Simultaneous radio and optical observations of the mid-latitude atmospheric response to a major geomagnetic storm of 6–8 April 2000

Basic properties of the mid-latitude traveling ionospheric disturbances (TIDs) during the maximum phase of a major magnetic storm of 6–8 April 2000 are shown. Total electron content (TEC) variations were studied by using data from GPS receivers located in Russia and Central Asia. The nightglow response to this storm at mesopause and termospheric altitudes was also measured by optical instruments FENIX located at the observatory of the Institute of Solar-Terrestrial Physics (51.9°N,103.0°E), and MORTI located at the observatory of the Institute of Ionosphere (43.2°N, 77.0°E). Observations of the O (557.7 and 630.0 nm) emissions originating from atmospheric layers centered at altitudes of 90 and 250 km were carried out at Irkutsk and of the O₂(b¹∑_g⁺−X³∑_g⁻) (0-1) emission originating from an atmospheric layer centered at altitude of 94 km was carried out at Almaty. Our radio and optical measurement network observed a storm-induced solitary large-scale wave with duration of 1 h and a wave front width of no less than 5000 km, while it traveled equatorward with a velocity of 200 m/s from 62°N to 38°N geographic latitude. The TEC disturbance, basically displaying an electron content depression in the maximum of the F2 region, reveals a good correlation with growing nightglow emission, the temporal shift between the TEC and emission variation maxima being different for different altitudes. A comparison of the auroral oval parameters with dynamic spectra of TEC variations and optical 630 nm emissions in the frequency range 0.4–4 mHz (250–2500 s periods) showed that as the auroral oval expands into mid-latitudes, also does the region with a developed medium-sale and small-scale TEC structure.     

灌淤土壤可溶性盐分空间变异性与棉花生长关系研究

运用地统计学方法，在灌淤土壤上进行了棉田土壤可溶性盐分的空间变异规律与棉花生长关系系统研究。传统统计学分析表明土壤盐分测试数据基本符合正态分布；在一定取样间距下，土壤可溶性盐分的田间合理取样数目为27。半方差分析显示：土壤可溶性盐分具中等的水平变异性，但随着聚样深度的增加未表现出明显的垂直变异特性；随着棉花的生长发育，土壤可溶性盐分呈现出逐渐减弱的时间变异规律，采用直线或曲线拟合方程估计了可溶性盐分的半方差图及其参数，并绘制了其相应的等值线图。土壤可溶性盐分与棉花产量之间的相关分析表明：可溶性盐分含量与棉花产量之间呈显著负相关关系，且花铃期的相关性较播前显著。研究结果为提高田间试验有效性以及盐渍化土壤改良提供了科学依据与基础资料。     

等离子体发射光谱法直接测定海洋沉积物中的微量稀土元素

应用全谱直读电感耦合等离子体发射光谱法对海洋沉积物中微量稀土元素的测定进行了研究，选择了最佳的仪器工作条件，采用多谱线拟合技术进行校正，样品的加标回收率为94．0％-110．0％。方法采用海底沉积物国家一级标准物质进行验证，测定结果与标准值较吻合，各元素10次测定的RSD≤11．3％。     

单道扫描电感耦合等离子体发射光谱法测定珊瑚礁中主量和微量元素

建立了用单道扫描电感耦合等离子体发射光谱法测定珊瑚礁中主量和微量元素的方法。珊瑚礁样品经酸溶解后,直接进行Ca、Mg、K、Na、V、Sr、Ba、Co、Ni、Pb、Li、Rb的测定,方法检出限为0.0004～0.1mg/L,精密度RSD<5%(n=6),样品的加标回收率为97%～105%。测定w(CaO)为50%的样品,结果与传统的EDTA容量法相符。方法经碳酸盐岩石国家一级标准物质验证可行,已用于大批量的珊瑚礁样品的测定。     

加卸载响应比(LURR)理论的实验研究

利用大尺度岩石试件破坏声发射实验，对加卸载响应比(Load/Unload Response Ratio)理论进行了实验研究。实验采用的加载条件力求能够模拟地下岩石的复杂受力过程。在加载过程中，岩石试件内部出现的损伤用声发射技术进行了记录。实验数据经过分析之后所得的结论与加卸载响应比理论预测的结果相符合。把加卸载响应比值Y的变化情况与声发射事件定位的过程相对比，也可以进一步看出岩石材料内部的损伤发展过程与加卸载响应比Y值的变化具有一致性。而高Y值的异常情况出现，又是在材料发生最终破坏之前，所以，可以用加卸载响应比理论定量地分析岩石试件损伤演化情况，从而对岩石材料的破坏及地震做出预测。实验结果再一次验证了加卸载响应比理论。     

