Th-and U-bearing minerals in the SE Mediterranean margin of Spain

This paper presents the first specific study of the Th-and U-bearing minerals, which were recently found in the SE Mediterranean margin of Spain (El Hoyazo area,Almeria province). These minerals are REE phosphates (mainly monazite) which occur as amoeboidal-to-elongate inclusions,from around 10 120μm to 120μm, hosted in single garnet crystals from dacite lavas and metamorphic rocks from the El Hoyazo Volcanic Complex. Th and U contents are higher than 1 wt%, with 3.04 to 5.62wt% for Th02, and 0.7 to 1.75 wt% for UO2. Both elements are also found in xenotime (ThO2:0.24,UO2:0.27wt%). Given that the erosion of the volcanic source rocks has generated a “placer-type” deposit of monazite sands and that garnets (main carriers of monazite) are being commercialised, an environmental monitoring and management plan should be urgently executed in the area.     

汞型活性炭纸富集-XRFA法测定水样中的痕量SCN^-

SCN^-的测定大都采用分光光度法[1，2]。用波长色散X-射线荧光光谱测定痕量SCN^-的方法，至今尚未见报道。     

β-环糊精-1，2，5，8-四羟基蒽醌包结物荧光法测定铍

本文对1，2，5，8-四羟基蒽醌(THA)与镀形成配合物和THA进入β-环期精(β-CD)的内空腔与镀形成包结物这两种测定镀的荧光分析方法进行了比较，试验表明，后者的灵敏度和重现性有显着提高．选择性明显改善。详细研究了方法的测定条件．并应用于矿样中痕量镀的测定，结果符合质量要求。     

Experimental Research on Microscopic Indicators of Temperature＇ s Returning-to-Zero in Deformation of Calcite and Discussions of Correlation Problem

In order to determine the degree of returning-to-zero of temperatures of deformed calcite, a series of rock-breaking experiments were designed to test calcite-rich limestone samples under fixed confining pressures and different temperatures. The consolidated deformed samples in their initial state were observed under a microscope and the microscopic indicators in different zero-returning states were put forward, thus providing a microscopic foundation for evaluation of reliability of dating values of deformation in calcite. At last, the correction of dating values of deformation for samples whose temperature has not yet returned to zero is discussed.