阿尔泰南缘麦兹盆地萨吾斯铅锌矿床控矿铁闪石矽卡岩的40Ar/39Ar年代学研究

萨吾斯矿床位于麦兹盆地东部,是一个新近发现和勘探的铅锌矿床。萨吾斯铅锌矿床赋存于下泥盆统康布铁堡组上亚组凝灰岩、流纹岩及其沉积碳酸盐夹层,矿（化）体直接受石榴黑云矽卡岩和铁闪石矽卡岩控制,表现出火山喷流-沉积成矿和矽卡岩矿床的双重特征。这两类矿床的重要区别之一是同生和后生成矿。对主要矽卡岩矿物铁闪石进行精确的Ar-Ar年龄测定,将其与康布铁堡组流纹岩的年龄对比,有助于确定萨吾斯铅锌矿床的成因。高精度、高灵敏度激光⁴⁰Ar-³⁹Ar测年方法,为解决闪石类低K矿物的定年提供了新的手段。岩芯样品SW85中,铁闪石晶粒较大、晶形发育,与闪锌矿、碳酸盐矿物和石榴子石都具有平直的边界,而不是复杂交生,不含矿物和流体包裹体,代表了相对简单均一的系统。对SW85的铁闪石做了激光⁴⁰Ar-³⁹Ar测年,其结果为412±15Ma,与康布铁堡组流纹岩的SIMS锆石U-Pb年龄（401±2.7Ma）和别斯萨拉玢岩的SIMS锆石U-Pb年龄（401±3.1Ma）在误差范围内一致,表明矽卡岩和铅锌矿的形成与康布铁堡组流纹质火山岩的喷发及其碎屑岩的沉积是同时的,成因上密切相关。其次,矽卡岩呈层状产出,局限于康布铁堡组凝灰岩及其铁锰钙质碳酸盐夹层的范围内;石榴子石为铁铝榴石、锰铝榴石,闪石为铁闪石,缺失透辉石、钙铁辉石。上述特征与接触交代矽卡岩不同,后者以钙铝榴石、钙铁榴石、透辉石/钙铁辉石为特征,闪石为角闪石。接触交代矽卡岩矿床是后成矿床,它晚于岩浆侵入体的围岩。综上所述,萨吾斯铅锌矿是一个与康布铁堡组火山喷发和浅成侵入有关的喷流-沉积矿床。麦兹盆地的控盆断裂巴寨断裂从北西端向南东发展而成。阿巴宫-库尔提断裂和琼库尔断裂是克兰盆地的控盆断裂,它们在北西撒开、向南东收敛,具有羽状张剪性断裂的特征。因此,阿尔泰南缘在早泥盆世具有活动陆缘的局部拉张性质。西伯利亚板块与哈萨克斯坦-准噶尔板块的推错,在阿尔泰南缘产生局部张剪性应力场,从而形成了上述断裂以及早泥盆世火山-沉积盆地。     

Sulfur isotope measurement of sulfate and sulfide by high-resolution MC-ICP-MS

We have developed a technique for the accurate and precise determination of ³⁴S/³²S isotope ratios (δ³⁴S) in sulfur-bearing minerals using solution and laser ablation multiple-collector inductively coupled plasma mass spectrometry (MC-ICP-MS). We have examined and determined rigorous corrections for analytical difficulties such as instrumental mass bias, unresolved isobaric interferences, blanks, and laser ablation- and matrix-induced isotopic fractionation. Use of high resolution sector-field mass spectrometry removes major isobaric interferences from O₂⁺. Standard-sample bracketing is used to correct for the instrumental mass bias of unknown samples. Background on sulfur masses arising from memory effects and residual oxygen-tailing are typically minor (< 0.2‰, within analytical error), and are mathematically removed by on-peak zero subtraction and by bracketing of samples with standards determined at the same signal intensity (within 20%). Matrix effects are significant (up to 0.7‰) for matrix compositions relevant to many natural sulfur-bearing minerals. For solution analysis, sulfur isotope compositions are best determined using purified (matrix-clean) sulfur standards and sample solutions using the chemical purification protocol we present. For in situ analysis, where the complex matrix cannot be removed prior to analysis, appropriately matrix-matching standards and samples removes matrix artifacts and yields sulfur isotope ratios consistent with conventional techniques using matrix-clean analytes. Our method enables solid samples to be calibrated against aqueous standards; a consideration that is important when certified, isotopically-homogeneous and appropriately matrix-matched solid standards do not exist. Further, bulk and in situ analyses can be performed interchangeably in a single analytical session because the instrumental setup is identical for both. We validated the robustness of our analytical method through multiple isotope analyses of a range of reference materials and have compared these with isotope ratios determined using independent techniques. Long-term reproducibility of S isotope compositions is typically 0.20‰ and 0.45‰ (2σ) for solution and laser analysis, respectively. Our method affords the opportunity to make accurate and relatively precise S isotope measurement for a wide range of sulfur-bearing materials, and is particularly appropriate for geologic samples with complex matrix and for which high-resolution in situ analysis is critical.     

