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61.
62.
An Investigation of Digestion Methods for Trace Elements in Bauxite and Their Determination in Ten Bauxite Reference Materials Using Inductively Coupled Plasma‐Mass Spectrometry
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Wen Zhang Liang Qi Zhaochu Hu Cunjiang Zheng Yongsheng Liu Haihong Chen Shan Gao Shenghong Hu 《Geostandards and Geoanalytical Research》2016,40(2):195-216
Trace elements from samples of bauxite deposits can provide useful information relevant to the exploration of the ore‐forming process. Sample digestion is a fundamental and critical stage in the process of geochemical analysis, which enables the acquisition of accurate trace element data by ICP‐MS. However, the conventional bomb digestion method with HF/HNO3 results in a significant loss of rare earth elements (REEs) due to the formation of insoluble AlF3 precipitates during the digestion of bauxite samples. In this study, the digestion capability of the following methods was investigated: (a) ‘Mg‐addition’ bomb digestion, (b) NH4HF2 open vessel digestion and (c) NH4F open vessel digestion. ‘Mg‐addition’ bomb digestion can effectively suppress the formation of AlF3 and simultaneously ensure the complete decomposition of resistant minerals in bauxite samples. The addition of MgO to the bauxite samples resulted in (Mg + Ca)/Al ratios ≥ 1. However, adding a large amount of MgO leads to significant blank contamination for some transition elements (V, Cr, Ni and Zn). The NH4HF2 or NH4F open vessel digestion methods can also completely digest resistant minerals in bauxite samples in a short period of time (5 hr). Unlike conventional bomb digestion with HF/HNO3, the white precipitates and the semi‐transparent gels present in the NH4HF2 and NH4F digestion methods could be efficiently dissolved by evaporation with HClO4. Based on these three optimised digestion methods, thirty‐seven trace elements including REEs in ten bauxite reference materials (RMs) were determined by ICP‐MS. The data obtained showed excellent inter‐method reproducibility (agreement within 5% for REEs). The relative standard deviation (% RSD) for most elements was < 6%. The concentrations of trace elements in the ten bauxite RMs showed agreement with the limited certified (Li, V, Cr, Cu, Zn, Ga, Sr, Zr and Pb) and information values (Co, Ba, Ce and Hf) available. New trace element data for the ten RMs are provided, some of which for the first time. 相似文献
63.
Huawei Qin Zhen Cai Jianjun Wang Wei Ye Ying Chen 《Marine Georesources & Geotechnology》2016,34(5):403-408
The shortcomings of gravity corers in sampling marine sediments have been observed extensively in various field tests. In order to optimize the coring, this article provides an alternative numerical way to model the gravity coring and analyze the sampling effect. Based on this analysis, a new hydraulic hammer corer is devised. A coupled Eulerian-Lagrangian method with capability of simulating the problem involving extreme deformation, penetration is used to simulate the coring process. The results show that the hydrostatic pressure and deviator stress increase and reach their peak when the pile tip is slightly above or at the level of the observation point and then drop rapidly when the pile tip slides below the observation point. In addition, the stress path indicates that the soil element sustains plastic compression before yielding and then expands until recovering to the original state. The obvious “under-sampling” phenomenon is also well-captured by the finite element model. 相似文献
64.
Coupled Dynamic Response Analysis of A Multi-Column Tension-Leg-Type Floating Wind Turbine 总被引:4,自引:3,他引:1
This paper presents a coupled dynamic response analysis of a multi-column tension-leg-type floating wind turbine (WindStar TLP system) under normal operation and parked conditions. Wind-only load cases, wave-only load cases and combined wind and wave load cases were analyzed separately for the WindStar TLP system to identify the dominant excitation loads. Comparisons between an NREL offshore 5-MW baseline wind turbine installed on land and the WindStar TLP system were performed. Statistics of selected response variables in specified design load cases (DLCs) were obtained and analyzed. It is found that the proposed WindStar TLP system has small dynamic responses to environmental loads and it thus has almost the same mean generator power output under operating conditions as the land-based system. The tension mooring system has a sufficient safety factor, and the minimum tendon tension is always positive in all selected DLCs. The ratio of ultimate load of the tower base fore-aft bending moment for the WindStar TLP system versus the land-based system can be as high as 1.9 in all of the DLCs considered. These results will help elucidate the dynamic characteristics of the proposed WindStar TLP system, identify the difference in load effect between it and land-based systems, and thus make relevant modifications to the initial design for the WindStar TLP system. 相似文献
65.
