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331.
本文采用了流动注射分析技术,用氢化物发生原子吸收分光光度法直接连续测定砷、锑、铋。在稀盐酸介质中,试样溶液中以不同氧化态存在的待测元素被硫脲、碘化钾、抗坏血酸混合还原抑制剂溶液在线还原为易生成氢化物的形式,与硼氢化钠反应生成氢化物,经我们自制的带雾化器的气液分离器分离后进入原子化器。方法稳定灵敏,再现性好,一次溶样可直接连续测定地质样品中砷、锑、铋3种元素。用本方法测定地质标样结果吻合很好,其检出限(3σ)分别为8.84,6.91,12.29×10 ̄(-8)g/L。相对标准偏差小于2%。 相似文献
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本文描述了原子吸收数据采集系统。由单片机控制的数据通过RS-232接口传送给微机进行数据处理。最后由微机打印出被测样品的测量结果。 相似文献
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J. Laštovička 《Pure and Applied Geophysics》1982,120(4):607-614
Nitric oxide concentration in the upper D-region is estimated by comparing empirically derived ratios of Lyman- and X-ray contributions to the total radio-wave absorption (2775 kHz. A3 method) in medium latitudes with model ratios. Typical NO concentrations are about 8.5×1013 m–3, at 90 km and 6.5×1013 m–3 at 78 km. These values are higher than generally accepted model NO concentrations, but lie within the broad range of experimental values. 相似文献
337.
André Girard Jean Besson Renée Giraudet Louis Gramont 《Pure and Applied Geophysics》1978,117(3):381-394
Summary Spectrometric experiments performed, in November 1976, within the framework of the Latitude Survey Mission on board the NASA Convair 990 from Ames Research Center are briefly deseribed. The results presented concern odd nitrogen molecules, HCl and water vapor. In terms of vertical column density, HNO3 is predominant over NO+NO2 at all latitudes higher than 40 degrees. A seasonal variation of NO2 abundance is observed, with larger values in the summer hemisphere at high latitude. The mean zenith column density of HCl above 11 km is 1.5×1015 mol.cm–2, with no evidence for any seasonal or climatic variation. Local number densities as high as 1.4×1010 mol.cm–3 for HNO3 and 5.4×1014 mol.cm–3 for water vapor have been measured during the same flight near 11 km. 相似文献
338.
ZhangZhenfei HuGuangdao YangMingguo LiuXing WangZhenlmi LiWenhui ZhangXiaobing HeLi 《中国地质大学学报(英文版)》2003,14(3):257-260
Field data of outcrop spectrums provide important basis for modeling of hyper-spectral remote sensing aiming at mineral prospecting. We make an approach to the application of rough set theory in spectral discriminiation of rocks. We build a decision table with an adequate number of samples (out-crops) of known rock type (the universe), of which the conditional atributes are discretized “area spectrum absorption indexes“ (ASAI) corresponding to wavelength intervals, and the decision atribute is rock type. We search to obtain the exhaustive set of reducts of the table, each of which will serve as a variable number of deduction rules. Suppose we have n (usually a very big number) rules in total and there are m types of rocks in our universe, for any unknown sample, we judge its rock type by each of those rules. An unknown sample may be recognized as a different type by different rules because it is out-side our universe, and we accept the most frequent judgment result and ignore the other m-1 types of results. Our ASAI is an improvement upon the traditional spectrum absorption index (SAI), better applicable to field spectrums: given a spectrum curve and a wavelength interval, we take the average reflectance within the interval as a base line and let ASAI=αbelow/(αabove αbelow), where αbelow and αabove stand for total areas, bounded by the curve, the base line and the borders of the intervalbelow and above the base line respectively. With the equipments of FieldSpectr Fr (made by ASD Co., US), we collected data from Baiya gold deposit, Yunnan, and applied the above method to discriminate altered rocks as an experiment. The results show satisfactory performance of the method. 相似文献
339.
Fifteen samples of (Mg,Fe)SiO3 majorite with varying Fe/Mg composition and one sample of (Mg,Fe)(Si,Al)O3 majorite were synthesized at high pressure and temperature under different conditions of oxygen fugacity using a multianvil press, and examined ex situ using X-ray diffraction and Mössbauer and optical absorption spectroscopy. The relative concentration of Fe3+ increases both with total iron content and increasing oxygen fugacity, but not with Al concentration. Optical absorption spectra indicate the presence of Fe2+–Fe3+ charge transfer, where band intensity increases with increasing Fe3+ concentration. Mössbauer data were used in conjunction with electron microprobe analyses to determine the site distribution of all cations. Both Al and Fe3+ substitute on the octahedral site, and charge balance occurs through the removal of Si. The degree of Mg/Si ordering on the octahedral sites in (Mg,Fe)SiO3 majorite, which affects both the c/a ratio and the unit cell volume, is influenced by the thermal history of the sample. The Fe3+ concentration of (Mg,Fe)(Si,Al)O3 majorite in the mantle will reflect prevailing redox conditions, which are believed to be relatively reducing in the transition zone. Exchange of material across the transition boundary to (Mg,Fe) (Si,Al)O3 perovskite would then require a mechanism to oxidize sufficient iron to satisfy crystal-chemical requirements of the lower-mantle perovskite phase. 相似文献
340.
JIANG Guoliang ) * YANG Dong ) LIU Yun ) ZHANG Guanghua ) LI Zhongjun ) ZHANG Xinhua ) ) College of Marine Life Sciences Ocean University of China Qingdao P..R.China) Fisheries College Ocean University of China Qingdao P..R.China) Agriculture bureau of Anqiu Anqiu P..R.China 《中国海洋大学学报(英文版)》2003,2(1):62-64
1 Introduction Chinaisboththelargestproducerandthelargestconsumerofchemicalfertilizersintheworld .Since1984 ,Chineseconsumptionofchemicalfertilizerhasincreasedmorethanonetimes ,fromabout 17millionmetrictonsto 35millionmetrictons .However ,dur ingthesameperiod ,theyieldoffoodproductionhasincreasedonlyabout 10 % .Thediscrepancybetweenfertilizerconsumptionandyieldincreasehasindicatedthedrasticdecreaseofthebenefitsofchemicalfertiliz ers .Infact ,theutilizationefficiencyofnitrogenfer tilizerinC… 相似文献