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61.
The more sensitive an analysis method the more care must be given to sample preparation. Solid phase extraction (SPE) onto RP 18 phases has established itself as a general purification and enrichment technique for trace components in aqueous samples. Various factors may thereby influence the recovery rate. For example, the ratio amount of sorbent and sample volume should be taken into account to avoid breakthrough of the investigated substance. Extracting phenylurea herbicides from drinking water, the ratio should be 1 g RP 18 sorbent per 1 L water sample. Concerning the flow rate for the fungicides procymidone, vinclozolin, and iprodione, the recovery rate decreases using higher flow rates than 3 or 6 mL/min. In the case of phenylurea herbicides, a flow rate of 10 or 14 mL/min showed best results. Even the coefficient of variation is below ± 5% at these flow rates. Furthermore, the company dependence should be considered because the recovery rate might differ by up to 40% using the nominally identical material. The same applies to the batch dependence of quality from the same company. The concentration of the eluate must also be monitored and carried out with great care to avoid decreasing the recovery rate. Considering these factors of influence, SPE is a very useful tool in sample preparation, particularly if an automated system is used. 相似文献
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本文在遥感技术系统分析的基础上,给出了一个效益分析模型与相应的一些计算方法。在找寻提高遥感效益关键所在及制定遥感发展战略、政策和规划的过程中,它们是一个非常有效的工具。 相似文献
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Thomas J. East 《地球表面变化过程与地形》1985,10(5):441-463
Q-mode factor analysis of soil particle size data is used to identify the three dominant geomorphic processes responsible for the spatial variability of particle size in a catchment on the basaltic Darling Downs landsurface. Three factors are shown to account for 95 per cent of the textural variability of a suite of transported and sedentary materials. The spatial characteristics of groups of samples associated with the three factors suggests that the three factors are associated with suspended sediment transport and deposition, weathering, and bedload transport and deposition respectively. These interpretations are supported by the detailed graphical analysis of the cumulative particle size curves. The spatially variable influence of the three factors and related processes is given by their respective factor loadings which are mappable for the surface layer materials. 相似文献
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深部气层和干层的区分是常规测井解释的难题。认识始于实践。本文依据东濮凹陷深层试采资料,建立了两个模式各四个参数的隶属度曲线,进行气层和干层模糊综合评判研究,并用该地区深层试井资料作了检验,效果颇佳。证明模糊综合评判是区分深部气层和干层的一种行之有效的方法。 相似文献
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采用二进小波变换,构造了位场基小波,通过简单模型,分析了位场信号小波分解与重构的物理实质,阐明了小波变换的频带分布与“归一化”位场空间分布的一致性,以及小波重构的规律,并叙述了小波重构与异常分解的关系. 相似文献
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Wagner José Barreto Ieda Scarminio Maria Cristina Solci Dílson Norio Ishikawa Melissa Tiemi Ogasawara Sônia Naomi Nomi Sônia Regina Giancoli Barreto 《洁净——土壤、空气、水》2007,35(3):239-245
Seventeen physical and chemical parameters were obtained from a hydroelectric reservoir located in a tropical region in the south of Brazil. Multivariate Principal Component Analysis (PCA) and Hierarchical Group Analysis (HGA) were used to identify the parameters discriminating the origin of water from the Tibagi and the Primeiro de Maio River, after it has passed the mixing region. The study was conducted during the dry and rainy seasons in July 2002 and February 2003 at three depths and three sampling sites located 0, 5, and 10 km away from the mixing region. The statistical methods showed to be appropriate for identifying the contribution of each tributary in the water mixing site of a complex water system. The most important discriminating parameter was the absorbance relation A(253 nm)/A(203 nm), followed by the concentrations of Fe(III), Mn(III), and Ni(II). An anthropogenic interference was found in the reservoir due to high Ni(II) and orthophosphate concentrations caused by a nearby town sewage discharge. The interference was more important during the dry periods due to the lower dispersion of the pollutants. Urgent initiatives should be taken from the state government to build treatment stations for the wastewater of the small cities around the Capivara hydroelectric reservoir to prevent the drinking water quality from deteriorating. 相似文献
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