济宁二号矿孤岛工作面冲击矿压危险及其控制

孤岛工作面及其周围巷道附近应力集中程度高,顶板运动剧烈,再加上地质构造的影响,采深较大时,冲击危险程度就高,很容易引发冲击矿压。《煤矿安全规程》要求孤岛工作面按冲击矿压危险工作面来管理。孤岛工作面冲击矿压危险检测预报及控制的技术是先分析冲击危险程度,确定冲击危险指数,提出早期预报;采用电磁辐射和钻屑法进行及时预报;采用卸压爆破进行处理,并采用电磁辐射和钻屑法检验防治措施的效果。实践证明,这套技术安全、可靠、有效,能够保证工作面的安全高效生产。     

单道扫描电感耦合等离子体发射光谱法测定大洋标准物质中稀土元素

采用单道扫描等离子体发射光谱法测定了大洋多金属结核及深海沉积物中的稀土元素与钪，比较了不同功率下各稀土元素的检测限，研究了低功率下的稳定性，拟定了可靠的样品处理方法。方法经多金属结核及深海沉积物国家标准ＧＢＷ０７３１３、ＧＢＷ０７２４９分析验证，结果与标准值相符。测定精度（ＲＳＤ）在１３％～５３％。已用此法为第２批多金属结核和深海沉积物标准物质提供了定值数据，其结果无剔除值     

锇粉中杂质元素分析方法研究

利用ＩＣＰ＿ＭＳ技术建立了锇粉中痕量杂质元素的分析方法。在浓ＨＮＯ３介质中，锇以ＯｓＯ４形式挥发除去，分离锇基体后，可直接测定的痕量元素达５０余种。取样量０．１ｇ，测定限为０．２～２４６ｎｇ／ｇ，可实现质量分数ｗ（Ｏｓ）为９９．９９９９％锇粉中杂质元素测定。结合ＩＣＰ＿ＡＥＳ测定Ｋ、Ｎａ、Ｃａ、Ｍｇ、Ａｌ、Ｆｅ、Ｓｉ和Ｐ，可实现锇粉原料及产品的纯度分析。     

发射光谱载体蒸馏法测定地质样品中微量硼铍锡银

选择了适合的缓冲剂,利用载体蒸馏法将被测元素与基体元素分离,使Be转变为易挥发的氟化物与B、Sn、Ag同时蒸发;降低了谱线背景及元素检出限;加入内标元素Au、Bi,提高了方法的准确度和精密度;采用普通 3mm×3mm×0.7mm杯型电极,装样量少,操作简单。方法检出限(wB/10-6)分别可达B1.5、Be0.3、Sn0.8、Ag0.02;准确度(Δlog C)基本在-0.05～0.05,精密度(RSD,n=8)为2.9%～17%。     

Submillimeter-wave and observations of the event on 28 November, 2001

We present a detailed study of a 1B/M6.9 impulsive flare combining high time resolution (1 ms) and instantaneous emission source localization observations at submillimeter frequencies (212 GHz), obtained with the solar submillimeter telescope (SST), and Hα data from the Hα solar telescope for argentina (HASTA). The flare, starting at 16:34 UT, occurred in active region (AR) 9715 (NOAA number) on November 28, 2001, and was followed by an Hα surge. We complement our data with magnetograms from the Michelson Doppler Imager (SOHO/MDI). SST observed a short impulsive burst at 212 GHz, presenting a weak bulk emission (of about 90 sfu) composed of a few shorter duration structures. The integrated Hα and the 212 GHz light curves present a remarkable agreement during the impulsive phase of the event. The delay between both curves stays below 12 s (the time resolution of the Hα telescope). The flare as well as the surge are linked to new flux emergence very close to the main AR bipole. Taking into account the AR magnetic field evolution, we infer that magnetic field reconnection, occurring at low coronal levels, could have been at the origin of the flare; while in the case of surge this would happen at the chromospheric level.