MnO2共沉淀直接β计数测定小体积海水中的234Th

探讨了MnO₂共沉淀直接β计数测定小体积海水中234Th方法在固体闪烁α/β计数仪上实现的可能性,对实验流程空白、流程化学回收率、仪器探测效率、MnO₂共沉淀量对全程回收率的影响以及检测核素的特征性等进行了研究.结果表明,该方法具有稳定的流程空白和全程回收率、高的探测效率和化学回收率,且所检测核素与234Th的理论半衰期基本吻合.将该流程应用于亚热带北太平洋表层水中234Th的分析也得到了令人满意的结果.与传统方法相比,该方法具有流程简单、所用水样体积小、快速获得结果等特点,适合于船载分析,由此可实现高时空分辨率数据的获取,为海洋颗粒有机碳输出通量以及颗粒物迁移速率的研究提供了更好的分析手段.     

An Inshore Poleward Current in the NW of the Iberian Peninsula Detected from Satellite Images, and its Relation withG. catenatum and D. acuminata Blooms in the Galician Rias

Toxic Gymnodinium catenatum blooms usually occur in the Galician Rias at the end of the upwelling season, which necessitates a ban on harvesting shellfish extraction, with subsequent economic losses for this sector. One of the possible causes cited in the literature is the advection of populations from outside the area but no evidence was available to substantiate this.Oceanographic conditions at the end of the upwelling season in the NW coast of the Iberian Peninsula (39°–43°N) have been studied for the years 1986, 1990, 1995 and 1998. Sea surface temperature data from satellite images, wind data, drifter tracks and in situ oceanic data from the Galician Rias have been combined to clarify the oceanographic structures in the area at the commencement of the blooms. On the inner shelf, an inshore poleward current advecting warm water has been identified after the cessation of upwelling. On the middle and outer shelf, a tongue of cold water as a remnant of the previous upwelling continued to move southward. On the slope and offshore, the poleward counter current reported by several authors was detected carrying warm oceanic water northwards.It is suggested that the inshore poleward current, not previously reported in the literature, could advect initial populations of dinoflagellates to the Rias from northern Portuguese waters. This would explain why blooms such as G. catenatum have been found usually in Portuguese waters several weeks before the Galician Rias, showing an apparent northward movement, but cells of this toxic dinoflagellate species have not been found in waters of the offshore poleward counter current.     

WDS-A微扫测井测斜系统电路设计

为了完成测斜系统传感器信号调制、控制、三总线信号驱动、转换及上传数据解调电路功能,根据三总线信号特点,设计出一套数据接口、信号采集与控制电路,帧形成及字形成电路.经过室内及十余次野外油田试验,表明:接口及信号调制控制传输电路达到功能设计要求,微电扫测斜系统电子仪传输后转换精度达到4.2‰,表示每帧数据传输时间的时间字偏差不超过0.3‰,说明该短节电路设计可靠稳定,满足功能要求.     

江西经济社会可持续发展之矿产资源合理利用与保护的对策思路

２１世纪初期是江西经济实现第二步战略目标并向第三步战略目标迈进的关键时期,本文通过对江西省矿产资源状况及面临的严峻形势的分析,指出了地勘单位和矿山企业当前存在的问题,强调了节约资源保护环境的重要性和在保护中开发,在开发中保护的原则,提出了实施江西经济社会可持续发展的矿产资源方面的对策思路。     

Improved Inter‐calibration of Faraday Cup and Ion Counting for In Situ Pb Isotope Measurements Using LA‐MC‐ICP‐MS: Application to the Study of the Origin of the Fangshan Pluton,North China

