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41.
提出用VS-Ⅱ型强碱性阴离子交换纤维定量富集、硫脲解脱,流动注射在线分离富集—火焰原子吸收光谱法测定地质样品中痕量金银的分析方法。该方法检出限低,金为1.4μg/mL,银为0.35μg/mL,相对标准偏差均小于2%,采样频率为120次/h,用于地质样品中痕量金银的直接测定,结果令人满意。 相似文献
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岩层移动动态过程的离散单元法分析 总被引:2,自引:0,他引:2
采动覆岩动态发展过程受地质、采矿条件诸多因素的影响,是一个十分复杂的时空过程。通过离散单元法数值模拟,揭示了综放开采条件下采场上覆岩层动态发展规律,特别是覆岩离层缝隙的分布规律、发展形态、空间位置以及与地质采矿条件的关系,揭示了工作面推进过程中,采场上覆岩层中重新分布的应力大小、方向及其发展变化规律,该应力的存在和变化规律是确定井下开采方法、支护方式的依据。 相似文献
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Bernard Pelletier Pierre Dutilleul Guillaume Larocque James W. Fyles 《Mathematical Geology》2004,36(3):323-343
In geostatistical studies, the fitting of the linear model of coregionalization (LMC) to direct and cross experimental semivariograms is usually performed with a weighted least-squares (WLS) procedure based on the number of pairs of observations at each lag. So far, no study has investigated the efficiency of other least-squares procedures, such as ordinary least squares (OLS), generalized least squares (GLS), and WLS with other weighing functions, in the context of the LMC. In this article, we compare the statistical properties of the sill estimators obtained with eight least-squares procedures for fitting the LMC: OLS, four WLS, and three GLS. The WLS procedures are based on approximations of the variance of semivariogram estimates at each distance lag. The GLS procedures use a variance–covariance matrix of semivariogram estimates that is (i) estimated using the fourth-order moments with sill estimates (GLS1), (ii) calculated using the fourth-order moments with the theoretical sills (GLS2), and (iii) based on an approximation using the correlation between semivariogram estimates in the case of spatial independence of the observations (GLS3). The current algorithm for fitting the LMC by WLS while ensuring the positive semidefiniteness of sill matrix estimates is modified to include any least-squares procedure. A Monte Carlo study is performed for 16 scenarios corresponding to different combinations of the number of variables, number of spatial structures, values of ranges, and scale dependence of the correlations among variables. Simulation results show that the mean square error is accounted for mostly by the variance of the sill estimators instead of their squared bias. Overall, the estimated GLS1 and theoretical GLS2 are the most efficient, followed by the WLS procedure that is based on the number of pairs of observations and the average distance at each lag. On that basis, GLS1 can be recommended for future studies using the LMC. 相似文献
45.
The shear viscosities and 1 bar heat capacities of glasses and melts along the 67mol% silica isopleth in the system SiO2-Al2O3-Na2O-TiO2 have been determined in the temperature ranges 780-1140 K and 305-1090 K respectively. Anomalous behaviour of both these properties is observed for compositions rich in TiO2 and/or Al2O3, an observation attributed to liquid-liquid phase separation followed by anatase crystallization. For samples which do not show anomalous behaviour, it is found that the partial molar heat capacity of the TiO2 component previously determined in Al-free compositions reproduces our heat capacities to within 1.3%. Viscosity data show that addition of TiO2 tends to increase viscosity and melt fragility at constant temperature. Furthermore, heat capacity and viscosity data may be combined within the framework of the Adam-Gibbs theory to extract values of the configurational entropy of the liquids and qualitative estimates of the variation of the average energy barrier to viscous flow. Configurational entropy at 900K is inferred to decrease upon addition of TiO2, in contrast to previous results from Al-free systems. The compositional limit separating normal from anomalous behaviour, as well as the data for homogenous melts have been used to constrain the structural role of Ti in these samples. Our data are consistent with a majority of Ti in five-fold coordination associated with a titanyl bond, in agreement with previous spectroscopic studies. Furthermore, we find no evidence for a Ti-Al interaction in our samples, and we are led to the conclusion that Al and Ti are incompletely mixed, a hypothesis consistent with the observed reduction of configurational entropy upon addition of TiO2, suggesting an important role of medium range order in controlling the variations in thermodynamic properties. 相似文献
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Rural Hong Kong contains culturally protected enclaves of remnant woodlands that provide sanctuary for vegetation, wildlife and soil. This study focuses on the influence of natural and cultural factors on soil properties in woodlands with different human activities. At each of the nine selected sites, two pits were dug to collect soil samples for analysis of 24 physical and chemical properties. Analyses of variance between soil attributes and site factors suggest the prominence of woodland size, and important contribution of topography, aspect and parent material. Soil indicators of human impacts and the tenacity of woodland soil towards anthropogenic disturbance were demonstrated. 相似文献
48.
基于方差分量估计的自适应融合导航 总被引:23,自引:4,他引:23
多源传感器观测信息的精度一般不一致,利用方差分量估计理论可以合理地顾及各传感器观测信息在融合导航解中的权比.首先给出基于多源观测信息的融合导航解算模式,进而基于方差分量估计讨论了各传感器观测信息在融合导航解中的合理平衡问题,然后应用自适应因子顾及动力学模型预报信息的贡献,给出了计算过程,并利用模拟数据进行了试算与比较. 相似文献
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50.
On the basis of an experimental study and thermodynamic calculation, the mechanisms of paragenesis and separation of silver, lead and zinc in the hydrothermal system have been studied. At acidic to nearly neutral pH, their chloride complexes are stable, and among them the chloride complexes of zinc are most stable. And the sulfide complexes are the dominant species at nearly neutral to alkaline pH,while the sulfide complexes of silver are most stable. With decreasing temperature, [ Cl^-] ,fO2, and increasing pH, the solubilities of silver, lead and zinc will decrease, leading to their deposition and separation. For sulfide complexes, the concentrations of reduced sulfur and pH are two important factors affecting their stabilities. Complexes of different forms and stabilities respond to the variation of conditions to different extents, which gave rise to the paragenesis and separation of silver, lead and zinc in the whole ore-forming process of dissolution, transport and deposition. 相似文献