济宁二号矿孤岛工作面冲击矿压危险及其控制

孤岛工作面及其周围巷道附近应力集中程度高,顶板运动剧烈,再加上地质构造的影响,采深较大时,冲击危险程度就高,很容易引发冲击矿压。《煤矿安全规程》要求孤岛工作面按冲击矿压危险工作面来管理。孤岛工作面冲击矿压危险检测预报及控制的技术是先分析冲击危险程度,确定冲击危险指数,提出早期预报;采用电磁辐射和钻屑法进行及时预报;采用卸压爆破进行处理,并采用电磁辐射和钻屑法检验防治措施的效果。实践证明,这套技术安全、可靠、有效,能够保证工作面的安全高效生产。     

发射光谱载体蒸馏法测定地质样品中微量硼铍锡银

选择了适合的缓冲剂,利用载体蒸馏法将被测元素与基体元素分离,使Be转变为易挥发的氟化物与B、Sn、Ag同时蒸发;降低了谱线背景及元素检出限;加入内标元素Au、Bi,提高了方法的准确度和精密度;采用普通 3mm×3mm×0.7mm杯型电极,装样量少,操作简单。方法检出限(wB/10-6)分别可达B1.5、Be0.3、Sn0.8、Ag0.02;准确度(Δlog C)基本在-0.05～0.05,精密度(RSD,n=8)为2.9%～17%。     

Submillimeter-wave and observations of the event on 28 November, 2001

We present a detailed study of a 1B/M6.9 impulsive flare combining high time resolution (1 ms) and instantaneous emission source localization observations at submillimeter frequencies (212 GHz), obtained with the solar submillimeter telescope (SST), and Hα data from the Hα solar telescope for argentina (HASTA). The flare, starting at 16:34 UT, occurred in active region (AR) 9715 (NOAA number) on November 28, 2001, and was followed by an Hα surge. We complement our data with magnetograms from the Michelson Doppler Imager (SOHO/MDI). SST observed a short impulsive burst at 212 GHz, presenting a weak bulk emission (of about 90 sfu) composed of a few shorter duration structures. The integrated Hα and the 212 GHz light curves present a remarkable agreement during the impulsive phase of the event. The delay between both curves stays below 12 s (the time resolution of the Hα telescope). The flare as well as the surge are linked to new flux emergence very close to the main AR bipole. Taking into account the AR magnetic field evolution, we infer that magnetic field reconnection, occurring at low coronal levels, could have been at the origin of the flare; while in the case of surge this would happen at the chromospheric level.     

Experimental study on soil CO2 emission in the alpine grassland ecosystem on Tibetan Plateau

The Tibetan Plateau, the Roof of the World, is the highest plateau with a mean elevation of 4000 m. It is characterized by high levels of solar radiation, low air temperature and low air pressure compared to other regions around the world. The alpine grassland, a typical ecosystem in the Tibetan Plateau, is distributed across regions over the elevation of 4500 m. Few studies for carbon flux in alpine grassland on the Tibetan Plateau were conducted due to rigorous natural conditions. A study of soil respiration under alpine grassland ecosystem on the Tibetan Plateau from October 1999 to October 2001 was conducted at Pangkog County, Tibetan Plateau (31.23°N, 90.01°E, elevation 4800 m). The measurements were taken using a static closed chamber technique, usually every two weeks during the summer and at other times at monthly intervals. The obvious diurnal variation of CO2 emissions from soil with higher emission during daytime and lower emission during nighttime was discovered. Diurnal CO2 flux fluctuated from minimum at 05:00 to maximum at 14:00 in local time. Seasonal CO2 fluxes increased in summer and decreased in winter, representing a great variation of seasonal soil respiration. The mean soil CO2 fluxes in the alpine grassland ecosystem were 21.39 mgCO2 · m-2 · h-1, with an average annual amount of soil respiration of 187.46 gCO2 · m-2 · a-1. Net ecosystem productivity is also estimated, which indicated that the alpine grassland ecosystem is a carbon sink.     

Study of statistically correcting model CMAQ-MOS for forecasting regional air quality

