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81.
为寻找天然抗污损活性化合物,以抗硅藻附着活性为导向,采用有机溶剂萃取、半制备高压液相色谱对分离自海绵的芽孢杆菌UST050418-715代谢产物进行分离,纯化抗硅藻附着活性物质,并利用气相色谱-质谱联用仪、核磁共振波谱分析活性物质结构。从菌株UST050418-715代谢产物中分离得到7种具有抗硅藻附着活性的环二肽类化合物,分别鉴定为:(1)环(L-亮氨酸-反式-8-羟基-L-脯氨酸-)、(2)环(L-缬氨酸-L-脯氨酸)、(3)环(D-脯氨酸-L-亮氨酸)、(4)环(L-脯氨酸-D-亮氨酸)、(5)环(甘氨酸-L-脯氨酸)、(6)环(L-苯丙氨酸-顺式-8-羟基-D-脯氨酸-)、(7)环(L-苯丙氨酸-反式-8-羟基-L-脯氨酸-)。说明海绵附生芽孢杆菌UST050418-715代谢产物中存在大量环二肽类化合物,可以帮助宿主海绵实现对硅藻附着的化学防御。 相似文献
82.
Automated Extraction of a Five‐Year LA‐ICP‐MS Trace Element Data Set of Ten Common Glass and Carbonate Reference Materials: Long‐Term Data Quality,Optimisation and Laser Cell Homogeneity 下载免费PDF全文
LA‐ICP‐MS is increasingly applied to obtain quantitative multi‐element data with minimal sample preparation, usually achieved by calibration using reference materials (RMs). However, some ubiquitous RMs, for example the NIST SRM 61× series glasses, suffer from reported value uncertainties for certain elements. Moreover, no long‐term data set of analyses conducted over a range of ablation and tuning conditions exists. Thus, there has been little rigorous examination of the extent to which offsets between measured and reported values are the result of error in these values rather than analytically induced fractionation. We present new software (‘LA‐MINE’), capable of extracting LA‐ICP‐MS data with no user input, and apply this to our system, yielding over 5 years of data (~ 5700 analyses of ten glass and carbonate RMs). We examine the relative importance of systematic analytical bias and possible error in reported values through a mass‐specific breakdown of fourteen of the most commonly determined elements. Furthermore, these data, obtained under a wide range of different ablation conditions, enable specific recommendations of how data quality may be improved, for example the role of diatomic gas, the effect of differential inter‐glass fractionation factors and choice of transport tubing material. Finally, these data demonstrate that the two‐volume Laurin ablation cell is characterised by no discernible spatial heterogeneity in measured trace element ratios. 相似文献
83.
Wei‐Xin Lv Hao‐Ming Yin Meng‐Shu Liu Fang Huang Hui‐Min Yu 《Geostandards and Geoanalytical Research》2021,45(1):245-256
A dry ashing method is commonly used to remove organic material from samples prior to geochemical analysis. In the course of this study, the Cd isotope ratios of a series of soil and plant reference materials and samples were studied to evaluate the effect of the dry ashing method on measurement results of Cd isotope ratios. The samples were pre‐treated using the dry ashing method and high‐pressure bomb for comparison. The results show that the digestion using high‐pressure bombs did not lead to Cd loss, but using the dry ashing method would cause different proportions of Cd loss. The whole range of Cd isotope difference between two methods was from ?0.07‰ to 3.01‰. There was also an obvious difference in measured Cd isotope ratios from the same leaf sample pre‐treated independently by the dry ashing method, indicating that the amount of Cd loss and the effect on Cd isotope measurement during dry ashing is related to the properties of the samples. Therefore, dry ashing may not be appropriate for the removal of organic material in Cd isotope ratio measurement, especially for samples with high organic contents. The δ114/110Cd values of reference materials NIST SRM 1573a and GSD‐30 are reported for the first time in this study. 相似文献
84.
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87.
