反相流动注射催化光度法测定废水中的亚硝酸根

采用反相流动注射技术与催化光度法相结合，用微机化流动注射分析仪准确控制反应时间，优化了实验条件，克服了催化光度法反应时间难以控制引起的方法精密度、准确度不高的弱点，拟定了测定痕量亚硝酸根的流动注射催化光度方法。分析速度第小时20次，NO2^- 质量浓度在0．00－2．00mg/L，回归方程斜率为0．155。方法直接测定电厂测水中NO2^-的结果与Griess法相符合，RSD＜5．0％（n=5）。     

Determination of structures of Ca2CoSi2O7, Ca2MgSi2O7, and Ca2(Mg0.55Fe0.45)Si2O7 in incommensurate and normal phases and observation of diffuse streaks at high temperature

 The structures of Ca₂CoSi₂O₇, Ca₂MgSi₂O₇, and Ca₂(Mg_0.55Fe_0.45)Si₂O₇ have been determined in the temperature range between 297 and 773 K with arbitrary intervals. The structures of the incommensurate phase of the three compounds are characterized by the presence of the six-, seven-, and eight-coordinated Ca–O polyhedra and of the bundles along the c-axes consisting of four arrays of the six-coordinated Ca–O polyhedra and an array of T¹O₄ (T¹: Co, Mg, or Mg–Fe) tetrahedra in the structures. The number of bundles in each material decreases at elevated temperatures. The incommensurate phase undergoes a phase transition into the normal phase at 493 K in Ca₂CoSi₂O₇, at 360 K in Ca₂MgSi₂O₇, and at 510 K in Ca₂(Mg_0.55Fe_0.45)Si₂O₇. The features of the structures of the normal phase are almost the same as those found in the basic structures (the averaged structures of the incommensurate structures), and this fact implies that the characteristics of the structures, such as the six-coordinated Ca–O polyhedra or fragments of the bundles, should be partially preserved at higher temperatures both in the incommensurate structures and also in the structures of the normal phase. Analyses of anisotropic displacement parameters clarified that disorder of the modulation waves is developed in the structures at higher temperatures. The evolution of a disorder in the structures was ascertained by observation of the circular diffuse streaks in the vicinity of the transition temperature between the incommensurate and normal phases. Received: 3 July 2000 / Accepted: 26 October 2000     

“科钻一井”一开泥浆技术

“科钻一井”一开井段采用了钠膨润土-高粘CMC泥浆体系，视漏失情况添加GD-Ⅲ随钻堵漏剂，满足了施工携带岩屑和堵漏防漏要求。介绍了该井一开井段的泥浆技术，并对泥浆成本进行了分析。     

山东省干旱演变规律及其影响

利用近５００年旱涝资料分析了干旱对山东省农业，工业及环境的危害。利用功率谱和模糊判别函数研究了旱涝的周期性和阶段性，指出旱涝的演变规律可为气候预测提供依据。     

Introduction to an Invariant Quantity Method

ＩｎｔｒｏｄｕｃｔｉｏｎｔｏａｎＩｎｖａｒｉａｎｔＱｕａｎｔｉｔｙＭｅｔｈｏｄＬｉｕＧｕｉｆｕ（刘桂复）（ＮａｍｉｎｇＩｎｓｔｉｔｕｔｅｏｆＭｅｔｅｏｒｏｌｏｇｙ，Ｎａｍｉｎｇ２１００４４ＲｅｃｅｉｖｅｄＭａｒｃｈ１１．１９９５，ｒｅｖｉｓｅｄＪｕｎ...     

ALow-order Model of Two-dimensional Fluid Dynamics on the Surface of a Sphere

ＡＬｏｗ－ｏｒｄｅｒＭｏｄｅｌｏｆＴｗｏ－ｄｉｍｅｎｓｉｏｎａｌＦｌｕｉｄＤｙｎａｍｉｃｓｏｎｔｈｅＳｕｒｆａｃｅｏｆａＳｐｈｅｒｅＭｏｚｈｅｎｇＷｅｉ（ＣＲＣｆｏｒＳｏｕｔｈｅｒｎＨｅｍｉｓｐｈｅｒｅＭｅｔｅｏｒｏｌｏｇｙ，ＣＳＩＲＯＤｉｖｉｓｉｏ...     

Amplitude Ratio of Regional Seismic Phases: An Efficient Indicator of Thermal State of the Lithosphere

By analyzing seismograms of short period records at the Beijing SeismoJogicaJ Observatory, the present paper investigates the amplitude ratio of seismic phases. The results indicate that the amplitude ratio of Sn/Lg is correlated with the lithosphere structure, the thermal state, and strong earthquake occurrence in the region the seismic rays pass through. The significance of such a correlation in the study on the genesis and prediction of strong earthquakes is discussed.     

Inversion of Q value structure beneath the Tibet Plateau

A total of 11 earthquakes with 15 Rayleigh wave paths, recorded at 11 broadband digital PASSCAL seismometers installed in the Tibet Plateau by the Sino-U.S. joint research group, were used to determine the phase velocity and attenuation coefficient of surface waves in periods of 10–130 s. The average shear wave velocity and quality factor {ie271-1} structures in the crust and upper mantle were obtained in this region. The result shows the average {ie271-2} is low and there exists a high attenuation ({ie271-3}=93–141) layer in the crust. The depth range of the low {ie271-4} value layer (16–42 km) is consistent with the range of low velocity layer (21–51 km) in the crust. Below 63 km in the lower crust, {ie271-5} decreases with depth from 114 to 34 at depth of 180 km. The low shear wave velocity and low value of {ie271-6} at the same depth range in the crust indicate that the rocks in the range is probably melted or partially melted. According to the shear wave velocity structure, the average thickness of the crust is about 71 km and a clear velocity discontiniuty appears at the depth of 51 km. The low-velocity zone (4. 26 km/s) at depth of 96–180 km may be corresponding to the asthenosphere. Contribution No. 96A0047, Institute of Geophysics, SSB, China. This study was supported by the National Natural Science Foundation of China.     

Study on the characteristics of crust－mantle transition zone in Western Yunnan Province

Ｓｔｕｄｙｏｎｔｈｅｃｈａｒａｃｔｅｒｉｓｔｉｃｓｏｆｃｒｕｓｔ┐ｍａｎｔｌｅｔｒａｎｓｉｔｉｏｎｚｏｎｅｉｎＷｅｓｔｅｒｎＹｕｎｎａｎＰｒｏｖｉｎｃｅＨＯＮＧ－ＸＩＡＮＧＨＵ（胡鸿翔）ＺＨＯＮＧ－ＹＡＮＧＬＩＮ（林中洋）ＹＩＮ－ＪＵＢＩＡＮ（边银...     

1996年上半年世界地震灾害综述

１９９６年上半年全世界共发生６级以上地震５８次，其中７级以上地震１０次，成灾的地震１０次，死亡人数总５１０人，伤约１．５万人，经济损失为８３亿－１００亿元人民币。其中我国境内灾害地震３次，死亡人数共计３４９人，伤约１．４５万人，经济损失约７８亿元人民币。我国因地震死亡的总人数约占全世界地震