Based on analysis of the air pollution observational data at 8 observation sites in Beijing including outer suburbs during the period from September 2004 to March 2005, this paper reveals synchronal and in-phase characteristics in the spatial and temporal variation of air pollutants on a city-proper scale at deferent sites; describes seasonal differences of the pollutant emission influence between the heating and non-heating periods, also significantly local differences of the pollutant emission influence between the urban district and outer suburbs, i.e. the spatial and temporal distribution of air pollutant is closely related with that of the pollutant emission intensity. This study shows that due to complexity of the spatial and temporal distribution of pollution emission sources, the new generation Community Multi-scale Air Quality (CMAQ) model developed by the EPA of USA produced forecasts, as other models did, with a systematic error of significantly lower than observations, albeit the model has better capability than previous models had in predicting the spatial distribution and variation tendency of multi-sort pollutants. The reason might be that the CMAQ adopts average amount of pollutant emission inventory, so that the model is difficult to objectively and finely describe the distribution and variation of pollution emission sources intensity on different spatial and temporal scales in the areas, in which the pollution is to be forecast. In order to correct the systematic prediction error resulting from the average pollutant emission inventory in CMAQ, this study proposes a new way of combining dynamics and statistics and establishes a statistically correcting model CMAQ-MOS for forecasts of regional air quality by utilizing the relationship of CMAQ outputs with corresponding observations, and tests the forecast capability. The investigation of experiments presents that CMAQ-MOS reduces the systematic errors of CMAQ because of the uncertainty of pollution emission inventory and improves the forecast level of air quality. Also this work employed a way of combining point and area forecasting, i.e. taking the products of CMAQ for a center site to forecast air pollution for other sites in vicinity with the scheme of model products "reanalysis" and average over the "area".     

Localization of mining-induced horizontal fractures along rock layer interfaces in overburden: field measurements and prediction

The locations of mining-induced horizontal fractures along rock interfaces in the overburden of Donetsk Coal Basin were identified using an original experimental device. The device traps methane from horizontal fracture zone (100–fold coal seam thickness) over an active longwall mining excavation. Presence or absence of horizontal fractures along rock layer interfaces is correlated with physical characteristics of the overburden, such as thickness, uniaxial compressive strength of overburden rock layers, location of rock layer interfaces and thickness of extracted coal seams. As a result, a combined criterion based on these physical characteristics is proposed to predict the presence of overburden horizontal fracturing in coal mine operations.     

On Tension Failure of 2-D Rock Specimens and Associated Acoustic Emission

Summary To understand the failure mechanism of quasi-brittle materials like rock under tensile stress, observations on the failure process of granite and marble plate specimens under tension are summarized and presented. Micro- and macro-failure properties of rock plates under uniaxial tension have been characterized by using an acoustic emission technique. Acoustic emission signals associated with micro-fractures are captured to locate the sources. An algorithm based on arrival time difference is developed for this purpose. The results reveal clearly the failure processes of rock which include initiation, nucleation and propagation of micro-fractures when the axial stress is close to the peak strength of rock. It is believed that the difference in heterogeneity between granite and marble specimens leads to different fracture shapes and different behaviors of associated acoustic emissions. Numerical simulation of acoustic emissions for two-dimensional tensile test is also carried out. The simulated characteristics are in good agreement with the experimental results.     

阳城煤矿瓦斯地质规律研究

运用沉积学、构造地质学、煤地质学、数学分析等相关学科和方法,综合分析瓦斯涌出量的地质构造、顶底板岩性、上覆基岩厚度等地质因素,对阳城地区瓦斯含量、涌出量进行量化预测,并作出其全井田瓦斯含量、涌出量的等值线图。研究表明,阳城井田属低瓦斯矿井,瓦斯含量的变化主要与煤层埋深有关,随着煤层上覆基岩厚度以及煤层埋深的增高,瓦斯含量与涌出量在区内由北向南有增高趋势。     

水平电极发射光谱法测试多目标生态地球化学土壤样品中的钼

以K2SO4、S粉、C粉、聚三氟氯乙烯粉、Al2O3、MgO混合物作为缓冲剂,以Sb为内标,电极发射光谱法测试多目标地球化学土壤样品中的钼。方法的检出限为0.28μg/g(3S),方法的精密度(RSD)为7.25%~8.66%。测试了国家一级地球化学标准物质,结果与标准值相符合。该方法已用于10000多件土壤样品的分析,并取得满意的结果。     

卤水浸泡后盐岩声发射特征试验研究

为了研究盐穴能源地下储库建造过程中,腔体围岩处在地温、卤水和地应力地质环境中盐岩的损伤演化特点,利用声发射技术分析盐岩受不同温度的饱和卤水作用后的单轴压缩损伤破坏过程。试验发现：在一定温度的饱和卤水中浸泡30 d后盐岩的单轴抗压强度和弹性模量有所降低,但降低的平均幅度很小;卤水对盐岩主要表现为溶蚀作用,而浸泡弱化作用非常小;单轴压缩过程中盐岩的应力-应变曲线与声发射-应变曲线具有较好的一致性,卤水浸泡后盐岩的累计声发射数随卤水的温度升高略有增加;卤水作用后盐岩试件的声发射率和累计数要小于无卤水作用盐岩;盐穴建造期盐岩受一定温度的卤水作用后盐岩的强度将出现一定弱化,但卤水也会促进损伤盐岩体的重结晶恢复,盐岩的这种特性有利于盐穴建造期安全和稳定。