和第二次卵裂。它使细胞核染色质分散，抑制了原核的移动和染色体的分离，并防碍卵裂沟和极叶的形成，从而诱导出四倍体胚胎。对第一次卵裂的抑制产生８２．８％的四倍体胚胎；第二次卵裂抑制产生５８．６％的四倍体胚胎。由于６－ＤＭＡＰ如此有效，而且价格便宜以及对人体无害，与沿用的化学诱导剂细胞松弛素Ｃ．Ｂ．相比，它应该可以成为双壳类软体动物染色体操作研究的理想化学诱导剂之一。     

AccQ-Tag法测定毛蚶抗贫血口服液中的氨基酸含量

以 6 -氨基喹啉 - N-羟基琥珀酰亚胺基氨基甲酸酯 (AQC)为衍生剂 ,与毛蚶抗贫血口服液中的氨基酸柱前定量衍生 ,用 Waters HPL C仪 ,Acc Q- Tag TM专用 C18柱 (3.9mm× 15 cm) ,以140 mmol· L-1的醋酸钠溶液 (p H5 .0 2 )为溶剂 A,乙腈为溶剂 B,超纯水 (Milli- Q水 )为溶剂 C,进行梯度洗脱 ,检测波长为 2 4 8nm,35 min测试完毕。各种氨基酸测定的重现性 RSD%均 <3.0 %(n=5 )。该方法简便快速 ,结果准确可信。     

中国对虾及中华绒螯蟹多倍体诱导中6-DMAP在卵子中残留量的检测

海洋动物多倍体的诱导目前已成为海水养殖中品种改良的重要手段(楼允东，1984)。在美国，太平洋牡蛎和虹鳟的多倍体诱导已大规模应用于生产，并获得良好的经济和社会效益。我国也先后开展了鱼类(桂建芳等，1991；尤锋，1993)、中国对虾(戴继勋等，1993；相建海等，1992)、贝类(喻子牛等，1995)及中华绒螯蟹(陈立侨等，1997)等多种海洋动物多倍体诱导的研究，并取得了一些进展。6-二甲基氨基嘌呤(6-DMAP)由于其低毒、经济和高效，目前已成为海洋动物多倍体诱导中经常使用的诱导剂，但至今，国内外尚无关于6-DMAP在卵子内的残留的报道。在环境保护和生物安全倍受关注的今天，人们非常关心多倍体诱导食物的安全性问题，本文首次利用高压液相色谱技术检测了在中国对虾和中华绒螯蟹多倍体诱导处理后，卵子和幼体内6-DMAP的残留量，并对检测结果进行了分析讨论。     

Period analysis of theδ Scuti star HD93044

HD93044 was observed electrophotometricaly on April 21, May 1, 2 and 4, 1991 at Xinglong Station of Beijing Astronomical Observatory. Combining the data with Li Zhiping's data together and a period analysis was completed using a program which consists of a combination of Fourier transforms of prewhitened data and the multifrequency least squares of brightness residuals (LSR). Three pulsation frequencies (11.90809, 16.79553, 22.44827 cycles per day) with visual amplitudes between 0.0056 and 0.0203 mag were found. The solution fits the observations to +0.0071 mag which is equal to the mean square deviation of observations. The first frequency (11.90809 cycles per day) must be the right value of the fundamental frequency of HD93044.     

WRF2.2在FC6系统上的安装运行

简要介绍了WRF模式的概况,并着重介绍了如何在Fedora Core6上安装运行WRF模式的最新版本WRF2.2。它主要包括两个部分,WPS前处理模块及WRF主模块。在介绍WPS前处理模块时,还对WPS的图形界面程序DomainWizard进行了简介。     

Origin of glacial–fluvial landforms in the Azas Plateau volcanic field, the Tuva Republic, Russia: Role of ice–magma interaction

The basaltic Azas Plateau volcanic field is located in the Tuva Republic of the Russian Federation. The area was glaciated multiple times, and the field is characterized by the formation of subglacial volcanoes called tuyas, but subaerial volcanoes and lava fields also exist. A combined study of remote sensing and field observations in the vicinity of the tuyas in the southeastern Azas Plateau volcanic field identified landforms that are best explained by the jökulhlaup hypothesis. The landforms include elongated hills, paleochannels, and butte and basin topography. These landforms are hypothesized to have formed by both erosion and deposition caused by high-energy water streams. The triggering for the hypothesized jökulhlaups was either melting of ice by subglacial volcanism and/or destabilization of ice-dammed/subglacial reservoirs. The age estimation of the flood events is difficult, but they probably occurred during the ice ages of the Quaternary, as late as in the Middle-Late Pleistocene.     

利用MODIS资料反演北京及其周边地区气溶胶光学厚度的方法研究

基于 6S辐射传输模式 ,文中同时采用暗像元法和结构函数法建立了利用EOS Terra/MODIS 0 .6 6和 0 .4 7μm通道数据反演陆地气溶胶光学厚度的遥感模型 ,用于获取北京及其周边地区的气溶胶光学厚度。同时 ,利用与卫星观测同步的地基太阳光度计观测资料估计的气溶胶光学厚度数据验证卫星资料反演结果。研究结果给出了如何选择算法、卫星通道数据和气溶胶模型的最佳组合获取理想气溶胶光学厚度的方法。采用 4种气溶胶模型供反演计算选择。在研究中发现 ,暗像元法不适用于城市地区气溶胶光学厚度反演 ,这不仅与亮地表条件的限制有关 ,而且具有强吸收特性的城市气溶胶也是重要影响因素。两种算法由相同气溶胶模型假定误差造成的气溶胶光学厚度反演误差方向 (增加或减小 )相反。反演试验获取的气溶胶光学厚度分布指出 ,石家庄—北京—天津一线易出现气溶胶光学厚度高值带。     

不同类型岩土对六价铬的抗污染性分析

对已经受铬污染的、未受铬污染的以及受造纸厂废水污染的不同岩土样，分别用蒸馏水和铬污染水作为淋液进行淋滤试验。受铬污染的岩土会发生二次溶解，导致淋滤液受Cr^6 污染。受造纸废液污染的土样对污染水中的Cr^6 具有较强的吸附截留作用，其去除Cr^6 效果远优于一般岩土，即对Cr^6 的抗污染性较好。