高温密闭溶样电感耦合等离子体质谱准确测定辉钼矿铼-锇地质年龄

采用Carius管高温密闭溶样,电感耦合等离子体质谱(ICP MS)法对采自两个不同金属矿床的辉钼矿样品的Re Os同位素地质年龄进行了准确测定。所得出的Re Os年龄的平均值分别为14.26±0.19Ma和34.39±0.81Ma,相对标准偏差分别为1.3%(以2s计算,n=6)和2.4%(以2s计算,n=7)。采用国际通用的ISOPLOT软件按Model1模式对这两组样品分别进行处理,所得Re Os等时线年龄分别为14.32±0.46Ma和34.52±0.38Ma(均为95%置信水平)。同批次样品中所带的内部管理样JDC的Re Os年龄与国际先进实验室采用负离子热表面电离质谱测量所得的结果吻合也较好。说明在严格的质量体系保证及有效地降低实验室空白水平的前提下,ICP MS完全可以准确地测定辉钼矿的Re Os年龄。     

环电流区中性原子观测特性模拟研究

为了给双星计划中性原子(ENA)探测仪的研制提供可靠 的理论依据，并为未来中性原子探测数据的分析及研究做好准备，针对双星轨道初步模拟计 算了双星ENA探测仪对磁暴时中性原子的观测特性. 建立了磁暴主相期间环电流离子分布的 一 个近似理论模式，并模拟计算了极轨卫星在极区上空、赤道面以及其他位置上对不同强度磁 暴主相期间环电流区ENA空间角分布及能谱的观测结果. 研究表明，存在环电流区方向和南 北极区环电流粒子沉降带两个中性原子强度极大区域；磁暴越强烈，注入区高度越低，环电 流区观测到的ENA通量越高；处于有利位置的ENA探测器可分辨注入区内边界或注入前沿；EN A探测器能够分辨环电流带离子分布的不均匀性；由于离子交换截面的差异，H，O，He 3种E NA的能谱分布不同；在10～80keV能谱范围内通量较强，易于观测；环电流区H，O两种ENA 通 量较强，有利于观测；而环电流区He ENA通量很弱，不易于观测. 模拟计算研究表明，双星 极轨卫星能够对环电流区ENA进行有效探测；低纬轨道上的ENA探测器也能够对环电流区ENA 进行一些观测；ENA探测器的研制应重视低、中能量范围ENA的探测.     

石龟山大桥直径3～4.4m空心桩施工技术

施工φ３￣４．４ｍ空心桩，需要预制空心桩节和护筒，搭建水上平台，进而介绍了钻孔施工，桩节组拼以及压浆等工艺。与实心桩相比，空心桩显示了独特的优越性。     

桩后劈裂压浆施工技术

阐述了桩后劈裂压浆提高单桩承载力的机理、使用设备、操作方法工艺参数和操作注意事项，并对劈裂压浆的压入量及压力进行了初步探讨。     

Observations of flux rope – associated particle bursts with GEOTAIL in the distant tail

Geotail energetic particle, magnetic field data and plasma observations (EPIC, MGF and CPI experiments) have been examined for a number of energetic particle bursts in the distant tail (120Re < |X_GSM| < 130 Re), associated with moving magnetic field structures, following substorm onsets. The features obtained from this data analysis are consistent with the distant magnetotail dynamics determined first by ISEE3 observations and explained in terms of the neutral line model. At the onset of the bursts, before plasma sheet entrance, energetic electrons appear as a field-aligned beam flowing in the tailward direction, followed by anisotro-pic ions. Within the flux rope region, suprathermal ions exhibit a convective anisotropy, which allows determination of the plasma flow velocity, assuming that the anisotropy arises from the Compton-Getting effect. The velocities thus determined in the plasma sheet are estimated to be 200–650 km/s, and compare favourably with the velocities derived from the CPI electron and proton experiment. The estimated length of magnetic field structures varies between 28 and 56 Re and depends on the strength of the westward electrojet intensification. Finally, the three structures reported here show clear magnetic field signatures of flux rope topology. The existence of a strong magnetic field aligned approximately along the Y-axis and centred on the north-to-south excursion of the field, and the bipolar signature in both By and/or Bz components, is consistent with the existence of closed field lines extending from Earth and wrapping around the core of the flux rope structure.     

区域采样法测定水中硫酸根离子的研究

在分散度不同的区域内进行区域采样用于水中硫酸根离子的测定，结果令人满意。应用此方法测定硫酸根离子的线性范围为２００．０～３０００ｍｇ／Ｌ；进样频率为１２０次／ｈ；相对标准偏差为１．７０％     

地质样品中微量金银的在线分离富集方法

提出用ＶＳ－Ⅱ型强碱性阴离子交换纤维定量富集、硫脲解脱，流动注射在线分离富集—火焰原子吸收光谱法测定地质样品中痕量金银的分析方法。该方法检出限低，金为１．４μｇ／ｍＬ，银为０．３５μｇ／ｍＬ，相对标准偏差均小于２％，采样频率为１２０次／ｈ，用于地质样品中痕量金银的直接测定，结果令人满意。     

钻孔扩底灌注桩施工新工艺

本文介绍钻孔扩底灌注桩的施工新工艺，多应式扩底钻头特点，成桩技术标准，适用范围及经济效益分析。     

复合注浆法在基础加固中的应用

复合注浆法是将静压注浆法和高压旋喷注浆法进行时序上的结合，分别发挥两种注浆加固方法各自的优点，又可克服各自的技术和工艺缺陷的一种基础加固新方法，它可以较好地对既有建筑物地基和新建建筑基础出现质量问题进行加固处理。简述了复合注浆法的加固作用机理、设计及计算模型，在此基础上通过工程实例介绍其施工技术并分析其加固效果和经济性。     

Low-Frequency Plasma Waves in the Outer Polar CUSP: A Review of Observations from Prognoz 8, Interball 1, Magion 4, and Cluster

This paper presents a review of the most interesting observations of low-frequency plasma waves together with plasma particles which were made by the Interball 1, Magion 4 and Prognoz 8 satellites in the outer polar cusp. Accelerated plasma particles, hot electron populations and very strong wave activity, particularly at low frequencies, are observed. A detailed study of the wave spectra together with the distribution function for electrons indicate the correlation between the presence of lower-hybrid waves and the population of the particles with higher energy than in the surrounding space. These experimental facts suggest that strong coupling between waves and particles is responsible for plasma heating. During polar cusp crossings by Interball 1 and Prognoz 8, FFT analysis of the wave form indicates many bursts of ULF emissions in both electric and magnetic components. These waves have highly non-stationary characteristics. To study the dynamics of changes in the spectral characteristics of the waves wavelet analysis has been used. Nonlinear interactions are studied using bispectral methods of analysis. This presentation gives the results of such an analysis for selected cusp crossings at different altitudes. An example of wave activity registered by the STAFF instrument onboard the CLUSTER spacecraft in the polar cusp is also presented.