Lulu Zhang Fang Wu Yafei Zheng Lihong Chen Jie Zhang Xu Li 《Georisk: Assessment and Management of Risk for Engineered Systems and Geohazards》2018,12(3):169-182
Multiple types of responses, such as displacements, ground water level, pore water pressures, water contents, etc., are usually measured in comprehensive monitoring programmes for rainfall-induced landslide prevention. In this study, a probabilistic calibration method for coupled hydro-mechanical modelling of slope stability is presented with integration of multiple types of measurements. A numerical example of a soil slope under rainfall infiltration is illustrated to compare the effects of single and multiple types of responses on parameter estimation and model calibration. The results show that the soil parameters can be estimated with less uncertainty and total uncertainty bounds are narrower with multiple types of responses than with a single type of response. Model calibration based on multiple types of responses can compromise different responses and hence the means and standard deviations of model error are the smallest. A feasible correlation coefficient between soil modulus and permeability can be obtained from model calibration with multiple types of responses and single type of response as long as the responses include displacement data. 相似文献
66.
易地扶贫搬迁改变了搬迁农户生计策略,同时影响了其土地利用行为,二者之间的耦合协调度直接影响着农户的可持续生计。本文以贵州省习水县易地搬迁农户调研数据为基础,构建以农户生计策略和土地利用行为为子系统的耦合协调度模型,分析2个子系统之间的耦合关系和耦合协调关系。研究表明:纯农型农户、农兼型农户、兼农型农户生计策略与土地利用行为之间的耦合度值介于0.4~0.5之间,水平较低,处于拮抗状态;不同类型农户生计策略与土地利用行为系统耦合协调度值均处于0.39~0.49之间,处于濒临失调阶段,存在较大优化空间;传统的农业生产形式对于改善农户生计无明显效果,引导农户向专业农业型农户转变对于促进移民安置区“人地系统”协调发展大有裨益。研究结果可为农户生计与土地利用的可持续发展提供理论依据。 相似文献
67.
开展降雨型地质灾害预报是减少灾害损失的有效方法。该文在讨论降雨型地质灾害预报相关概念的基础上,结合国内外已有的研究成果,系统总结了隐式统计模型、显式统计模型和动力模型等降雨型地质灾害预报模型的特点和适用条件。近几年区域降雨型地质灾害的预报技术研究有以下新特点:统计模型简单实用,目前已经由单一考虑降雨特征的第1代隐式统计模型,进一步发展为考虑地质、地貌等静态因子的显示统计模型;动力模型逐渐由基于垂直入渗理论的边坡稳定性模型开始向基于水土耦合机制的复杂预报模型发展;降雨型地质灾害业务预报预警的核心是地质灾害预报模型的本地化运行,我国已经基于统计模型搭建了服务于不同区域的业务预报预警系统。结合多源预报降雨资料,搭建基于水土耦合机制的降雨型地质灾害集合预报预警系统是未来可能的发展方向。 相似文献
68.
Y. H. CHAI 《地震工程与结构动力学》1996,25(2):149-161
The current approach for seismic retrofit of deficient bridge columns in California involves extensive use of steel jacketing. In this paper, the influence of steel jacketing on the lateral response of circular bridge columns is studied; particularly, the enhancement of the ultimate compressive strain of concrete, the increase in curvature ductility capacity and the increase in lateral stiffness are investigated. The current steel jacket thickness used in California is shown to enhance the ultimate compressive strain of concrete by 4–9 times the spalling strain of unconfined concrete. For larger steel jacket thickness, the ultimate limit state of steel-jacketed columns may be governed by the low-cycle fatigue fracture of the longitudinal reinforcement instead of the ultimate compressive strain of concrete. Steel jacketing is also expected to increase significantly the lateral stiffness of columns if full-height steel jackets are used. The increase in lateral stiffness of flexural columns (3⩽L/D⩽9) is estimated to be 35–60 per cent using current jacket thickness. Inelastic dynamic analyses of steel-jacketed columns using ground motions recorded during the 1989 Loma Prieta earthquake indicated that the current steel jacket thickness provides adequate protection against the damage potential of the ground motions with comparable spectral acceleration as that specified in current design spectra, and the damage sustained by the steel-jacketed column is likely to be repairable. 相似文献
69.
The mathematical base of the double porosity concept, consisting of the continuity and equilibrium equation respectively, is briefly reviewed. A quasi-steady-state transfer function, the so-called leakage term, is used. Important aspects of the developed code, based on the double porosity theory, are presented together with two hypothetical example problems. The resulting trend of the settlements are compared to those from previous work and was found to be significantly different. However, the implications are that the present study exhibits a more realistic prediction for the settlement. 相似文献
70.
预应力混凝土连续梁桥振动特性变异及舒适度评价 总被引:2,自引:1,他引:1
由于预应力损失、混凝土收缩徐变、超载等原因,预应力混凝土桥梁出现了较强的振动。本文通过对福建省福州市闽江三桥全桥环境振动试验和正常运营条件下24小时的监测,研究预应力混凝土连续梁桥的动力特性及其变异和振动舒适度,结果表明:在较为稳定的风和温湿度环境下,固有频率在一天内的最大变化为3.06%,模态阻尼比的最大变化为37.93%,舒适度的狄克曼指标降到“能忍受短时间振动”的区域。 相似文献