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501.
循环水及污水中总磷的国家标准方法是用分光光度法测定,当样品中有机磷含量高时,分解易碳化,操作繁琐,分析误差大.本文应用磷钼黄显色示差分光光度技术测定某钢厂循环管道除垢污水中的总磷,通过正交实验确立了采用硝酸-高氯酸消解样品,将样品中聚磷酸盐、有机磷酸盐转化为正磷酸盐,在硝酸溶液中,正磷酸盐与钒钼酸铵作用生成可溶性黄色磷钒钼酸配合物,基于其颜色强度与磷的浓度成正比测定高浓度磷的含量.实验对使用的氧化剂用量、溶解温度、显色条件、测定波长进行优化,结果表明,磷含量在10.0 ~ 40.0 mg/L范围符合朗伯-比尔定律,方法精密度(RSD)<1.0%(n=5),加标回收率为98.8%~105.0%.建立的示差光度法比一般光度法相对误差小,准确度更高;与电感耦合等离子体发射光谱法的测定结果基本吻合,且测定成本更低. 相似文献
502.
《International Journal of Digital Earth》2013,6(1):85-102
ABSTRACTThis paper aims to demonstrate results and considerations regarding the use of remote sensing big data for archaeological and Cultural Heritage management large scale applications. For this purpose, the Earth Engine© developed by Google© was exploited. Earth Engine© provides a robust and expandable cloud platform where several freely distributed remote sensing big data, such as Landsat, can be accessed, analysed and visualized. Two different applications are presented here as follows: the first one is based on the evaluation of multi-temporal Landsat series datasets for the detection of buried Neolithic tells (‘magoules’) in the area of Thessaly, in Greece using linear orthogonal equations. The second case exploits European scale multi-temporal DMSP-OLS Night-time Lights Time Series to visualize the impact of urban sprawl in the vicinity of UNESCO World Heritage sites and monuments. Both applications highlight the considerable opportunities that big data can offer to the fields of archaeology and Cultural Heritage, while the studies also demonstrate the great challenges that still are needed to be overcome in order to make the exploitation of big data process manageable and fruitful for future applications. 相似文献
503.
A new method based on orthogonal least square (OLS) of multiquadric algorithm (MOLS) is proposed for digital elevation model (DEM) generalization by the retrieval of critical points from a grid-based DEM to construct a triangulated irregular network surface. The focus is on the method for accurately obtaining the critical points, which maximally retain the important terrain feature lines. The grid-based DEM to be generalized is first approximated in terms of multiquadric method, and then the significances of the grids are assessed based on OLS method with the merit that each selected grid point gives the maximal increment to the explained variance of the desired output. We used six study sites with different terrain complexities to comparatively analyze the generalization accuracies of MOLS and the classical methods including very important method and point-additive method (Latticetin) under different numbers of retrieved significant points. The results indicate that MOLS averagely performs better than the classical methods for the original DEM generalization in terms of root mean square error. The analytical results also show that MOLS has the better ability in maintaining the feature lines inherent in the original DEM than the classical methods in terms of streamline matching rate. The perfect performance of the newly proposed method can be attributed to the high accuracy of multiquadric method for surface approximation and the effectiveness of OLS for point significance assessment. 相似文献
504.
从金银花中提取绿原酸的工艺研究 总被引:7,自引:0,他引:7
用不同浓度的乙醇从金银花中提取绿原酸,以正交实验进行优化工艺研究,采用紫外分光光度法测定提取液中绿原酸的含量,探讨了乙醇浓度、乙醇倍量、回流时间、pH值、浸泡温度对绿原酸含量的影响。实验结果表明,最佳的工艺条件是:10倍量50%乙醇为浸提剂,浸泡温度为70℃,pH=7,回流时间为1h,提取次数为2次。 相似文献
505.
比较了4种常用蛋白酶对中国毛虾的酶解效果,筛选出胰蛋白酶和枯草杆菌蛋白酶为最佳用酶,并利用正交试验优化了水解条件,在各自最佳水解条件下采用先加胰蛋白酶再加枯草杆菌蛋白酶的酶解方式对中国毛虾进行联合双酶水解,水解度可达67 .83%。 相似文献
506.
Object-based shadow detection in urban areas is an important topic in very high resolution remote sensing image processing. Multi-resolution segmentation (MRS) is an effective segmentation method, and is used for object-based shadow detection. However, several input parameters within MRS may result in unstable performance for final shadow detection; thus, the evaluation and optimization for the parameters upon the final shadow detection accuracy cannot be overlooked. In this paper, the three parameters in MRS (scale s, weight of colour wcolor and weight of compactness wcompact) upon the final result of a recently proposed method, object-based shadow detection with Dempster–Shafer theory, were evaluated and optimized by sensitivity analysis and Taguchi’s method with three experimental data. Experiments show that scale s is the most sensitive parameter among the three parameters within MRS. More importantly, according to the Taguchi’s method theory, there is a very significant interaction effect between s and wcolor, which cannot be overlooked. The shadow detection accuracy yielded by the optimum parameter combination in consideration of the interaction effect is higher than that only optimized by covering the main effect of single parameter in most cases. 相似文献
507.
508.
509.
针对高悬浮物矿井水,设计了5水平6因素的L25(56)正交混凝试验,并通过极差分析确定了混凝的最优化条件,即选择PAC作为混凝剂,pH值调节为9,混凝剂与助凝剂浓度比为20∶1,助凝剂PAM投加滞后30 s,水力条件依次为n=350 r.min-1快速搅拌30 s,n=120 r.min-1中速搅拌4 min,n=60 r.min-1慢速搅拌6 min。通过单因素分析了6种因素对混凝的影响程度,即:PAM投量>混凝剂种类>pH值>混凝剂投量>水力条件>投加时间。依试验结果,对垂向轴式混合反应池进行了参数设计。 相似文献
510.
A season-reliant empirical orthogonal function(S-EOF) analysis was applied to the seasonal mean SST anomalies(SSTAs) based on the HadISST1 dataset with linear trend removed at every grid point in the South Pacific(60.5-19.5 S,139.5 E-60.5 W) during the period 1979-2009.The spatiotemporal characteristics of the dominant modes and their relationships with ENSO were analyzed.The results show that there are two seasonally evolving dominant modes of SSTAs in the South Pacific with interannual and interdecadal variations;they account for nearly 40% of the total variance.Although the seasonal evolution of spatial patterns of the first S-EOF mode(S-EOF1) did not show remarkable propagation,it decays with season remarkably.The second S-EOF mode(S-EOF2) showed significant seasonal evolution and intensified with season,with distinct characteristics of eastward propagation of the negative SSTAs in southern New Zealand and positive SSTAs southeast of Australia.Both of these two modes have significant relationships with ENSO.These two modes correspond to the post-ENSO and ENSO turnabout years,respectively.The SEOF1 mode associated with the decay of the eastern Pacific(EP) and the central Pacific(CP) types of ENSO exhibited a more significant relationship with the EP/CP type of El Nin o than that with the EP/CP type of La Nin a.The S-EOF2 mode contacted with the EP type of El Nin o changing into the EP/CP type of La Nin a showed a more significant connection with the EP/CP type of La Nin a. 相似文献