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161.
用m-氨基苯甲酸作原料,经溴代、重氮化、还原脱氨、酰氯化和酯化反应等步骤,合成了六种新型的三溴苯甲酸的溴代和非溴代芳酯,即;双(2,4,6-三溴苯甲酸)-2',3',5',6'-四溴-1',4'-苯二酯,2,4,6-三溴苯甲酸-2',3',4',5',6'-五溴苯酯,2,4,6-三溴苯甲酸-2',4',6'-三溴苯酯,2,4,6-三溴苯甲酸-4'-溴苯酯,2,4,6-三溴苯甲酸-4'-甲基苯酯和2,4,6-三溴苯甲酸苯酯.通过对产物中碳、氢、溴元素的定量分析以及红外吸收光谱和氢核磁共振谱的研究,验证了合成产物的结构。 相似文献
162.
163.
基于3S技术的朝阳港潟湖湿地景观格局演变研究 总被引:7,自引:0,他引:7
在朝阳港潟湖湿地景观分类体系基础上,利用3S技术对多时相的潟湖湿地景观格局进行了定量分析,结果表明,从1954年到2002年人工景观面积增加了532 hm2,景观格局指数呈现出景观多样性和均匀度增加、优势度下降的趋势;潟湖总体斑块密度从0.017 4个/hm2增加到0.034 6个/hm2,廊道密度从0.69 54 m/hm2增加到22.05 640m/hm2,景观破碎化程度逐渐增强. 潟湖湿地景观格局变化与人类的干扰活动密切相关,因此在潟湖湿地资源保护中合理调控人类的干扰活动尤为重要. 相似文献
164.
165.
Jonathan M. Bull Martin Gutowski Justin K. Dix Timothy J. Henstock Peter Hogarth Timothy G. Leighton Paul R. White 《Marine Geophysical Researches》2005,26(2-4):157-169
Chirp sub-bottom profilers are marine acoustic devices that use a known and repeatable source signature (1–24 kHz) to produce
decimetre vertical resolution cross-sections of the sub-seabed. Here the design and development of the first true 3D Chirp
system is described. When developing the design, critical factors that had to be considered included spatial aliasing, and
precise positioning of sources and receivers. Full 3D numerical modelling of the combined source and receiver directivity
was completed to determine optimal source and receiver geometries. The design incorporates four source transducers (1.5–13 kHz)
that can be arranged into different configurations, including Maltese Cross, a square and two separated pairs. The receive
array comprises 240 hydrophones in 60 groups whose group-centres are separated by 25 cm in both horizontal directions, with
each hydrophone group containing four individual elements and a pre-amplifier.
After careful consideration, it was concluded that the only way to determine with sufficient accuracy the source–receiver
geometry, was to fix the sources and receivers within a rigid array. Positional information for the array is given by a Real
Time Kinematic GPS and attitude system incorporating four antennas to give position, heading, pitch and roll. It is shown
that this system offers vertical positioning accuracy with a root-mean-square (rms) error less than 2.6 cm, while the horizontal
positioning rms error was less than 2.0 cm. The system is configured so that the Chirp source signature can be chosen by software
aboard the acquisition vessel.
The complete system is described and initial navigational and seismic data results are presented. These data demonstrate that
the approach of using fixed source-receiver geometry combined with RTK navigation can provide complete 3D imaging of the sub-surface. 相似文献
166.
Graham P. Wilson Angela L. Lamb Melanie J. Leng Silvia Gonzalez David Huddart 《Estuarine, Coastal and Shelf Science》2005,64(4):685-698
Microfossil analysis (e.g. diatoms, foraminifera and pollen) represents the cornerstone of Holocene relative sea-level (RSL) reconstruction because their distribution in the contemporary inter-tidal zone is principally controlled by ground elevation within the tidal frame. A combination of poor microfossil preservation and a limited range in the sediment record may severely restrict the accuracy of resulting RSL reconstructions. Organic δ13C and C/N analysis of inter-tidal sediments have shown some potential as coastal palaeoenvironmental proxies. Here we assess their viability for reconstructing RSL change by examining patterns of organic δ13C and C/N values in a modern estuarine environment. δ13C and C/N analysis of bulk organic inter-tidal sediments and vegetation, as well as suspended and bedload organic sediments of the Mersey Estuary, U.K., demonstrate that the two main sources of organic carbon to surface saltmarsh sediments (terrestrial vegetation and tidal-derived particulate organic matter) have distinctive δ13C and C/N signatures. The resulting relationship between ground elevation within the tidal frame and surface sediment δ13C and C/N is unaffected by decompositional changes. The potential of this technique for RSL reconstruction is demonstrated by the analysis of part of an early Holocene sediment core from the Mersey Estuary. Organic δ13C and C/N analysis is less time consuming than microfossil analysis and is likely to provide continuous records of RSL change. 相似文献
167.
