From geometry to dynamics of microstructure: using boundary lengths to quantify boundary misorientations and anisotropy

The microstructure of a quartzite experimentally deformed and partially recrystallised at 900 °C, 1.2 GPa confining pressure and strain rate 10⁻⁶/s was investigated using orientation contrast and electron backscatter diffraction (EBSD). Boundaries between misoriented domains (grains or subgrains) were determined by image analysis of orientation contrast images. In each domain, EBSD measurements gave the complete quartz lattice orientation and enabled calculation of misorientation angles across every domain boundary. Results are analysed in terms of the boundary density, which for any range of misorientations is the boundary length for that range divided by image area. This allows a more direct comparison of misorientation statistics between different parts of a sample than does a treatment in terms of boundary number.The strain in the quartzite sample is heterogeneous. A 100×150 μm low-strain partially recrystallised subarea C was compared with a high-strain completely recrystallised subarea E. The density of high-angle (>10°) boundaries in E is roughly double that in C, reflecting the greater degree of recrystallisation. Low-angle boundaries in C and E are produced by subgrain rotation. In the low-angle range 0–10° boundary densities in both C and E show an exponential decrease with increasing misorientation. The densities scale with exp(−θ/λ) where λ is approximately 2° in C and 1° in E; in other words, E has a comparative dearth of boundaries in the 8–10° range. We explain this dearth in terms of mobile high-angle boundaries sweeping through and consuming low-angle boundaries as the latter increase misorientation through time. In E, the density of high-angle boundaries is larger than in C, so this sweeping would have been more efficient and could explain the relative paucity of 8–10° boundaries.The boundary density can be generalised to a directional property that gives the degree of anisotropy of the boundary network and its preferred orientation. Despite the imposed strain, the analysed samples show that boundaries are not, on average, strongly aligned. This is a function of the strong sinuosity of high-angle boundaries, caused by grain boundary migration. Low-angle boundaries might be expected, on average, to be aligned in relation to imposed strain but this is not found.Boundary densities and their generalisation in terms of directional properties provide objective measures of microstructure. In this study the patterns they show are interpreted in terms of combined subgrain rotation and migration recrystallisation, but it may be that other microstructural processes give distinctive patterns when analysed in this fashion.     

川北地区岩石反射谱波特征

四川北部地区既有岩浆岩、变质岩构成的前震旦系结晶变质基底,又有震旦纪以后的沉积盖层,岩石类型十分齐全。本文根据该区的120件岩(矿)石样品反射波谱测试结果,绘制了区内主要岩石类型典型波谱曲线,并对这些波谱曲线进行了初步分析,总结了主要岩石类型的波谱特征,这些岩石波谱特征在西南地区有一定的代表性。     

地球化学样品中硒的循序提取技术

研究开发了一种硒的循序偏提取步骤，将地球化学样品中的硒选择性地循序提取到六个“操作上”定义的相态中：水溶性硒（水提取）；吸附在氧化矿物和粘土矿物上配位可交换的亚硒酸根离子（０．１ｍｏｌ／ＬＫＨ２ＰＯ４提取）；与有机质结合的硒（０．１ｍｏｌ／ＬＮａ４Ｐ２Ｏ７提取）；与铁锰铝氧化物和碳酸盐结合的硒（４．０ｍｏｌ／ＬＨＣｌ提取）；硫化物中的硒（ＫＣｌＯ３＋浓ＨＣｌ提取）；硅酸盐残渣中以副矿物和被硅质包裹的硒微粒存在的硒（ＨＦ＋ＨＮＯ３＋ＨＣｌＯ４强混合酸溶解）。对提取步骤的可行性和实用性作了详细的讨论。     

锦屏Ⅰ级水电站坝区岩体结构面特征研究

本文根据锦屏Ⅰ级水电站坝区体结构面野外调资料，对坝区结构面优势方位、间距、张开度、连通率、隙间充填物及形态特征进行了分析，为坝区岩体分类及其物理力学参数的确定提供了重要依据。     

Stability analysis of rock wedges with multiple sliding surfaces

Summary Although wedge and plane sliding stability analyses are well established in the geotechnical literature, certain geologic environments produce blocks which cannot be adequately modelled as either wedges or plane slides. An example is blocks forming in cylindrically folded sedimentary rocks, where the surface of sliding is neither a single plane nor a double plane but is curved. This type of block may be idealized as a prismatic block with multiple sliding planes, all with parallel lines of intersection. If the sliding planes number three or more, the distribution of normal forces, and hence the factor of safety, is indeterminate. A new analytical model for sliding stability analysis is described in which the distribution of normal forces on the contact planes is chosen to minimize the potential energy of the system. The classic wedge and plane solutions are shown to be special cases of this more general model, which allows determination of the safety factor for any shape of prismatic contact surface. An example from Tennessee concerning a block with a curved sliding surface is described and the factor of safety compared with the standard wedge analysis. It is shown that with three or more contact planes, the safety factor may be significantly lower than that calculated from the wedge model, which provides an upper limit on stability.     

内蒙古科尔康油田沙海组储集层的岩石学特征

根据碎屑岩铸体薄片和扫描电镜观察分析资料，研究了科尔康油田沙海组储集层的岩石学特征。科尔康油田沙海组储集层的岩石类型主要为岩屑砂岩和岩屑砂砾岩。碎屑岩的岩性特征对沙海组储集层的成岩作用具有显著的影响作用。     

我国磁法勘探的研究与进展

简要概述了我国磁法勘探50年来的研究与进展，主要包括：地面、航空与海洋磁测工作，磁力仪研制与生产，磁异常处理与转换技术，磁异常解释理论与方法，岩石磁性研究，磁法勘探在基础地质研究、固体矿产勘查、油气勘查和其他领域中的应用．     

地质速率计—矿物氧扩散的应用

概述了同位素封闭体系内的矿物氧扩散和同位素交换机制及其在地质速率计上的应用。火成岩从高温冷却或变质岩从高峰主质温度冷却过程中，由于冷却速度不同，扩散作用导致的矿物晶体内部及晶粒间氧同位素再平衡也有所不同。通过实测岩石中各组成矿物氧同位素比值，模式含量和颗粒半径，据矿物氧扩散和同位素交换模型，可以估算出岩石的冷却速率。     

岩体力学试验的理论分析

本文通过对岩石力学试验中岩石试件破坏方式的分析, 在理论上解释了岩体力学试验中经常遇到的一些力学现象并且作出了定量的回答, 同时还建立了岩石的各种破坏模式的判据。     

硅酸盐样品微波加热碱熔分解方法

本文研究了硅酸盐样品在常压下，用微波炉进行碱熔分解的熔样时间，试剂用量和滴加水量等情况对分解的影响，确定了最佳实验条件，将此法用于地球化学标准参考样品ＳｉＯ２的测定，取得了满意的结果。