药用滑石粉酸中可溶物测定方法考察

考察药用滑石粉酸中可溶物测定方法的重复性、耐用性 ,分析主要影响因素。比较酸溶物提取液滤过介质对测定结果差异的影响 ;采用重量法随机测定酸溶物含量和室间差异。两种滤过介质处理对测定结果没有显著差异 ;室间测定结果没有显著差异 ;30批样品平行测定结果的 RSD值范围为 0 %～ 18.2 %。酸中可溶物测定法存在重复性和耐用性不佳的问题 ,应相应调整酸中可溶物含量限度     

用于新生代定年的Ar-Ar法标准样品候选样品初测结果

Ar Ar法定年的特点是必须要有一套年龄从小到大的标准样。迄今用于新生代定年的国内标准样极少。为满足新生代矿物Ar Ar法定年的需要,初选了一个标准样候选者BT 1透长石。样品总重366g,粒级6080目,纯度100%,缩分为100瓶,每瓶3 66g。Ar Ar阶段加热法初测结果为:全部12个阶段给出的总气体年龄为30 8±0 9Ma,412阶段视年龄十分接近,年龄谱平坦,对应的39Ar析出量达96%,坪年龄为29 6±0 4Ma,等时年龄为29 6±0 6Ma,MSWD=1 01。40Ar/36Ar初始值为293 6±3 9,与尼尔值295 5相当。重复测定结果为:全部气体年龄为31 0±0 9Ma(全部9个阶段),坪年龄为29 5±0 4Ma,等时年龄为29 4±0 6Ma,MSWD=1 94,40Ar/36Ar初始值为282 2±6 3。这些结果表明,BT 1透长石不含过剩氩,作为新生代定年的Ar Ar法标准样品候选者是较为理想的。     

活树桩固坡对边坡稳定性影响的数值分析

作为一种经济、环保的植物固坡方法,活树桩在发达国家得到了较为广泛的应用.笔者介绍了活树桩固坡方法的应用和施工方法,讨论了其加固机理.采用弹塑性有限元分析活树桩固坡对边坡稳定性的影响,研究了活树桩的入土长度、加固位置、数量、角度及其根系发展等因素对边坡安全系数影响的规律.     

人工土层冻结法加固在盾构出洞施工中的应用

软土地区盾构出洞施工中洞口土体易失稳、渗水,上海明珠线二期工程浦东大道站至张扬路站区间,隧道在盾构出洞施工中,为确保地面建筑及地下管线的安全及正常使用,首次采用了人工土层冻结加固,取得了良好的效果;本文介绍了该工程出洞口土体加固的方案选择、关键技术处理及实际取得的效果,并探讨了人工土层冻结加固在含水松软土层的地下工程中的应用前景.     

应用MapGIS构建上海及邻近海域地震与新构造活动关系数据库

基于MapGIS构建上海及邻近海域地震和新构造活动数据库。该数据库由空间和属性两大数据库组成。其中，空间数据库包括地理底图库及地震、活动断裂、新生代盆地、岩浆岩分布多个专题图库；属性数据库主要针对专题图库而建立，有地震属性库、活动断裂属性库及新生代盆地属性库。通过图形数据结构和属性数据结构共有的标识码实现图形数据库和属性数据库之间的连接。为方便查询检索，对重要的属性数据如断裂走向、地震震级等以编码方式表示。该数据库的建立为定量研究和评价本区地震与新构造活动的关系，以及防震减灾提供了重要的科学依据。     

增量位移反分析在水电地下洞室工程中的应用

反分析是确定计算模型参数的有效方法.通常多采用量测所得全量位移进行反演计算.但地下工程中许多量测数据为增量位移,且实际施工过程可以通过建立分步开挖的有限元模型来模拟.据此,结合某水电站地下洞室工程中地下厂房的开挖,建立了模拟动态施工的有限元模型,利用某一开挖步施工前后量测值之差,采用增量位移优化反分析方法对洞室附近初始地应力场及围岩弹性模量进行了反演.计算所得增量位移与实测值符合较好,表明了这种方法的可行性.同时,根据分析结果对该方法进行了评价.     

