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991.
试样经碱熔,盐酸提取的钛,在以盐酸、硫酸、磷酸组成的强酸性溶液体系中,利用铝片的强还原性,还原四价钛为三价钛。再用三价铁氧化三价钛为四价钛,过量的三价铁离子与硫氢酸根离子生成血红色络合物,根据此原理测定高含量钛。实验证明,溶液在此强酸性体系中,隔绝空气和控制时间的条件下,其含量范围在0.13%~100%内,测定结果准确度高。 相似文献
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To reconstruct the formation and evolution process of the warm current system within the East China Sea (ECS) and the Yellow Sea (YS) since the last deglaciation, the paleoceangraphic records in core DGKS9603, core CSH1 and core YSDPI02, which were retrieved from the mainstream of the Kuroshio Current (KC), the edge of the modem Tsushima Warm Current (TWC) and muddy region under cold waters accreted with the Yellow Sea Warm Current (YSWC) respectively, were synthetically analyzed. The results indicate that the formation and evolution of the modem warm current system in the ECS and the YS has been accompanied by the development of the KC and impulse rising of the sea level since the last deglaciation. The influence of the KC on the Okinawa Trough had enhanced since 16 cal kyr BE and synchronously the modem TWC began to develop with the rising of sea level and finally formed at about 8.5 cal kyr BP. The KC had experienced two weakening process during the Heinrich event 1 and the Younger Drays event from 16 to 8.5 cal kyr BP. The period of 7-6 cal kyr BP was the strongest stage of the KC and the TWC since the last deglaciation. The YSWC has appeared at about 6.4 cal kyr BP. Thus,the warm current system of the ECS and the YS has ultimately formed. The weakness of the KC,indicated by the occurrence of Pulleniatina minimum event (PME) during the period from 5.3 to 2.8 cal kyr BE caused the main stream of the TWC to shift eastward to the Pacific Ocean around about 3 cal kyr BP. The process resulted in the intruding of continent shelf cold water mass with rich nutrients. Synchronously, the strength of the YSWC was relatively weak and the related cold water body was active at the early-mid stage of its appearance against the PME background, which resulted in the quick formation of muddy deposit system in the southeastern YS. The strength of the warm current system in the ECS and the YS has enhanced evidently, and approached to the modern condition gradually since 3 cal kyr BP. 相似文献
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J. Bhattacharjee 《Ocean Engineering》2009,36(11):831-841
In the present study, the effect of shear current on the propagation of flexural gravity waves is analyzed under the assumptions of linearized shallow-water theory. Explicit expressions for the reflection and transmission coefficients associated with flexural gravity wave scattering by a step discontinuity in both water depth and current speed are derived. Further, trapping and scattering of flexural gravity waves by a jet-like shear current with a top-hat profile are examined and certain limiting conditions for the waves to exist are derived. The effects of change in water depth, current speed, incident wavelength and the angle of incidence on the group and phase velocities as well as on the reflection and transmission characteristics are analyzed through different numerical results. 相似文献
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Maiorano Luigi; Bartolino Valerio; Colloca Francesco; Abella Alvaro; Belluscio Andrea; Carpentieri Paolo; Criscoli Alessandro; Jona Lasinio Giovanna; Mannini Alessandro; Pranovi Fabio; Reale Bruno; Relini Giulio; Viva Claudio; Ardizzone Gian Domenico 《ICES Journal of Marine Science》2009,66(1):137-146
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