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61.
气相色谱法测定地下水中六六六结果的不确定度评定 总被引:7,自引:4,他引:3
依照《测量不确定度评定与表示》,对气相色谱法测定地下水中六六六(HCH)四种单体结果进行了不确定度评定。分析了测量过程中引入的不确定度来源,包括提取液体积的量取、样品提取溶液的定容体积、分析仪器的进样量、标准系列溶液的测量以及仪器重复测定等分量引入不确定度及其各参数的采集和计算方法,最后合成标准不确定度,通过乘以95%概率下的扩展因子2,获得测量结果的扩展不确定度。 相似文献
62.
碱消解-高效液相色谱-电感耦合等离子体质谱法测定生物样品中的甲基汞和乙基汞 总被引:7,自引:2,他引:5
建立了碱消解-高效液相色谱-电感耦合等离子体质谱联用系统测定生物样品中甲基汞(MeHg)与乙基汞(EtHg)的分析方法。为提高灵敏度,选用微流量的PFA雾化器,在优化的检测条件下,MeHg及EtHg检出限可达到0.036μg/L和0.03μg/L;线性范围达到4个数量级,两条工作曲线线性相关系数为1。对1.78μg/L MeHg、1.65μg/L EtHg的混合标准溶液重复测定7次,色谱峰面积的相对标准偏差(RSD)分别为1.79%和1.44%。对标准物质BCR 464(金枪鱼)的分析结果表明,测定值与标准值基本吻合,但略低于标准值;甲基汞和乙基汞的加标回收率分别为85.9%和84.5%。高效液相色谱与质谱联用技术的高灵敏度和低检出限能够满足生物样品中汞形态定量分析的要求。 相似文献
63.
64.
激光拉曼光谱法分析多种显微组分荧光变化及其应用 总被引:1,自引:1,他引:0
利用激发488 nm激光的氩离子激光器作为RENISHAW inVia型激光拉曼光谱仪的光源,建立了多种显微组分荧光变化(FAMM)分析方法,并对镜质体反射率明显抑制的东营凹陷有效烃源岩进行了测定。结果表明,东营凹陷有效烃源岩的有机质类型越好,镜质体反射率抑制程度越高,有效烃源岩的真实成熟度应主要处于0.64%~1.30%,而不是实测镜质体反射率所反映的0.37%~1.10%。 相似文献
65.
熔积岩指的是侵入、混合到未固结或弱固结的湿沉积物中的熔浆分解、原位形成的一类特殊岩石。正确地认识该类岩石,有利于增进人们对岩浆-水(沉积物)相互作用过程的理解,恢复古环境。在青海南部沱沱河地区发现了一套角砾为撕片状、锯齿状及浑圆状的安山岩,胶结物为铁硅质组合的特殊熔积岩。研究表明,该熔积岩的角砾为岩浆遇水后快速淬火、裂解的产物,铁硅质组合为海底喷气沉积形成的含铁建造;且安山岩与含铁建造发生混合时,含铁建造尚未固结。该套熔积岩的发现,改变了长期以来对开心岭铁矿为火山热液交代安山岩而形成的认识,对于在矿区寻找VMS型矿床、区域内寻找海底热水喷流沉积型矿床具有重要的启示意义。 相似文献
66.
高、低煤阶煤层气藏地质特征及控气作用差异性研究 总被引:4,自引:0,他引:4
高、低煤阶煤层气地质特征及控气作用差异性是研究煤层气富集成藏的重要组成部分,是煤层气勘探开发理论研究过程中重要的基础性研究领域之一。本文以中国沁水、阜新盆地和美国粉河盆地等典型的含气盆地为例,探讨了高、低煤阶煤层气的储层物性差异,分析了构造控气和水文地质控气作用的差异性。研究表明,高煤阶气藏含气量高,CH4百分含量高,δ13C1值大于-38.75‰,储层渗透率变化小,储层改造难,构造热事件对煤层气的生成、富集贡献大,持续的水动力使气藏遭到破坏,且破坏幅度大,现今地下水格局对气藏的形成具有一定的影响;低煤阶气藏含气量低,CH4百分含量低,δ13C1值大于-49.11‰,储层渗透率变化大,储层易改造,煤热演化史及煤阶影响着煤层气的生成、富集,在煤层气生成过程中活跃的水动力是甲烷生成的主要的水文地质条件之一,但持续的水动力使气藏遭到破坏,且破坏幅度小,而合适的地层水矿化度则是低煤阶煤层气生成的重要条件,地下水格局对气藏的调整和改造起到决定性的影响。 相似文献
67.
