复方清痹片糖衣片改薄膜衣片质量标准研究

目的：研究复方清痹片糖衣片改薄膜衣片的质量标准。方法：将原由滑石粉、糖浆、川蜡等辅料包糖衣片改为由胃溶型薄膜包衣预混剂包薄膜衣片,对薄膜衣片质量标准进行研究,对赤芍、防己、黄柏、甘草等进行薄层鉴别研究,并对赤芍中芍药苷进行含量测定方法学研究。结果：赤芍、防己、黄柏、甘草薄层鉴别斑点清晰,专属性强;芍药苷在2.9858～29.8584μg/ml之间有良好的线性关系,平均回收率98.33%,RSD%为1.70%。结论：糖衣片改薄膜衣片工艺可行,质量控制可靠、准确,可用于复方清痹片的质量控制。     

基于DPPH-HPLC-Q-TOF-MS/MS技术的安化黑茶发酵前后抗氧化活性物质基础研究

目的：建立基于高效液相色谱串联四级杆飞行时间质谱技术（HPLC-Q-TOF-MS/MS）的安化黑茶抗氧化活性成分快速筛选和鉴别的方法,并对安化黑茶生茶及熟茶的抗氧化活性成分分别进行检测和分析。方法：采用Inertsil ODS-2C_{18色谱柱（250mm×4.6mm,5μm）反相HPLC梯度洗脱法分离各主要成分,在负离子模式下,利用四级杆-飞行时间串联质谱对各主要活性成分进行检测;进而在安化黑茶生茶及熟茶乙酸乙酯及正丁醇部位分别加入适量1,1-二苯基-2-苦基苯肼（DPPH）作为实验组,避光室温反应30min后经液质联用分析,并与不加入DPPH的空白组物质进行比较,快速发现其活性成分;并采用对照品、文献比对、质谱裂解规律分析鉴定生茶、熟茶的抗氧化活性成分。结果：依据质谱裂解规律及文献检索,从安化黑茶生茶乙酸乙酯部位中共鉴定出32个抗氧化活性成分,从生茶正丁醇部位中共鉴定出28个抗氧化活性成分;从熟茶乙酸乙酯部位中共鉴定出31个抗氧化活性成分,从熟茶正丁醇部位中共鉴定出26个抗氧化活性成分。结论：利用DPPH-HPLC-Q-TOF-MS/MS技术快速筛选和鉴别安化黑茶中抗氧化活性成分的有效方法,为其质量控制及物质基础研究提供了技术支持。}     

Spatio-temporal variability of small fishes related with environmental factors in a typical domestic tap water lake,Eastern China

The knowledge of prey small ?sh stock, distribution and abundance is necessary to guide stocking of piscivorous ?sh for the biomanipulation in domestic tap water lakes. This study describes the current status of small ?sh community in Kuilei Lake(China), and examines the spatial and seasonal variations of the community in relation to key environmental factors. Based on submerged macrophyte cover and water depth, the lake was divided into ?ve major habitats:(1) macrophyte covered shallow habitat of water depth< 2.00 m,(2) uncovered or less-covered shallow habitat(2.00 m–3.50 m),(3) uncovered medium shallow habitat(3.50 m–5.00 m),(4) uncovered medium deep habitat(5.00 m–6.50 m) and(5) uncovered deep habitat(6.50 m–8.50 m). The abundance and composition of small ?sh were monitored by benthic fykenet sampling from April 2013 to January 2014. A total of 2881 individuals belonging to 5 families and 21 species were collected. Based on their abundance(accounted for 88.96% of the total) and occurrence(more than 33.33%), Acheilognathus chankaensis, Acheilognathus macropterus, Microphysogobio microstomus,Pseudorasbora parva and Rhinogobius giurinus were recognized as dominant small ?sh species. The results of correlation analysis identi?ed that species richness( Sr), Shannon-Wiener diversity index( H′)and Margalef′s richness index( D) were signi?cantly negatively correlated with water depth, but positively correlated with biomass of submerged macrophytes.Redundancy analysis(RDA) revealed that the spatial distributions of most small ?shes were negatively associated with water depth. The details of these ?ndings are bene?cial to understanding the adaptation of the small ?shes in degraded environments, and to developing suitable biomanipulation strategies for the management of ?sh resources and water quality in the lakes along the lower reach of the Changjiang(Yangtze) River basin.     

