坚持所内外“三结合”，自力更生发展我国科学技术——记JQ-1型轻便式X射线晶体分析仪的试制和投产

在继续普及、深入、持久地开展批林批孔运动的大好形势下，由我所研制、我国某地仪器厂生产的JQ-1型轻便式X射线晶体分析仪正式投产了。这种仪器是以X射线粉末法用来作晶体物相分析的。它与同类大型仪器相比，具有体积小(不到大型的十分之一)、重量轻(仅为大型的十分之一)、操作简单、携带方便和造价低廉(成本为大型的四分之一)等     

DF—1型电化学分析仪

Model DF-1 electrochemical analyzer is a many-purpose electrochemical instrumentation with following five functional select switches for operating conditions: cathodic /anodie polarization; single/cycle sean；two/three electrodes system；direct/derivative output；normal/differential mode. Consequently they can be combined into several working manners, result in different experimental methods as consistent with desire. This instrument has manifold compensator and adjuster with a wide-range, so that the sensitivity and the signal graph have been able to improve. In addition, the instrument incorporates a strip-chart recorder and an exact timer. It is also equipped with electrochemical bench and a set of electrodes including the rotating glassy carbon electrode, gold plate electrode, silver plate electrode, mercury coated silver base electrode, hanging mercury electrode etc. In order to broaden the field of its application, all units of the instrument can be unitized, but each and every can be also used independently. The instrument is applicable to polarography, voltammetry, potentiometric stripping, potentiostatic electrolysis,differential technique, coulometry, linear polarization method, cycle voltammetry, passivation curve, and some other electrochemical technique, which have need for electrochemical cell with two, three，or four electrodes. This paper describes the design fundament, feature and specification of the electrochemical analyzer, and finally gives laboratory application some experimental examples.     

施加有机降解菌制剂虾池底质中有机碳和总氮的变化

2001年7月至10月，进行了有机降解菌制剂改良底质的实用实验，测定了底质有机污染指标：有机碳和总氮。结果显示，有机碳未出现积累，对照组与处理组差异显（P＜0．001），有机降解菌降解有机碳效果显；总氮出现积累现象，处理组与实验组之间差异不显；碳氮比在底质中呈下降趋势。     

BJKF-1型便携式近红外矿物分析仪在宝玉石鉴定中的应用

将国产便携式近红外矿物分析仪引入宝玉石无损伤鉴定。通过实测图谱比对,就矿物的近红外光漫反射光谱特征,对主要宝玉石品种的可鉴别性进行分析;对翡翠等作为多矿物集合体表现出的近红外光谱特点及翡翠A货、B货、C货的可区分性亦作了初步分析。实测结果表明,利用易于普及的BJKF-1型近红外矿物分析仪在波长1 300~2 500 nm的近红外测量区域内对黄玉、绿柱石、电气石等部分宝石类,透闪石、叶蜡石、蛇纹石、硬玉等大部分玉石类样品开展日常检测工作,有广阔的应用前景。     

两台营养盐分析仪性能评价与结果比对分析

对863计划重点项目研制的两台营养盐分析仪进行了技术性能评价,并对两台仪器检测结果与国标法检测结果进行了一致性评价。结果表明,两台国产仪器的技术性能均能达到长江口示范区的监测要求,检测结果与国标方法具有良好的一致性。     

辽河大伙房水库汇水区农业非点源污染入库模拟

利用输出系数法和SWAT模型,对大伙房水库汇水区农业非点源污染(ANSP)进行了入库模拟研究,并用2006—2009年的水文和水质监测数据对模型进行了校准和验证。研究结果表明:汇水区年均输入到水库的泥沙量、总氮和总磷负荷分别为82.65×103 t、1 873.49t和81.97t;月入库泥沙量、总氮和总磷负荷与径流量有着较强的相关性,ANSP的产生和迁移受降水、径流过程影响很大,每年7、8月份的氮、磷和泥沙流失量达到年内最大值,分别占全年流失总量的42.64%、44.42%和67.91%。水库汇水区各流域对水库氮、磷污染的贡献率由大到小依次为:浑河流域(清原段)、苏子河流域、社河流域和水库周边小流域。     

元素分析仪-同位素比值质谱仪测定海洋沉积物有机碳稳定同位素方法初探

初步建立了利用元素分析仪-同位素比值质谱仪(EA-IRMS)联用技术测定海洋沉积物中有机碳稳定同位素的方法。标定了标准工作参考气CO2(δ13CvsPDB为-32.053‰);验证了仪器的稳定性,标准偏差为0.009‰;当离子流强度范围为0.4～8.7 V时,总体线性为0.0337‰/V,小于仪器线性指标0.06‰/V的要求;同时测定了国家标准物质GBW 04408、国际标准物质Urea和海洋沉积物样品M01的精密度和准确度,标准偏差在0.04‰～0.13‰范围内;并在三家实验室进行了测量比对实验,标准偏差小于0.20‰,满足地质样品再现性0.5‰的要求。所选样品区域δ13Corg范围为-25.29‰～-22.30‰,表明该海域总有机碳是陆源和海源两种来源的混合物。     

水样原位自动采集分析仪获实用新型发明专利

中国地质科学院水文地质环境地质研究所自主研发的水样原位自动分析仪于近日获得实用新型发明专利。水样原位自动分析仪包括采样机、控制面板、跨绕采样机电缆的采样支架以及连接在电缆自由端的采     

Laboratory application of laser grain-size analyzer in determining suspended sediment concentration

Suspended sediment concentration （SSC） is an important parameter in marine sedimentology. With the development of technology, many acoustic and optical devices, such as the Laser In-Situ Scattering and Transmissometry, have been designed to meas-ure in situ SSC and grain size distribution. But due to fund or other restrictions, many experiments were only conducted in laboratory, using an indoor laser grain-size analyzer and gravimetric method to measure grain size distribution and concentration, respectively. In this study the laboratory experiment is simplified by omitting the tiring step of gravimetric method. The connections between SSC and other parameters （obscuration, D50 and sorting index） were investigated based on 124 surface sediment samples collected from different offshore areas. A new method is developed for determining SSC in laboratory using a laser grain-size analyzer.