A laser ablation multi‐collector inductively coupled plasma‐mass spectrometry (LA‐MC‐ICP‐MS) method was developed to obtain precise and accurate Pb isotopic ratio measurements in low‐Pb materials (< 10 μg g^?1) using a combination of Faraday cups and ion counters (FC–IC). The low abundance ²⁰⁴Pb (~ 1.4%) was collected using an IC. A NBS 981 standard solution was used to cross‐calculate the FC–IC gain and to investigate the signal response characteristics of the IC. A significant, continuous and linear decrease in the FC–IC gain was observed within 1 hr, but this drift could be corrected using the calibrator‐sample‐calibrator bracketing method. In addition, a non‐linear response of the IC used in this study was observed and corrected by a non‐linear correction algorithm, which was established by measuring a series of gravimetrically prepared NBS 981 standard solutions (NIST SRM 981). Compared with the conventional arrangement, the use of the newly designed X skimmer cone and Jet sample cone improved the signal intensities from Pb isotopes by a factor of 1.9. Compared with only Faraday cups, using a combination FC–IC array was found to enhance the measurement repeatability (RSD) of ^20xPb/²⁰⁴Pb by approximately one order of magnitude when the ²⁰⁴Pb intensity was < 8 mV. Eight natural glasses and the NIST SRM 612 reference material glass (as a calibration material) were measured to evaluate the new protocol for Pb isotope determination. The analytical results were in agreement with the reference values within 2s measurement uncertainties. For MPI‐DING ATHO‐G (5.67 μg g^?1 total Pb), KL2‐G (2.07 μg g^?1 total Pb) and ML3B‐G (1.38 μg g^?1 total Pb), the typical accuracies of ^20xPb/²⁰⁴Pb were 0.09% of preferred values with precisions of < 0.33% (2RSD). The Pb isotope ratios in feldspars from granodiorite and within mafic microgranular enclaves (MMEs) from the Fangshan pluton, North China, were measured using the present method. The Pb isotopic compositions of feldspars from the whole host granodiorite show that that are radiogenic in the margin zone and gradually become less radiogenic. For the MMEs, the Pb isotopic compositions of feldspars are highly variable and overlap with those of the whole host granodiorite. For single‐grain feldspar, the strong rim‐core‐rim variations of the Pb isotopic compositions and trace elements are interpreted to have been generated via magma mixing. These results suggest that the Fangshan pluton underwent magma mixing of mantle‐derived mafic magmas with felsic magmas, and the proportion of the mafic magma influx decreased over time.     

单片机控制的锁相频率合成技术

叙述了由单片机、定时计数器8253－5及单片集成锁相环路组成的可程控频率合成技术，而标频可经单片机设定预置值给定时器T1而形成，并经锁相环路产生各种离散的频率输出。     

�¼���ʱ����С�Ϳ��پ����������е�Ӧ��

????????????A032??ET??????С???????????????У?????FG5??112?е??????????????SR620??????????????????????????????????????????????????????洢????????????????????????     

3C390．3的弱秒差距尺度喷流及其变化

通过对射电星系３Ｃ３９０．３在历元１９８９．２９及６ｃｍ波长的ＶＬＢＩ观测数据的多软件包成象，辨认出其弱秒差距尺度喷流中几个分离的节，将它们和以前发表及未发表的同一波长的成象结果比较，显示了该源弱秒差距尺度喷流的弯曲和反喷流，并重新证认了喷流中节的视超光速运动。     

用于守时工作的时间间隔计数法与双混频时差测量比对法的比较

为了比较用于守时工作的时间间隔计数法和双混频时差测量法,分析了国家授时中心时频基准实验室的两种测量比对设备(SR620时间间隔计数器和PCOMP多通道相位比较仪)对同一组原子钟进行测量时所得到的结果(钟的速率、RMS、测量精度和稳定度)。分析所得的主要结论是:双混频时差测量法具有更高的比对精度,更适用于氢原子钟短期(τ≤5 d)稳定度的测量。     

1998年试验期间华南暴雨的系统配置和环流特点

在１９９８年华南暴雨试验和南海季风试验资料的基础上，分析和得出了这期 间六次暴雨的大尺度、天气尺度和中尺度系统特征和物理量的变化规律，发现 在华南暴雨期间不同程度地建立反哈得莱环流，并给出了华南ＭＣＣ的系统配置。