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This paper evaluates the analytical precision, accuracy and long‐term reliability of the U‐Pb age data obtained using inductively coupled plasma–mass spectrometry (ICP‐MS) with a frequency quintupled Nd‐YAG (λ = 213nm) laser ablation system. The U‐Pb age data for seven standard zircons of various ages, from 28 Ma to 2400 Ma (FCT, SL13, 91500, AS3, FC1, QGNG and PMA7) were obtained with an ablation pit size of 30 μm diameter. For 207Pb/206Pb ratio measurement, the mean isotopic ratio obtained on National Institute of Standards and Technology (NIST) SRM610 over 4 months was 0.9105 ± 0.0014 (n = 280, 95% confidence), which agrees well with the published value of 0.9096. The time‐profile of Pb/U ratios during single spot ablation showed no significant difference in shape from NIST SRM610 and 91500 zircon standards. These results encouraged the use of the glass standard as a calibration standard for the Pb/U ratio determination for zircons with shorter wavelength (λ = 213 nm) laser ablation. But 206Pb/238U and 207Pb/235U ages obtained by this method for seven zircon standards are systematically younger than the published U‐Pb ages obtained by both isotope dilution–thermal ionization mass spectrometry (ID‐TIMS) and sensitive high‐resolution ion‐microprobe (SHRIMP). Greater discrepancies (3–4% younger ages) were found for the 206Pb/238U ages for SL13, AS3 and 91500 zircons. The origin of the differences could be heterogeneity in Pb/U ratio on SRM610 between the different disks, but a matrix effect accuracy either in the ICP ion source or in the ablation‐transport processes of the sample aerosols cannot be neglected. When the 206Pb/238U (= 0.2302) newly defined in the present study is used, the measured 206Pb/238U and 207Pb/235U ages for the seven zircon standards are in good agreement with those from ID‐TIMS and SHRIMP within ±2%. This suggests that SRM610 glass standard is suitable for ICP‐MS with laser ablation sampling (LA‐ICP‐MS) zircon analysis, but it is necessary to determine the correction factor for 206Pb/238U by measuring several zircon standards in individual laboratories. 相似文献
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山区生态县区域协调发展的机制构建--以粤北始兴县为例 总被引:1,自引:0,他引:1
区域协调机制在不同类型地域和一种类型地域的不同的发展阶段是不同的。始兴县作为一个典型的山区生态县,工业进入加速发展时期,在此经济发展阶段的区域协调问题主要表现在:与外部区域经济、社会发展差距拉大,工业化与流域生态环境保护的矛盾已开始凸现,县政府协调区域发展的财政能力较低,区域协调机制不健全等。由此对始兴县的区域协调机制进行建构:建立健全多层次的区域协调机构;加大纵向和横向政府财政转移支付的力度;加强与相邻相关地区的协调;实施区域空间管治协调,保护城乡生态环境;科学合理选择产业,大力发展循环经济;全县推行绿色GDP考核等。 相似文献
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Residential RC framed structures suffered heavily during the 2001 Bhuj earthquake in Gujarat, India. These types of structures
also saw severe damage in other earthquakes such as the 1999 Kocaeli earthquake in Turkey and 921 Ji-Ji earthquake in Taiwan.
In this paper the seismic response of residential structures was investigated using physical modelling. Idealised soft storey
and top heavy, two degrees of freedom (2DOF) portal frame structures were developed and tested on saturated and dry sand models
at 25 g using the Schofield Centre 10-m Beam Centrifuge. It was possible to recreate observed field behaviour using these
models. As observed in many of the recent earthquakes, soft storey structures were found to be particularly vulnerable to
seismic loads. Elastic response spectra methods are often used in the design of simple portal frame structures. The seismic
risk of these structures can be significantly increased due to modifications such as removal of a column or addition of heavy
water tanks on the roof. The experimental data from the dynamic centrifuge tests on such soft storey or top-heavy models was
used to evaluate the predictions obtained from the response spectra. Response spectra were able to predict seismic response
during small to moderate intensity earthquakes, but became inaccurate during strong earthquakes and when soil structure interaction
effects became important. Re-evaluation of seismic risk of such modified structures is required and time domain analyses suggested
by building codes such as IBC, UBC or NEHRP may be more appropriate. 相似文献