TBP－（X－5）反相色谱分离m－NPF分光光度法测定铀

本文研究了以磷酸三丁酯为固定相，大孔聚乙烯苯（Ｘ－５型）为担体的浸渍树脂、垂直型反相色谱柱，对铀分离富集的基本性能，以及铀（Ⅳ）－间硝基苯基萤光酮（ｍ－ＮＰＦ）一氨三乙酸（ＮＴＡ）－吐温－８０显色体系的反应条件，提出了ＴＢＰ（Ｘ－５）分离，ｍ－ＮＰＦ－ＮＴＡ－吐温－８０光度法测定铀，经标准样品验证，结果满意。     

粘滑失稳及其物理场时空分布的实验研究

摩擦滑动的物理场实验研究表明：（１）能量空间分布的差异是失稳的重要条件，单发型大事件常发生于高能量向低能量的突变带或高能量背景区内的相对低能量区；（２）单发型大事件的孕育过程常常经历若干个能量输入输出循环，产生多个前兆阶段，并在失稳前源区常有一个弱化过程。小震或群发型事件失稳前常常只有一个能量积累与强化的过程，失稳前兆阶段性反映较差；（３）粘滑失稳时断层的位错与声发射的大小未见明显关系     

镉—5—Br—PADAP—溴化十六烷基三甲基铵—十八醇聚氧乙烯(20)醚显色体系的研究及应用

本文研究了镉-5-Br-PADAP-溴化十六烷基三甲基铵-peregalo显色体系的光谱特征,显色条件,络合物的组成、干扰及其消除。实验证明该法灵敏度高,ε=1.3×10~5l·mol~(-1)·cm~(-1)。选择性较好,显色酸度范围较宽pH=8.0-9.5,络合物最大吸收波长为560nm,镉在0-10μg/25ml的含量范围内服从比尔定律。经标准水样、工业废水及生活用水验证,不经分离可测定水中PPb级的微量镉。     

MM5中尺度非静力模式对云南省降水预报检验

根据MM5／V3中尺度非静力模式数值预报结果，检验了该模式在云南2001年汛期（6－10月）的降水预报效果。结果表明，MM5模式降水预报对云南大部分地区的小雨有较高的TS评分，对于全省性大雨过程，MM5模式24小时降水预报的TS评分高于同期预报员的主观预报，但对暴雨及以上量级的降水预报，模式结果不太理想。     

中尺度数值模式(MM5V3)在沈阳区域气象中心的试用

简单介绍了沈阳区域气象中心在微机上调试和试用中尺度数值模式MM5V3的情况，MM5V3在前、后处理上使用Fortran90编程，与MM5V2有一定差别，利用T106L19资料和常规探空报形成经、纬网格的初值，预处理场和侧边界，代入模式前处理系统中，模式运行完毕后，预报产品直接进入MICAPS、Vis5d、Grads系统，进行图形显示，在2000年汛期试用中发现，MM5V3对东北地区的强降水过程有一定的预报能力，预报评分表明，MM5V3的降水预报结果和MM5V2互有优劣，总体来看，MM5V3的预报质量略高于MM5V2。     

湘东─赣西NNE向走滑构造

湘东─赣西构造岩浆带位于郯庐断裂南延的关键性部位。中生代以来，该区 NNE向左旋走滑构造主要由会聚走滑和 K─ E离散走滑构造叠加而成。会聚走滑作用造就了 NNE向雁列式剪切断裂系、剪切弯曲和旋转构造、压剪性煤盆地以及断层动热变质─剪切重熔型花岗岩；而离散走滑作用则控制了该区广泛发育的张剪性红盆地、盆岭式构造地貌、以及大规模中低温热液矿床的形成。湘东─赣西复杂的平移构造型式很可能与该区地壳结构分层特征、前期断裂构造格局、平移幅度和多期走滑构造作用四个因素有关。     

Processing of oxidised nitrogen compounds by passage through winter-time orographic cloud

Four case studies are described, from a three-site field experiment in October/November 1991 using the Great Dun Fell flow-through reactor hill cap cloud in rural Northern England. Measurements of total odd-nitrogen nitrogen oxides (NO _y ) made on either side of the hill, before and after the air flowed through the cloud, showed that 10 to 50% of the NO _y , called NO _z , was neither NO nor NO₂. This NO _z failed to exhibit a diurnal variation and was often higher after passage through cloud than before. No evidence of conversion of NO _z to NO₃ ^- in cloud was found. A simple box model of gas-phase chemistry in air before it reached the cloud, including scavenging of NO₃ and N₂O₅ by aerosol of surface area proportional to the NO₂ mixing ratio, shows that NO₃ and N₂O₅ may build up in the boundary layer by night only if stable stratification insulates the air from emissions of NO. This may explain the lack of evidence for N₂O₅ forming NO₃ ^- in cloud under well-mixed conditions in 1991, in contrast with observations under stably stratified conditions during previous experiments when evidence of N₂O₅ was found. Inside the cloud, some variations in the calculated total atmospheric loading of HNO₂ and the cloud liquid water content were related to each other. Also, indications of conversion of NO _x to NO _z were found. To explain these observations, scavenging of NO _x and HNO₂ by cloud droplets and/or aqueous-phase oxidation of NO₂ ^- by nitrate radicals are considered. When cloud acidity was being produced by aqueous-phase oxidation of NO _x or SO₂, NO₃ ^- which had entered the cloud as aerosol particles was liberated as HNO₃ vapour. When no aqueous-phase production of acidity was occurring, the reverse, conversion of scavenged HNO₃ to particulate NO₃ ^-, was observed.     

菏泽5.9级地震前后水准测量与承压水变化关系的研究

利用深层承压水头观测结果,对东明——菏泽长水准测线8——9号测段的高差变化进行了回归计算和相关分析。认为菏泽市城区9号测点下沉的主要原因是受深层承压水头变化的影响。排除地下水影响因素后证实,1983年11月7日菏泽5.9级地震前后仅3mm左右的升降变化,表明9号测点对这次中强地震仅能反映微弱的形变信息量。     

昆明1943年5级地震的发震地段考证

结合资料记载与调查,认为该地震发生在昆明市区西南边缘的西山断裂地段。