Jason-3卫星高度计于2016年1月17日成功发射,2016年2月12日进入预定轨道,与Jason-2高度计同轨进入编队飞行阶段,并落后Jason-2高度计约1分20秒,两者相距约560 km。2016年9月1日,Jason-2高度计变换轨道,编队飞行阶段结束,两高度计进入平行轨道,以增加卫星高度计对地观测的空间覆盖。本研究主要开展了Jason-3高度计的数据质量的评估与检验,包括Jason-3高度计数据可用性和有效性的验证,以及Jason-3高度计和校正辐射计各参数的数据质量监测。重点开展了Jason-2与Jason-3高度计各项参数的综合比较,利用Jason-2与Jason-3高度计编队飞行阶段的数据精确评估了两高度计参数的一致性,并从全球数据角度分析了Jason-3高度计获取各参数的能力以及稳定性;通过与Jason-2互交叉点比较分析评估Jason-3高度计海面高度数据质量情况,验证Jason-3高度计数据精度。结果表明,Jason-3高度计的数据质量满足高度计测高的要求,具有与Jason-1、Jason-2、T/P等高度计相同或更高的测高精度以监测全球海平面变化,此外,Ja... 相似文献
168.
无机碳与雨生红球藻(Haematococcus pluvialis)细胞调节物质 总被引:4,自引:0,他引:4
以单细胞雨生红球藻为材料,采用酸碱滴定和CO2加富通气培养微藻的方法,对旧液中HCO3^-和CO3^2-浓度变化以及对红球藻细胞生长的影响进行了研究。结果表明,旧液具有限制红球藻细胞生长和诱导细胞转化的作用。同时,旧液中无机碳离子浓度明显高于新液。培养液中富含CO3^2-时,各细胞数量与CO3^2-浓度呈正相关,相关系数为0.88。溶液中仅有HCO3^-时,各细胞数与HCO3^-浓度也呈正相关性。因此,排除了CO3^2-和HCO3^-作为旧液中的调节物质,限制红球藻细胞生长和诱导细胞转化的可能性。旧液乙酸乙酯提取物生物检测实验表明,在粗提取物中有降低细胞增长和诱导细胞转化的活性,表明调节物质能溶于有机相,也反过来证实无机碳离子不是旧液中的调节物质。DNA含量和倍性分析结果表明,红球藻游动细胞DNA复制可以加倍后不经过原生质分裂就可以再次进行,因此推测旧液中的调节物质对原生质分裂过程产生抑制作用,而不对DNA复制过程产生抑制作用。 相似文献
169.
170.
The natural human female hormones oestrone and 17β-oestradiol have been implicated in the disruption of endocrine systems in some wildlife adjacent to sewage effluents. The sorption behaviour of these two compounds under estuarine conditions was studied by spiking either 2.55 μg of oestrone or 2.65 μg of 17β-oestradiol in kinetic experiments. In equilibrium experiments, 3 ng of oestrone or 3.2 ng of 17β-oestradiol was added in each of the centrifuge tubes. Sorption onto sediment particles was relatively slow, with sorption equilibrium being reached in about 70 and 170 h for oestrone and 17β-oestradiol, respectively. The effects of a variety of environmental parameters on sorption were studied including salinity, sediment concentration (SC), the presence of a third phase, particle size and, also, surfactant concentrations. Results show that although salinity did not induce any statistically significant effect on the sorption of 17β-oestradiol, it did statistically enhance the sorption of oestrone, and a salting constant of 0.3 l mol−1 was derived. The partition coefficient for both compounds decreased with increasing sediment concentration, a phenomenon that has been widely reported and attributed to the presence of colloids (which could enhance dissolved concentrations). In this paper, the true partition coefficients for sediment particles (Kptrue) and colloidal particles (Kctrue) have been calculated, and a Kptrue value of 141 and 102 ml g−1 was obtained for oestrone and 17β-oestradiol, respectively. In addition, Kctrue values for oestrone (222×102 ml g−1) and 17β-oestradiol (135×102 ml g−1) were two orders of magnitude higher than their respective Kptrue values, suggesting that the colloidal particles are significantly stronger sorbents for natural oestrogens than sediment particles. Particles of different sizes were found to have different partition coefficients due to the strong relationships between partition coefficients for the two compounds and particulate organic carbon (POC) contents and specific surface areas (SSAs). The presence of a surfactant was shown to reduce the partition coefficients for the two compounds, although its concentrations being used were higher than those normally found in the natural environment. 相似文献