钻孔灌注桩常见问题分析与探讨 总被引:3,自引:0,他引:3
从对常见灌注桩的缺陷入手,找出造成缺陷的原因.在此基础上分别对影响成孔及灌注质量的有关因素进行了分析,并提出提高钻孔灌注桩质量的对策. 相似文献
88.
Shengming Hu Zhijian Chen Chenghui Wan Chun Tang Wen Xiong 《Marine Georesources & Geotechnology》2020,38(4):385-392
AbstractCompared with traditional methods, the three-dimensional laser-scanning (3D-LS) technique can efficiently acquire many high-quality geometric properties of rock discontinuities. In practice, engineers usually prefer to simplify the processing by using single-station point data and roughly orienting owing to the complexity of registration/georeferencing multi-station point data. However, prior published studies have paid little attention to the accuracy and reliability when determining discontinuity orientations using 3D-LS. We propose a reliable and accurate method with robust on-site applicability. As part of an ongoing effort, we are evaluating the precision of the commonly used coarse registration method and the fine registration method, and promoted the optimized coarse- and fine-registration methods and evaluated their precision. It is found that: (1) the common and the optimized registration method can meet our project’s engineering requirements, and the optimized registration method improved accuracy in the dip direction by approximately 1°; (2) fine registration using an iterative closest point (ICP) algorithm can correct both dip direction and dip angle; and (3) the orientation is of high precision with commonly used coarse and fine registration, whereas the optimization effect to correct the orientation is slightly limited. 相似文献
89.
Population,urbanization and economic scenarios over the Belt and Road region under the Shared Socioeconomic Pathways 总被引:1,自引:0,他引:1
Jing Cheng Tao Hui Jiang Tong Wang Yanjun Zhai Jianqing Cao Lige Su Buda 《地理学报(英文版)》2020,30(1):68-84
The countries throughout the Belt and Road region account for more than 60% of the world's population and half of the global economy. Future changes in this area will have significant influences on the global economic growth, industrial structure and resource allocation. In this study, the proportion of the urban population to the total population and the gross domestic product were used to represent the levels of urbanization and economic development, respectively. The population, urbanization and economic levels of the Belt and Road countries for 2020–2050 were projected under the framework of the IPCC's shared socioeconomic pathways(SSPs), and the following conclusions are drawn.(1) The population, urbanization and economic levels in the Belt and Road region will likely increase under all five pathways. The population will increase by 2%–8%/10 a during 2020–2050 and reach 5.0–6.0 billion in 2050. Meanwhile, the urbanization rate will increase by 1.4%–7.5%/10 a and reach 49%–75%. The GDP will increase by 17%–34%/10 a and reach 134–243 trillion USD.(2) Large differences will appear under different scenarios. The SSP1 and SSP5 pathways demonstrate relatively high urbanization and economic levels, but the population size is comparatively smaller; SSP3 shows the opposite trend. Meanwhile, the economy develops slowly under SSP4, but it has a relatively high urbanization level, while SSP2 exhibits an intermediate trend.(3) In 2050, the population will increase relative to 2016 in most countries, and population size in the fastest growing country in Central Asia and the Middle East countries will be more than double. Urbanization will develop rapidly in South Asia, West Asia and Central Asia, and will increase by more than 150% in the fastest growing countries. The economy will grow fastest in South Asia, Southeast Asia and West Asia, and increase by more than 10 times in some counties with rapid economic development. 相似文献
90.
提出了一种综合利用快速点特征直方图(FPFH)描述符和同名点引导ICP优化的地面激光扫描(TLS)点云配准方法。该方法包括3个步骤:1)点云金字塔构建;2)基于FPFH的粗配准;3)同名点引导的ICP精配准。首先使用体素网格滤波器构造点云的金字塔结构,在粗配准时,FPFH描述符用于金字塔顶层上点云的鲁棒匹配,在此基础上,再进行两层级同名点引导的ICP精配准优化,使用3组典型TLS点云对进行实验,结果表明本文方法可以高效地完成TLS点云的配准。 相似文献