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221.
222.
Youjuan Li Brian R. Jicha Wanfeng Zhang Wen Chen Brad S. Singer Dewen Zheng Huaiyu He 《Geostandards and Geoanalytical Research》2023,47(3):657-668
The precision and accuracy of 40Ar/39Ar dates are ultimately linked to co-irradiated reference materials of known age. Here we provide new data from the SK01 sanidine, which was analysed in three different laboratories to evaluate it as a 40Ar/39Ar reference material. Aliquots of 5 mg, incrementally heated in two laboratories, yielded indistinguishable results with a weighted mean age of 27.58 ± 0.06 Ma (95% confidence level). Single-crystal step heating and single-crystal total fusion analyses of SK01 sanidine were undertaken in the third laboratory to further test the intracrystalline homogeneity. For the seven step-heating analyses, six crystals yielded nearly concordant age spectra with 40Ar/39Ar ages ranging from 26.853 ± 0.094 Ma to 26.963 ± 0.067 Ma, whereas one crystal gave an older age of 27.774 ± 0.071 Ma with a slightly discordant age spectrum. Twenty-three single-crystal total fusion analyses yielded 40Ar/39Ar ages ranging from 27.070 ± 0.108 Ma to 27.736 ± 0.062 Ma with a dispersion of ~ 3.8%. The older ages from single-crystal total fusion dates are interpreted to reflect an inherited or excess argon component in some crystals. This is an initial characterisation of the SK01 sanidine, and additional work needs to be conducted to further evaluate the age dispersion so that it can be utilised as a 40Ar/39Ar reference material. 相似文献
223.
激光剥蚀电感耦合等离子体质谱元素微区分析标准物质研究进展 总被引:9,自引:5,他引:4
激光剥蚀电感耦合等离子体质谱(LA-ICP-MS)是目前地球科学分析领域的重要技术手段,元素微区分析标准物质研制是该分析技术发展的重要方向。本文对当前LA-ICP-MS元素微区分析标准物质的种类、元素分布以及应用上的优缺点和标准物质的制备方法进行了评述。现有的有证标准物质数量不多、种类不齐全,部分元素浓度较低,定值不确定度较大,应用上受到较大的局限性;研制标准也不成熟,均匀性检验方面尚未有统一的方法。本文参照岩石粉末标准物质均匀性检验方法提出了两步均匀性检验法,同时指出在标准物质种类方面,铂族元素及Au元素浓度适当、Pb-S等不同硫化物基体标准物质,以及化学成分不同的碳酸岩和磷酸岩基体标准物质是当前的迫切需求;在标准物质研制技术方面,纳米岩石粉末压片技术的研发、原位微区分析标准物质(固体)均匀性检验判别标准研究是亟待解决的问题。 相似文献
224.
针对WGS-84CGCS2000坐标基准差异问题,分析了用于估计基准转换参数的Bursa模型及其求解方法,初步尝试求取WGS-84CGCS2000的坐标基准转换参数。算例采用了中国区域内含有CGCS2000坐标值,同时安装有GPS接收机的21个观测站,并针对点位的区域分布问题,提出利用重心化的Bursa模型求解转换参数的思路,且得到一组较好的转换结果。 相似文献
225.
Mass Fractions of S,Cu, Se,Mo, Ag,Cd, In,Te, Ba,Sm, W,Tl and Bi in Geological Reference Materials and Selected Carbonaceous Chondrites Determined by Isotope Dilution ICP‐MS
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Zaicong Wang Harry Becker Frank Wombacher 《Geostandards and Geoanalytical Research》2015,39(2):185-208
Mass fractions of S, Cu, Se, Mo, Ag, Cd, In, Te, Ba, Sm, W and Tl were determined by isotope dilution sector field ICP‐MS in the same sample aliquot of reference materials using HF‐HNO3 digestion in PFA beakers in pressure bombs and glassy carbon vessels in a high‐pressure asher (HPA‐S) for comparison. Additionally, Bi was determined by internal standardisation relative to Tl. Because isobaric and oxide interferences pose problems for many of these elements, efficient chromatographic separation methods in combination with an Aridus desolvator were employed to minimise interference effects. Repeated digestion and measurement of geological reference materials (BHVO‐1, BHVO‐2, SCo‐1, MAG‐1, MRG‐1 and UB‐N) gave results with < 5% relative intermediate precision (1s) for most elements, except Bi. Replicates of NIST SRM 612 glass digested on a hot plate were analysed by the same methods, and the results agree with reference values mostly within 2% relative deviation. Data for the carbonaceous chondrites Allende, Murchison, Orgueil and Ivuna are also reported. Digestion in a HPA‐S was as efficient as in pressure bombs, but some elements displayed higher blank levels following HPA‐S treatment. Pressure bomb digestion yielded precise data for volatile S, Se and Te, but may result in high blanks for W. 相似文献
226.
极端气温和极端降水复合事件的气候特征 总被引:1,自引:0,他引:1
基于1961-2014年的中国台站资料,侧重探讨极端气温和极端降水复合事件的气候特征。结果表明,基于客观方法检测出四类极端复合事件:暖湿、暖干、冷湿和冷干。四类事件的频发区分别位于东北地区、华南地区、西藏及华南地区和长江以南及云贵高原一带。全国暖湿、暖干事件频数呈增加趋势,春夏季频发;冷湿事件频数在西藏东北一带呈增加趋势,而在长江流域呈减少趋势,夏秋冬季频发;冷干事件频数呈减少趋势,秋冬季频发。四类极端复合事件经验正交分解的时间序列主模态均表现为年代际信号。进一步分析四类复合事件与能源消费量的联系表明,极端湿事件与能源消费量呈正相关,而极端干事件则相反。 相似文献
227.
