岩石矿物及粉尘中游离二氧化硅的测定

改进了游离二氧化硅（fSiO2)测定中试样的分解方法，采用硫－磷混酸替代单独使用磷酸分解试样，防止了焦磷酸盐的形成，同时，氟硼酸对fSiO2的溶解率符合测定要求。改进的方法用于标准物质中fSiO2的测定，结果与标准值或磷酸溶矿重量法相符。对于ω(fSiO2)=3.26%的标样10次测定的RSD为2．4％。     

2—（2，3，5—三氮唑偶氮）—1，8—二羟基—3，6—萘二磺酸与钴的显色反应及应用

介绍了新水溶性显色剂 2 - ( 2 ,3,5 -三氮唑偶氮 ) - 1 ,8-二羟基 - 3,6-萘二磺酸与钴的显色反应及应用 ,建立了测定钴的新方法。在 pH 9.9的Na2 B4O7 NaOH缓冲液中该试剂与钴形成 1∶1蓝色稳定络合物 ,λmax为 5 88.8nm ,Co的质量浓度在 0～ 1 .0mg/L内符合比尔定律 ,表观摩尔吸光系数为 3.46× 1 0 4 L·mol- 1 ·cm- 1 。所拟方法用于环境水样及维生素B1 2 注射液中的微量钴测定 ,结果与原子吸收法相符 ,5次测定的RSD <1 %。     

华北地区震群活动的阶段性特征

通过对华北地区1970年以来震群活动的分析表明，唐山地震的震群活动显示出一定的迁移性和阶段性。应用流变介质包体孕震模型的理论进行了初步力学分析。张北地震的预测检验表明，震群活动的迁移性与阶段性对强震的中期预测具有一定指导意义。     

张北Ms6.2地震前重力异常及异常机制探讨

根据晋北和辽西地区地质构造背景及力学机制，分析了1998年张北Ms6.2地震前后出现在震中外围地区的重力异常变化，对沿深部断裂附近出现的重力异常进行了分析讨论，认为沿深部断裂出现的重力异常可作为地震前兆场的信息。     

1998年张北6.2级地震宏观烈度

充分利用震害评估和宏观考察的资料 ,采用震害程度和震害指数 2个标准共同确定了1 998年张北 6.2级地震的宏观烈度。极震区烈度为 度 ,呈 NWW和 NNE双向分布 ,以NWW为主 ,面积 1 35km2 。 度区呈 NE、NW双向伸展图象 ,但是 SE方向伸展不足 ,面积约340 km2。地震重伤人员普遍集中在 度区和 度区。 度区亦呈 NE、NW双向伸展图象 ,但是 NW、SW方向延伸长 , 度区面积约 1 0 0 0 km2 。宏观震中 :北纬 41°0 9′,东经 1 1 4°2 7′。在极震区的 NNE、SSW和 NWW方向 ,存在 3个烈度异常区 ,它们分别在极震区 3个分支的延伸方向上。文中讨论了烈度不高而震后较重的原因。震区没有发现地表破裂带 ,也没有发现第四纪强烈活动的大型断裂。极震区为主的 NWW方向和震前存在的小地震条带吻合 ,暗示可能存在成因上的联系     

张北6.2级地震地裂缝特征及其研究意义

张北6．2级地震现场调查结果表明，这次地震形成了大量的非构地裂缝,它们主要分布在极震区和Ⅶ度区。地裂缝的优势方位为NNE和NWW向，与Ⅶ度等震线双向展布基本一致。利用地裂缝的空间分布特征和统计的优势方位，探讨了地裂缝与烈度分区和发震构造的关系。     

Self‐purification in Upland and Lowland Streams

Ecological investigations at four streams in Saxony‐Anhalt have shown that there are considerable differences between the self‐purification power of upland and lowland streams. This result is reflected in chemistry and in microbiology. The structure of the bottom substrate mainly influences the degree of self‐purification in connection with rate of flow and flow velocity. The results and differences are demonstrated using the example of Katzsohlbach in the landscape unit “Mittel‐ and Unterharz” and the stream Olbe in the landscape unit “Magdeburger Börde”.     

Oxidation Experiment of Natural Megacrystal Clinopyroxene: Implications for Assignment of Mössbauer Spectra

The Mössbauer spectra of natural megacrystal clinopyroxene are usually fitted by 4 sets of symmetric doublets, A‐A', B‐B', C‐C' and D‐D', respectively, in terms of increasing Qs value in literature. But the assignments of those doublets are quite different, except the D‐D' doublet assigned to Fe³⁺at the lattice site M***1 in previous papers. Particularly, the assignment and interpretation of the C‐C' doublet are diverse. The oxidation experiments of natural megacrystal clinopyroxene collected from the Hannuoba basalt, North China, were performed under controlled conditions of temperature at 1000°C and oxygen fugacity of FMQ buffer in 1, 2, ***3 and 5 days respectively. The oxidized samples were then measured by X‐ray diffraction spectrometry and Mössbauer spectrometry. The oxidation of clinopyroxene is characterized by Fe²⁺ → Fe³⁺at M1 under the subsolidus conditions, which is consistent with the increase of the area of the D‐D' doublet when the heating time increases. Accordingly, the area of the A‐A' and B‐B' doublets decreases with the increasing heating time. However, the area of C‐C' keeps almost constant. Therefore, the 4 sets of doublets can be assigned correctly as follows: A‐A' doublet to Fe⁺²at M1, B‐B' Fe²⁺at M1, C‐C' Fe²⁺at M2, and D‐D' Fe³⁺at M1. The M1 site splitting is due to the NNN (Next Nearest Neighbour) effect of the M2 site. The amount of Fe³⁺at the tetrohedral site of megacrystal clinopyroxene is negligible according to this study.     

The use of sintered diamond anvils in the MA8 type high-pressure apparatus

A new multi-anvil type high-presure apparatus has been developed using sintered diamond anvils to generate pressures over 30 GPa and temperatures up to about 2000°C. A maximum sample volume of about 1 mm³ is available in this system. The pressure was confirmed by dissociation of forsterite into Mg-perovskite and periclase. The basic techniques and problems in utilizing sintered diamond in the MA8 type high-pressure apparatus are discussed with an emphasis on the future prospect of incorporating simultancous X-ray diffraction observation.     

利用IRS-P6卫星数据制作遥感影像地图

本文介绍了以IRS-P6卫星数据作为信息源完成大兴安岭林区的遥感影像地图制作的方法, 通过试验初步认识到:利用IRS-P6卫星数据制作遥感影像地图,可以满足1:50000、 1:25000比例尺的平面制图精度要求,在一些专业和专题应用中可以放大到1:15000比例尺使用。