高效液相色谱-紫外光谱分析氢醌-双(β-羟乙基)醚

建立了高效液相色谱-紫外光谱法测定聚氨酯扩链剂氢醌-双(β-羟乙基)醚(HQEE)工业品中HQEE主含量和对苯二酚残留的方法。在氰基柱上,以甲醇-水-1%乙酸溶液(体积比10∶50∶40)为流动相,流速1.0 mL/min时,HQEE、对苯二酚及其他相关杂质得到良好分离,紫外光谱285 nm检测。方法简便、快捷,结果准确可靠,在工业生产中可有效地指导HQEE合成过程的质量控制。     

http://www.sciencedirect.com/science/article/pii/S1674987112001545

The presence of natural voids and cavities in subsurface karstic limestones causes severe problem for civil engineering and environmental management.The presence of such features hinders the extension of urbanizations particularly in the new metropolitan.The eastern part of Saudi Arabia contains various types of karstic limestone,sinkholes,solution cavities and voids.In this context,geophysical methods particularly electrical resistivity technique is used as a cost-effective solution for investigating subsurface caves,voids,and shallow weathered zones.2-D electrical resistivity data sets have been acquired along seven profiles in the new urbanization at Al Hassa area.Data processing has been carried out taking into consideration the response of synthetic models,which simulates physical models of the most common karstic features in the area.The results are very useful to determine the extension of shallow weathered zones and to locate different cavities underneath them.The hard limestone bedrock can also be detected and traced along the surveyed profiles.     

青藏高原边缘积雪辐射特征

利用中国陆地生态系统通量观测研究网络的玛曲站观测的一次降雪过程的资料,对青藏高原东部边缘冬季的降雪、积雪过程的辐射特征进行了分析.研究结果表明;积雪期晴天和降雪过程的向上短波辐射的峰值分别约为降雪前晴天的3和2倍.无积雪晴天地表反射率主要分布在0.175～0.36,新雪地表反射率主要分布在0.8～0.9.大气逆辐射变化较小,降雪过程的最大,积雪时的最小.地表长波辐射则为降雪前最大,降雪时最小.积雪覆盖的晴天比无积雪时的净辐射变化幅度减小,且早上由负转正的时间推迟.     

1951-2006年黑龙江省积雪初终日期变化特征分析

利用黑龙江省1951-2006年积雪初终日期资料, 采用统计方法研究了黑龙江省积雪初终日期的时空变化特征. 结果表明: 黑龙江省多年平均有5.5个月的可积雪期, 积雪初日北早南晚, 南北相差1个月;终日南早北晚, 南北相差1.3个月. 积雪初日推后1.9 d·(10a)~(-1), 终日提早1.6 d·(10a)~(-1). 积雪初/终日期的退后/提前主要在较低纬度的平原地区.     

Structure and tectonic evolution of the Southern Eurasia Basin, Arctic Ocean

Multichannel seismic reflection data acquired by Marine Arctic Geological Expedition (MAGE) of Murmansk, Russia in 1990 provide the first view of the geological structure of the Arctic region between 77–80°N and 115–133°E, where the Eurasia Basin of the Arctic Ocean adjoins the passive-transform continental margin of the Laptev Sea. South of 80°N, the oceanic basement of the Eurasia Basin and continental basement of the Laptev Sea outer margin are covered by 1.5 to 8 km of sediments. Two structural sequences are distinguished in the sedimentary cover within the Laptev Sea outer margin and at the continent/ocean crust transition: the lower rift sequence, including mostly Upper Cretaceous to Lower Paleocene deposits, and the upper post-rift sequence, consisting of Cenozoic sediments. In the adjoining Eurasia Basin of the Arctic Ocean, the Cenozoic post-rift sequence consists of a few sedimentary successions deposited by several submarine fans. Based on the multichannel seismic reflection data, the structural pattern was determined and an isopach map of the sedimentary cover and tectonic zoning map were constructed. A location of the continent/ocean crust transition is tentatively defined. A buried continuation of the mid-ocean Gakkel Ridge is also detected. This study suggests that south of 78.5°N there was the cessation in the tectonic activity of the Gakkel Ridge Rift from 33–30 until 3–1 Ma and there was no sea-floor spreading in the southernmost part of the Eurasia Basin during the last 30–33 m.y. South of 78.5°N all oceanic crust of the Eurasia Basin near the continental margin of the Laptev Sea was formed from 56 to 33–30 Ma.     

时间剖面上小断层的计算机自动检测

煤田地震勘探一直探寻着对小断层的自动检测方法，因受各种因素的影响，至今尚无良策。本文介绍了多元地震参数的模式识别方法，并通过模型及实测资料成功地检测到１０ｍ以下小断层。     

L'archivage des activités humaines par les neiges et glaces polaires : le cas du plomb

The investigation of the occurrence of lead in dated snow and ice from Greenland and Antarctica has played a major role in our understanding of the history of the pollution of the atmosphere of our planet by this metal. Such studies have however proved to be very demanding, mainly because of the extreme purity of polar snow and ice. Reliable measurements can be obtained only if ultra-clean and highly sensitive procedures are used, as pioneered by Clair Patterson. The Greenland data show evidence of large-scale pollution of the atmosphere of the Northern Hemisphere for lead as early as two millennia ago during Greco–Roman times, especially because of mining and smelting activities in southern Spain. It peaked at the end of the 1960s, with lead concentrations in snow about 200 times higher than natural values, before declining during recent times because of the fall in the use of leaded gasoline. Lead pollution in Antarctica was already significant at the end of the 19th century as a consequence of whaling activities, the traffic of coal-powered ships crossing the Cape Horn, and mining activities in South America, South Africa and Australia. After declining because of the opening of the Panama Canal, the great economic depression and World War II, it reached a maximum during the 1980s, with lead concentrations 20 times higher than natural values. Other studies focus on past natural variations of lead in ancient ice dated from the last climatic cycles. To cite this article: C. Boutron et al., C. R. Geoscience 336 (2004).     

地质雷达在隧道检测中的应用

隧道施工完成后用常规方法很难对衬砌质量做出系统评价，地质雷达利用超高频脉冲电磁波探测目标介质的介电常数，很容易掌握砼衬砌结构的厚度、衬砌周围回填及空隙情况，围岩断层裂隙构造情况等，为工程技术评价提供依据。文章以实例，介绍了利用地质雷达对隧道进行检测所使用的仪器、工作参数及地质雷达资料处理解释步骤，并通过对几幅典型雷达图像进行分析介绍了不同异常结构在雷达剖面上的反映。     

挤扩支盘灌注桩成桩技术及工程应用

结合工程实践,介绍了挤扩支盘灌注桩技术在某水泥公司5000 t/d新型干法生产线项目桩基工程中的应用效果,并对部分施工措施进行了探讨。