Evaluating accuracy for two empirical methods in predicting settlement of drilled shafts

Several theoretical, empirical and semi-empirical methods are available in the literature to predict settlement of drilled shafts in sandy soils. In the Arabian Gulf countries, specifically in the United Arab Emirates, equations and procedure from the rest of the world are being used in analysis and design of drilled shafts without proper validation. It is the aim of this study to assess the applicability and evaluate the accuracy of two well known, and commonly used methods for pile prediction in the United Arab Emirates (UAE), namely Vesic (1977) and Poulos (1979), via comparison with data from field pile load tests conducted on shafts drilled in the region. Some of these tests were conducted for the purpose of this study, while others were made available through the courtesy of International Piling Contractors who are active in the region (e.g. Bauer International and Swiss Borings). Pile load test data were analyzed to back-calculate the model parameters related to settlement under different loading stages. Geological data and soil properties were obtained from studies conducted at the relevant sites. An effort is made to correlate soil properties with the prediction models. Statistical analysis is conducted to assess the accuracy of the results obtained from the two methods at different stages of loading via those obtained from pile load tests. Moreover, a detailed parametric study is conducted to assess the effect of the related parameters on the predicted pile settlement and the estimated settlement at different stages of loading. The study concluded with a recommendation of the most appropriate models and procedures to be followed for predicting the settlement of drilled shafts in the UAE, together with useful charts and correlation relations. Results showed that settlement values predicted by Vesic (1977) and Poulos (1979) overestimates the true values. This revised version was published online in July 2006 with corrections to the Cover Date.     

On the long-term seismic hazard analysis in the Zhangjiakou–Penglai seismotectonic zone, China

The Zhangjiakou–Penglai seismotectonic zone (ZPSZ) lies in the northern part of North China and extends along the Zhangjiakou–Beijing–Tianjin–Bohai Bay–Penglai–Yellow Sea. It is about 900 km long and some 250 km wide in a northwest direction. The great Sanhe-Pinggu (M_S=8.0) earthquake occurred on September 1679 and the Tangshan (M_S=7.8) earthquake on July 1976 caused serious economic and life losses. According to some differences in crust structure and regional tectonic stress field, the ZPSZ is divided into western and eastern segment by the 117°E line for study on long-term seismic hazard analysis. An analysis of Gutenberg–Richter's empirical relation of earthquake-frequency and time process of historic and recent earthquakes along the eastern and western segments shows that the earthquake activity obeys a Poisson process, and these calculations indicate that the earthquake occurrence probability of M_S=6.0–6.9 is 0.77–0.83 in the eastern segment and the earthquake occurrence probability of M_S=7.0–7.9 is 0.78–0.80 in the western segment of the ZPSZ during a period from 2005 to 2015.     

A time-space based approach for mapping rainfall-induced shallow landslide hazard

A rainfall-induced shallow landslide is a major hazard in mountainous terrain, but a time-space based approach is still an unsettled issue for mapping rainfall-induced shallow landslide hazards. Rain induces a rise of the groundwater level and an increase in pore water pressure that results in slope failures. In this study, an integrated infinite slope analysis model has been developed to evaluate the influence of infiltration on surficial stability of slopes by the limit equilibrium method. Based on this new integrated infinite slope analysis model, a time-space based approach has been implemented to map the distributed landslide hazard in a GIS (Geographic Information Systems) and to evaluate the shallow slope failure induced by a particular rainfall event that accounts for the rainfall intensity and duration. The case study results in a comprehensive time-space landslide hazard map that illustrates the change of the safety factor and the depth of the wetting front over time.     

The Significance of Multiple Saturation Points in the Context of Polybaric Near-fractional Melting

Experimental petrologists have successfully located basalticliquid compositions parental to mid-ocean ridge basalt thatare, within experimental resolution, multiply saturated withthree-phase harzburgite or four-phase lherzolite assemblageson their liquidus at some elevated pressure. Such an experimentalresult is a necessary consequence of any paradigm in which eruptedbasalts derive from single-batch primary liquids that equilibratewith a mantle residue and undergo no subsequent magma mixingbefore differentiation and eruption. Here we investigate whether,conversely, such evidence of multiple saturation is sufficientto exclude dynamic melting models wherein increments of meltare mixed after segregation from residues, during melt transportor in magma chambers. Using two independent models of crystal–liquidequilibria to simulate polybaric near-fractional peridotitemelting, we find that aggregate liquids from such melting processescan display near-intersections of liquidus surfaces too closeto distinguish experimentally from exact multiple saturationpoints. Given uncertainties in glass compositions, fractionationcorrections, experimental temperature and pressure conditions,and achievement of equilibrium, these results suggest that polybaricmixtures can in fact masquerade as mantle-equilibrated single-batchprimary liquids. Multiple saturation points on the liquidussurfaces of primitive basalts do, however, preserve informationabout the average pressure of extraction of their constituentincrements of liquid. KEY WORDS: mantle melting; basaltic volcanism; experimental igneous petrology; thermodynamic modelling; inverse method