GPS卫星的激光测距和应用研究

简述了SLR和GPS跟踪技术的发展概况。详细介绍了近几年来对GPS－35、36卫星的激光测距进展和应用研究的情况。给出了残差分析的初步结果,并指出了目前GPS卫星的稀少的激光测距资料对卫星精密定轨和站坐标的解算是有价值的。同时,也简单地评述了GPS卫星的微波和激光跟踪技术各自的优势和弱点．建议联合利用GPS-35、36卫星的SLR和GPS观测资料来开展有关的应用研究。最后,对今后的应用研究工作提出了建议．     

The International Laser Ranging Service and its support for IGGOS

The International Laser Ranging Service (ILRS) was established in September 1998 as a service within the IAG to support programs in geodetic, geophysical, and lunar research activities and to provide data products to the International Earth Rotation Service (IERS) in support of its prime objectives. Now in operation for 5 years, the ILRS develops: (1) the standards and specifications necessary for product consistency and (2) the priorities and tracking strategies required to maximize network efficiency. The service collects, merges, analyzes, archives and distributes satellite and lunar laser ranging data to satisfy a variety of scientific, engineering, and operational needs and encourages the application of new technologies to enhance the quality, quantity, and cost effectiveness of its data products. The ILRS works with: (1) the global network to improve station performance; (2) new satellite missions in the design and building of retroreflector targets to maximize data quality and quantity and (3) science programs to optimize scientific data yield. The ILRS Central Bureau maintains a comprehensive web site as the primary vehicle for the distribution of information within the ILRS community. The site, which can be accessed at: http://ilrs.gsfc.nasa.gov is also available at mirrored sites at the Communications Research Laboratory (CRL) in Tokyo and the European Data Center (EDC) in Munich.During the last 2 years, the ILRS has addressed very important challenges: (1) data from the field stations are now submitted hourly and made available immediately through the data centers for access by the user community; (2) tracking on low satellites has been significantly improved through the sub-daily issue of predictions, drag functions, and the real-time exchange of time biases; (3) analysis products are now submitted in SINEX format for compatibility with the other space geodesy techniques; (4) the Analysis Working Group is heavily engaged in Pilot Projects as it works toward an ILRS “standard” global solution and (5) SLR has significantly increased its participation in the International Terrestrial Reference Frame (ITRF) activity, which is important to the success of IGGOS.     

准噶尔盆地周边硅质岩激光40Ar/39Ar法定年

由于较低的钾元素含量以及过剩氩的存在,长期以来对硅质岩的40Ar/39Ar定年一直存在较大难度。近年来,由于仪器水平的不断提高,新实验技术和方法的应用,特别是激光全熔40Ar/39Ar定年技术的应用,40Ar/39Ar定年方法具有了足够高的测试精度和稳定的低本底水平,可以满足测试极低钾元素含量的硅质岩样品的要求。利用多组矿物颗粒测试数据计算等时线年龄的方法可以很好地去除过剩氩对硅质岩年龄的影响。本文利用激光全熔40Ar/39Ar定年方法对新疆准噶尔盆地边缘的两个硅质岩样品进行了定年研究。采自白碱滩地区的08BJT-3样品的年龄测试结果为294±14Ma,该年龄结果与硅质岩样品所处的晚石炭世地层沉积年代基本一致。采自卡拉麦里地区的KML-2样品的年龄测试结果为266±14Ma,该年龄结果与强烈变形改造硅质岩样品的卡拉麦里构造变形带活动年代十分一致,表明激光全熔40Ar/39Ar定年方法可以准确地对硅质岩进行定年。     