Delineation of groundwater protection zones by the backward particle tracking method: theoretical background and GIS-based stochastic analysis 总被引:1,自引:0,他引:1
Konstadinos N. Moutsopoulos Alexandra Gemitzi Vassilios A. Tsihrintzis 《Environmental Geology》2008,54(5):1081-1090
The backward particle tracking method, an effective and powerful tool that can be used to delineate groundwater protection
zones, is presented. The theoretical background and insights on the applicability of this method are provided. Moreover, the
present work enriches the backward particle tracking method with an uncertainty analysis concerning the porosity values, applying
a Monte Carlo (MC) approach, coupled with the use of geographical information systems (GIS). As an application example, a
wellfield in the Komotini area, Greece, is investigated. The present study may serve as a potential guideline for wellfield
delineation, particularly in areas like Greece where lack of data related to the hydrogeological system is often a problem. 相似文献
68.
The largest karst cave discovered in a tunnel during motorway construction in Slovenia’s Classical Karst (Kras) 总被引:1,自引:0,他引:1
Karst researchers of the Karst Research Institute ZRC SAZU are regularly consulted during the planning of Slovenia’s motorways
and invited to observe and monitor construction in the karst areas. More than 350 caves have been discovered in the course
of building 60 km of new motorways over the past decade. Access to the most important caves is preserved by concrete tubes
closed with metal covers at the roadside. The largest cave system in a tunnel, named LC-S647, is almost entirely preserved.
The protection of this cave will serve as a good example for the preservation of natural heritage in the future. Construction
work for the motorway uncovered a high degree of karstification. In particular, the discovery of this cave in the Kastelec
tunnel LC-S647 showed the existence of a major cave system in the geological and speleological past. A number of unconnected
passages have also been found. Caves discovered during highway construction have brought new knowledge about the cavernosity
and the geological history of this part of the karst. 相似文献
69.
Landslide susceptibility mapping for a landslide-prone area (Findikli,NE of Turkey) by likelihood-frequency ratio and weighted linear combination models 总被引:17,自引:0,他引:17
Landslides are very common natural problems in the Black Sea Region of Turkey due to the steep topography, improper use of
land cover and adverse climatic conditions for landslides. In the western part of region, many studies have been carried out
especially in the last decade for landslide susceptibility mapping using different evaluation methods such as deterministic
approach, landslide distribution, qualitative, statistical and distribution-free analyses. The purpose of this study is to
produce landslide susceptibility maps of a landslide-prone area (Findikli district, Rize) located at the eastern part of the
Black Sea Region of Turkey by likelihood frequency ratio (LRM) model and weighted linear combination (WLC) model and to compare
the results obtained. For this purpose, landslide inventory map of the area were prepared for the years of 1983 and 1995 by
detailed field surveys and aerial-photography studies. Slope angle, slope aspect, lithology, distance from drainage lines,
distance from roads and the land-cover of the study area are considered as the landslide-conditioning parameters. The differences
between the susceptibility maps derived by the LRM and the WLC models are relatively minor when broad-based classifications
are taken into account. However, the WLC map showed more details but the other map produced by LRM model produced weak results.
The reason for this result is considered to be the fact that the majority of pixels in the LRM map have high values than the
WLC-derived susceptibility map. In order to validate the two susceptibility maps, both of them were compared with the landslide
inventory map. Although the landslides do not exist in the very high susceptibility class of the both maps, 79% of the landslides
fall into the high and very high susceptibility zones of the WLC map while this is 49% for the LRM map. This shows that the
WLC model exhibited higher performance than the LRM model. 相似文献
70.
Greening as strategic development in industrial change - Why companies participate in eco-networks 总被引:1,自引:0,他引:1
Eckhard Störmer 《Geoforum》2008,39(1):32-47
Networking between companies and other regional key actors has grown into a widespread instrument for economic development since the 1990s. Participatory networks have formed the concept for many activities of Local Agenda 21. Simultaneously, economic geography has focused on network theories to explain innovation in and the economic success of regions.This article focuses on the reasons why individual actors participate in environmentally oriented information networks. The questions approached are: Does the concept of learning within networks influence a firm’s development? How do the participants interact with each other? What effects do the networks have on their environment (arenas)?The changing arenas of a firm are analysed with regard to environmental concerns. These changes need to be anticipated for reliable strategies. To gain information and knowledge about current behaviour and activities, the functions of networks as learning platforms are discussed. Drawing upon arguments from different network theories, the motivations of participating in a network are threefold: actor and firm oriented, network internal (inter-firm), and network external. From these, a generic target cube of network motivations and actions is set up.The concept is reviewed by examining 12 ‘regional environmental information-oriented corporation networks’ (RUN) in the Greater Munich Area. The empirical material reveals that this type of network does not provide a guarantee for significant improvements in a firm’s environmental behaviour. However, participants learn about best practices while pursuing explicit or implicit aims as to influence their arenas. 相似文献