60Co－γ辐照对坛紫菜原生质体诱变的研究

利用^60Co-γ射线对坛紫菜（Porphyra haitanensis）原生质体进行辐照诱变，发现原生质体对^60Co-γ射线有极强的耐受性。前期的培养结果表明，原生质体是一种理想的诱变材料。诱变结果表明，^60Co-γ射线对坛紫菜可诱变剂量范围很大，从200-1300 Gy均有突变株生成。诱变后细胞的存活率不宜作为坛紫菜诱变最佳剂量的指标。     

Origin and three-dimensional fluorescence spectrum of the chromophoric dissolved organic matter in Yangtze estuary, East China

Dissolved organic matter （DOM） is an important chemical component in natural water. Chromophoric dissolved organic matter （CDOM）, a fraction of optical properties, plays art important role in the biogeochemical cycle of nutrients in aquatic environment. People realized that DOM cycle is crucial in the global carbon and nitrogen flux, and also is inherently related to nutrients and trace metal elements. Therefore, CDOM was concerned by scientists in global oceanography and limnology fields. Water samples were collected from three sections （North Channel, South Channel and Zhuyuan） of the Yangtze （Changjiang River） estuary in March 2006 Three-dimensional excitation emission matrix （3-DEEM） fluorescence spectra were analyzed for those filtrates through Whatman GF/F filters. Dissolved organic carbon （DOC） was also measured by TOC analyzer. The tidal variety was also taken into account. The 3-D EEM fluorescence scans suggested the fluorescence characteristics of humic acid （Ex=332-344 nm, Em=439-451 nm） and fulvic acid （Ex=250-254 nm, Em=472-478 nm） were obvious, and the fluorescence group of protein-like and tyrosine （Ex=230 nm, Em=283 nm） was also found. They are mainly composed of CDOM in the Yangtze estuary. Further data analysis, especially the fluorescence index （f 450/500）, showed that terrestrial signal was rather strong （1.41-1.65） in the surface water, however, some terrestrial CDOM signals of bottom water showed excursions （1.28-1.39）. On the other hand, anthropogenic sign was impressed in the waters of Zhuyuan, which is one of the main drain outlets of Shanghai Metropolis. DOC concentrations ranged from 2.2 mg/L to 3.4 mg/L in Zhuyuan and South Channel, and from 2.0 mg/L to 2.4 mg/L in North Channel. The tide effect played a role in the composition of the CDOM measured by 3-D fluorescence scan technology.     

浙江古代青瓷(1127～1279年)的化学组成及其意义

本文用ENGLE-型微探针能量色散X荧光光谱(EDXRF)技术测定了一批青釉瓷残片中的16种元素氧化物的含量,其残片来自浙江杭州地区的南宋郊坛窑和老虎洞窑。由主量元素判别方程的Q值表明,两类青釉瓷均属官窑制品。主成分统计分析看出,郊坛官窑与老虎洞官窑的瓷釉成分有明显不同,但其胎质成分的分布,却有部分的重叠,这显示了当时两处官窑的工匠们在使用胎料中的交往。从釉层、过渡层、和胎层的Al2O3和CaO的含量数据表明,郊坛官窑和老虎洞官窑的青釉瓷制品,分别存有厚度为120～140μm和230～240μm的过渡层,表明两处使用釉料和烧制工艺上的…     

X射线衍射峰五基本要素的物理学意义与应用

本文根据Bragg衍射方程、Scherrer方程、衍射强度计算原理，研究讨论了X射线衍射5构成要素中的衍射峰位置、衍射峰宽度、衍射峰高度的物理学意义。根据实验研究证明了衍射峰不对称性的几何条件特征，并用地质事实验证了衍射形态变化与晶格应变和粒度大小的内在联系。从而阐明了单个衍射峰5基本构成要素的完整物理学意义，并以实例论证了5要素的实际应用价值。     

化探结合X射线荧光测量在西天山确定异常元素赋存矿物形式的实践

在新疆特克斯和昭苏地区开展化探工作中结合X射线荧光现场样品测试，进一步分析确定测区异常成矿元素赋存的矿物形式和可能的元素赋存状态，尤其是对赋存矿物形式的确定，对于指导勘探技术人员现场找准重要成矿异常部位具有现实意义。     

湖泊沉积物中胶黄铁矿的鉴出及其磁学意义

对青藏高原东部若尔盖盆地钻孔获取的湖泊沉积物进行了详细的岩石磁学调查及矿物学鉴定, 发现大量胶黄铁矿存在, 并认定其为主要的磁载体. 该矿物颗粒细小, 粒度均匀, 可能为生物化学成因. 与大量文献报道的相反, 在长期暴露于空气后, 样品中的胶黄铁矿仍未被氧化. 这可能与钻孔内该矿物被硅质胶结物包裹有关. 研究结果初步揭示了湖泊沉积物磁学研究的复杂性, 同时也为环境磁学机理的研究提供了新的线索.     

三羟基荧光酮在荧光分析中的应用

对三羟基荧光酮的性质、表面活性剂及其增敏作用以及在Ｃｕ等２０个元素分析的应用作了综述。引用文献４１篇。