基于多种探测资料对武汉一次短时暴雪天气的监测分析

利用Thies Clima激光雨滴谱仪、MP3000A微波辐射仪、多普勒雷达和人工加密观测资料,分析了2011年2月12日武汉一次暴雪天气过程的演变特征。结果表明:(1)在这次短时暴雪过程中,先后出现了降雨、雨夹雪和纯降雪3个阶段,激光雨滴谱仪监测到该降雨阶段的雨滴谱较宽,最大直径达4.5mm,数浓度比较小,为2～5 429个.m-3.mm-1,雨滴谱型呈双峰型分布特点;(2)微波辐射仪对水汽相态监测显示,08:12-09:34(世界时)期间在1.5～3.5km过冷层比湿维持14～16g.kg-1大值区,之后迅速由雨夹雪过程(仅16min)过渡到纯降雪阶段,在65min内武汉站降雪量达到5.035mm,占整个降雪量的80%以上;(3)雷达反射率因子与粒子谱宽和数浓度密切相关,若后两者越大则对应的雷达回波强度也越大;同时还发现,与微波辐射仪反演的水汽密度、激光雨滴谱仪测得的降水强度也有较好的对应关系,若将这些结合起来对降水的相态变化、强度、量级和持续时间有很好的监测能力。     

三维激光扫描在建设工程竣工规划核实中的应用研究

本文介绍了建设工程竣工规划核实的主要方式,阐述了测量在竣工规划核实中的重要性,及目前核实方式中存在的问题.然后,针对三维激光扫描的技术原理,分析了三维激光扫描技术在竣工规划核实中应用的可行性,并通过对控制点布设、点云配准、建筑物特征点提取等技术方法的研究,实现了三维激光扫描在竣工规划核实中的应用,具有一定理论意义和实用价值.     

渤海湾西北部潮间带沉积物激光法与筛析沉降法结果的比较

对渤海湾西北部潮间带16个样品分别进行了激光法与综合法(筛析沉降法)粒度测量.两种方法所获结果的相关分析表明,激光法测得的>63μm的砂的百分含量平均仅比综合法低5%,相关系数高达0.9,相关性显著.两种方法测得的粉砂和粘土含量相关系数分别为0.39和0.48.进一步将<63μm部分分为6个粒级对比两种方法的异同,结果显示<1μm、1~2μm、2~4μm、4~8μm、8~16μm和16~63μm部分的相关系数分别为0.24、0.7、0.7、0.61、0.61和0.37.据此认为,16个样品粒径<1μm和16~63μm部分两种方法的结果不能对比,其余粒级的激光法结果,通过各自的回归方程,可谨慎地代替传统的综合法.     

GRACE和SLR观测的地球动力学扁率最大熵谱及小波相关分析

卫星重力测量技术的实现为测定地球动力学扁率提供了新的方式和途径,GRACE卫星是目前最新的重力测量卫星,据其恢复的低阶重力场较以往精度得到大大提高,然而其观测地球动力学扁率（二阶项）却与卫星激光测距（SLR）结果相差较大.本文采用最大熵谱和小波分析方法对GRACE和SLR观测的地球动力学扁率时间序列信号进行定量比较分析,结果表明：GRACE观测的地球动力学扁率年际周期变化振幅仅为SLR观测结果的25%,并且目前GRACE观测的地球动力学扁率数据中含有系统输入信息和相位差,但前者较后者包含有较强的短周期（2～6月）信息.造成这种差异的主要原因可能来自于GRACE与SLR全球观测数据时空分布不同.