航行体近水面滑跳运动试验研究

航行体近水面滑跳运动是近年来跨介质航行体研究的热点问题之一,针对航行体水面滑跳运动现象开展研究。 首先设计了适宜滑跳的航行体构型,通过数值仿真方法确定航行体的主要技术参数,发现航行体滑跳过程对于重心位置非常敏感;然后,针对设计的构型,开展水面自由滑跳试验,试验表明本文设计的模型可以在近水面稳定滑跳,验证了滑跳运动方式的可行性。 工作可为后续跨介质航行体设计提供技术参考。     

PSD法测量大型射电望远镜副面位姿

指向精度是大型射电望远镜天线具有挑战性的关键技术指标.在望远镜运行中,方位俯仰角的变化、重力以及日照等对副面撑杆的综合影响会引起望远镜的副面位姿改变从而引起指向误差的增加和天线效率的降低.基于天马65 m射电望远镜,使用位置传感器装置(PSD)法构建了副面位置偏移量测定系统,可以实时采集副面的3维位移数据,构建重力模型,将测试结果与射电法构建的现有副面模型进行对比,有较好的一致性.此外,该系统可以分析日照(引起撑腿局部温度效应)引起的副面位移情况,也可以监视风载和瞬时启停对副面位姿的影响.     

SAGE测光巡天数据处理方法研究

元素丰度与星系演化(Stellar Abundance and Galactic Evolution,SAGE)是自主设计的能够准确计算恒星大气参数以及消光的新测光系统。对北天除银盘外共计约12 000 deg2的天区开展了SAGE系统测光巡天,计划获取约5亿颗恒星的高精度测光数据。单次曝光条件下100σ完备星等uSC～17. 3,vSAGE～16. 8(AB星等),这些为研究银河系提供宝贵的测光资料。介绍了巡天专用的数据处理程序的研究和开发,主要研究了针对单幅图像的快速自动化处理过程,重点介绍数据改正、天体测量校正、测光和流量定标过程,以及数据结果和数据质量检测等。     

基于容器技术的天文应用软件自动部署方法

平方千米阵列即将开始建设,各子工作包也进入关键设计评估阶段。基于云与容器技术是平方千米阵列科学数据处理器未来可能采用的平台技术。针对超大规模海量数据处理面临的天文应用软件快速部署、运行与实测要求,充分考虑天文应用软件运行环境复杂、云计算环境下超大规模计算集群部署困难等问题,系统研究并给出了一种使用容器技术的天文应用软件通用自动部署方法。以目前较为常用的可见度函数校准软件SAGECaL为例,首先分析了SAGECaL的相关特性和分布式部署方面存在的困难,进而给出了基于容器技术的SAGECaL分布式集群的自动部署方法。实验结果表明,自动部署方法极大地提高了SAGECaL分布式集群的部署效率,满足项目组承担平方千米阵列科学数据处理器相关测试工作所需要的基础平台部署与切换等需求,同时也为其它天文软件在云端的快速部署与执行提供了有益的思路。     

Test area of the SAGE survey

Sky surveys represent one of the most important efforts to improve developments in astrophysics,especially when using new photometric bands. We are performing the Stellar Abundance and Galactic Evolution(SAGE) survey with a self-designed SAGE photometric system, which is composed of eight photometric bands. The project mainly aims to study the stellar atmospheric parameters of ～0.5 billion stars in ～12 000 deg2 of the northern sky, which mainly focuses on Galactic astronomy, as well as some aspects of extragalactic astronomy. This work introduces the detailed data reduction process of the test field NGC 6791, including the data reduction of single-exposure images and stacked multi-exposure images, and properties of the final catalog.     

A PCA approach to stellar abundances I. testing of the method validity

The derivation of element abundances of stars is a key step in detailed spectroscopic analysis. A spectroscopic method may suffer from errors associated with model simplifications. We have developed a new method of deriving the various element abundances of stars based on the calibration established from a group of standard stars. We perform principal component analysis(PCA) on a homogeneous library of stellar spectra, and then use machine learning to calibrate the relationship between principal components and element abundances. By testing with spectral libraries S4 N and MILES, we find that our procedure provides good consistency when spectra from a homogeneous set of observations are used, and it could be expanded to stars with quite a wide range of stellar parameters, with both dwarfs and giants. Moreover, we discuss the four key factors that have a significant impact on the results of derived element abundances,including the resolution of the spectra, wavelength range, the signal-to-noise ratio(S/N) of spectra and the number of principal components adopted.     

Low-mass and high-mass supermassive black holes in radio-loud AGNs are spun-up in different evolution paths

How supermassive black holes(SMBHs) are spun-up is a key issue in modern astrophysics. As an extension to the study in Wang et al., here we address the issue by comparing the host galaxy properties of nearby(z 0.05) radio-selected Seyfert 2 galaxies. With the two-dimensional bulge+disk decompositions for the SDSS r-band images, we identify a dichotomy in various host galaxy properties for radio-loud SMBHs. By assuming that radio emission from the jet reflects a high SMBH spin, which stems from the well-known Blandford-Znajek mechanism of jet production, high-mass SMBHs(i.e., MBH 107.9 M⊙)have a preference for being spun-up in classical bulges, and low-mass SMBHs(i.e., MBH = 106-107 M⊙)in pseudo-bulges. This dichotomy suggests and confirms that high-mass and low-mass SMBHs are spun-up in different ways, i.e., a major "dry" merger and a secular evolution respectively.