城市化对人类生活息息相关的一些指标(如夏季极端暖夜等)的影响研究尚少.取环渤海地区气象观测站的夏季(6-8月)逐日最低气温资料(1958-2009年),使用广义极值(GEV)分布拟合夏季极端暖夜气温分布,并对拟合函数的3个分布特征参数的年际变化进行分析,根据特征参数变化特征进行城市化对极端暖夜的影响程度的分离.研究结果表明,环渤海地区,在极端暖夜气温分布的3个参数的年际变化中,以位置参数的代表性最好.在城市快速发展时期,城市偏高气温出现的可能性大,但极端气温变化幅度也较大.城市化对环渤海不同类型城市夏季极端暖夜气温的贡献均为上升作用,增温速度最大约为0.3℃/(10a). 相似文献
228.
Effects of Urbanization on Extreme Warmest Night Temperatures During Summer near Bohai 总被引:1,自引:0,他引:1
Many previous studies have focused on the impacts of urbanization on regional mean temperatures. Relatively few have analyzed changes in extreme temperatures. Here, we examine the impact of urbanization on extreme warmest night temperatures from 33 stations in the Bohai area between 1958 and 2009. We compute the Generalized Extreme Value(GEV) distribution of extreme warmest night temperatures and analyze long-term variations in its characteristic parameters. A new classification method based on the factor analysis of changes in extreme night temperatures is developed to detect the efects of urbanization in diferent cities. Of the three parameters that characterize the GEV distribution, the position parameter is the most representative of long-term changes in extreme warmest night temperatures. During the period of rapid urbanization(i.e., after 1978), all three parameters of the GEV distribution are larger for the urban station group than for the reference station group, so are the magnitudes of their variations, and the urban areas have been experiencing higher extreme warmest night temperatures with larger variability. Diferent types of cities in the Bohai area have all experienced an urban heat island efect, with an average urbanization efect of approximately 0.3 per decade. 相似文献
229.
利用乌兰乌苏镇1964~2012年的气象资料,选取逐年平均气温、极端最高气温、极端最低气温、大风、雷暴、沙尘暴、沙尘天气及大雾、轻雾天气出现的天数作为分析对象,运用3年移动平均法、回归分析法、非参数检验方法的Mann-Kendall趋势检验和突变检验法以及小波分析法,进行了多种天气事件的年纪变化趋势分析.结果表明:(1)大雾天气的发生日数呈增加趋势,沙尘天气、沙尘暴天气、轻雾天气、大风天气和雷暴天气的发生日数都呈减少趋势,其中大风天气发生日数减少趋势最为明显.(2)平均气温、年极端最高气温、年极端最低气温、大雾天气、轻雾天气、沙尘暴天气、雷暴天气和沙尘天气在研究时段都出现了突变,且平均气温、轻雾天气、沙尘天气和雷暴天气在突变之后不久都达到了极显著的上升或者下降变化趋势.(3)平均气温、年极端最低气温、年极端最高气温、大雾天气、雷暴天气和大风天气有明显的周期性,但是不同的气象要素周期性长短是不同的,沙尘、沙尘暴和轻雾天气则没有明显的周期性. 相似文献
230.
Connecting atmospheric science and atmospheric models for aerocapture at Titan and the outer planets
Many atmospheric measurement systems, such as the sounding instruments on Voyager, gather atmospheric information in the form of temperature versus pressure level. In these terms, there is considerable consistency among the mean atmospheric profiles of the outer planets Jupiter through Neptune, including Titan. On a given planet or on Titan, the range of variability of temperature versus pressure level due to seasonal, latitudinal, and diurnal variations is also not large. However, many engineering needs for atmospheric models relate not to temperature versus pressure level but atmospheric density versus geometric altitude. This need is especially true for design and analysis of aerocapture systems. Drag force available for aerocapture is directly proportional to atmospheric density. Available aerocapture “corridor width” (allowable range of atmospheric entry angle) also depends on height rate of change of atmospheric density, as characterized by density scale height. Characteristics of hydrostatics and the gas law equation mean that relatively small systematic differences in temperature versus pressure profiles can integrate at high altitudes to very large differences in density versus altitude profiles. Thus, a given periapsis density required to accomplish successful aerocapture can occur at substantially different altitudes (∼150-300 km) on the various outer planets, and significantly different density scale heights (∼20-50 km) can occur at these periapsis altitudes. This paper will illustrate these effects and discuss implications for improvements in atmospheric measurements to yield significant impact on design of aerocapture systems for future missions to Titan and the outer planets. Relatively small-scale atmospheric perturbations, such as gravity waves, tides, and other atmospheric variations can also have significant effect on design details for aerocapture guidance and control systems. This paper will discuss benefits that would result from improved understanding of Titan and outer planetary atmospheric perturbation characteristics. Details of recent engineering-level atmospheric models for Titan and Neptune will be presented, and effects of present and future levels of atmospheric uncertainty and variability characteristics will be examined. 相似文献