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61.
62.
John E. Hathaway Richard O. Gilbert John E. Wilson Brent A. Pulsipher 《Stochastic Environmental Research and Risk Assessment (SERRA)》2009,23(2):253-261
After site clean-up teams have removed all of what they believe to be UXO within a specific impact area, statistical compliance
sampling is a possible method for verifying with a specified probability that this area has been cleaned to specifications.
Schilling [J Qual Technol 10(2):47–51, 1978, Acceptance sampling in quality control. Marcel Dekker, Inc., New York, 1982] developed a compliance sampling methodology based on the hypergeometric distribution. Bowen and Bennett (1987) also use compliance sampling where they provide an approximation for estimating the number of samples (n) required to state with desired probability that the entire population of sample units (N, where n < N) are in compliance with cleanup goals. This article describes two methods (anomaly and transect) for applying the Schilling
[J Qual Technol 10(2):47–51, 1978, Acceptance sampling in quality control. Marcel Dekker, Inc., New York, 1982] compliance sampling method to military training sites. After describing these methods, a simulation study is presented which
demonstrates the performance of transect compliance sampling calculations based on varied degrees of clustered UXO within
a specific impact area and different types of sampling routines. 相似文献
63.
64.
Javiera Cervini-Silva Benjamin Gilbert Sirine Fakra Stephan Friedlich Jillian Banfield 《Geochimica et cosmochimica acta》2008,72(10):2454-2464
Highly insoluble Ce-bearing phosphate minerals form by weathering of apatite [Ca5(PO4)3.(OH,F,Cl)], and are important phosphorous repositories in soils. Although these phases can be dissolved via biologically-mediated pathways, the dissolution mechanisms are poorly understood. In this paper we report spectroscopic evidence to support coupling of redox transformations of organic carbon and cerium during the reaction of rhabdophane (CePO4·H2O) and catechol, a ubiquitous biogenic compound, at pH 5. Results show that the oxic–anoxic conditions influence the mineral dissolution behavior. Under anoxic conditions, the release of P and Ce occurs stoichiometrically. In contrast, under oxic conditions, the mineral dissolution behavior is incongruent, with dissolving Ce3+ ions oxidizing to CeO2. Reaction product analysis shows the formation of CO2, polymeric C, and oxalate and malate. The presence of more complex forms of organic carbon was also confirmed. Near edge X-ray absorption fine structure spectroscopy measurements at Ce-M4,5 and C-K absorption edges on reacted CePO4·H2O samples in the absence or presence of catechol and dissolved oxygen confirm that (1) the mineral surface converts to the oxide during this reaction, while full oxidation is limited to the near-surface region only; (2) the Ce valence remains unchanged when the reaction between CePO4·H2O and O2 but in the absence of catechol. Carbon K-edge spectra acquired from rhabdophane reacted with catechol under oxic conditions show spectral features before and after reaction that are considerably different from catechol, indicating the formation of more complex organic molecules. Decreases in intensity of characteristic catechol peaks are accompanied by the appearance of new π* resonances due to carbon in carboxyl (ca. 288.5 eV) and carbonyl (ca. 289.3 eV) groups, and the development of broad structure in the σ* region characteristic of aliphatic carbon. Evolution of the C K-edge spectra is consistent with aromatic-ring cleavage and polymerization. These results further substantiate that the presence of catechol, O2 (aq) causes both the oxidation of structural Ce3+ and the transformation of catechol to more complex organic molecules. Scanning Transmission X-Ray Microscopy measurements at the C K and Ce M4,5 edges indicate three dominant organic species, varying in complexity and association with the inorganic phase. Untransformed catechol is loosely associated with CeO2, whereas more complex organic molecules that exhibit lower aromaticity and stronger CO π* resonances of carboxyl-C and carbonyl-C groups are only found in association with the grains. These results further serve as basis to postulate that, in the presence of O2, CeO2 can mediate the oxidative polymerization of catechol to form higher molecular weight polymers. The present work provides evidence for a pathway of biologically-induced, non-enzymatic oxidation of cerium and formation of small CeO2 particles at room temperature. These findings may have implications for carbon cycling in natural and cerium-contaminated soils and aqueous environments. 相似文献
65.
R. Nagendra P. Sathiyamoorthy A. N. Reddy Harry Gilbert B. C. Jaiprakash 《Arabian Journal of Geosciences》2014,7(10):4133-4144
Grey shale Member of the Dalmiapuram Formation, Ariyalur Group, Cauvery Basin, India was studied for its stratigraphic position, age, and paleobathymetry with a re-look into the lithological relationship and foraminifer assemblages in the deepened limestone mine excavations at M/s Dalmia Cements, Dalmiapuram. Twenty grey shale samples from Kovandankurchchi (pit-4) and Kallakkudi mines yielded diversified calcareous, benthic, and rare index planktic foraminifera. The foraminiferal assemblages suggest a latest Albian age and middle neritic depositional conditions. The abundance of kaolinite and smectite clay minerals relate to warm/humid climate which corroborate with rising relative sea level during grey shale deposition. The grey shale occurs in patches within the marl bedded limestone member which exhibits cyclic deposition of limestone and marl. The limestone mine sections demonstrate that the grey shale forms part of basal marl bedded limestone, directly overlying the coral algal limestone. The present study demonstrates that the grey shale outcrops in Dalmiapuram Formation should be placed stratigraphically as part of marl bedded limestone. The member status for grey shale which is current usage stands discounted. 相似文献
66.
Gilbert Boillot 《Tectonophysics》1986,129(1-4)
There is a great similarity between the Galicia margin and the Aquitaine margin (i.e. the Aquitaine Basin and the North Pyrenean zone). In particular, the timing of the rifting as well as the resulting structures (exposure of perodotite, tilted fault blocks, normal and transverse faults, half grabens) are practically the same. This comparison leads to the interpretation that the northern side of the Pyrenean fold belt is inherited from the Mesozoic deep passive margin of Europe. The Cenozoic thrust sheets and reverse faults of the northern Pyrenees zone are tentatively interpreted as former rift structures (tilted blocks and listric faults) which were removed during the convergence of the Iberian and European plates during the Paleocene and Eocene. 相似文献
67.
Ship noise received on a horizontal array towed behind the ship is shown to be useful as a potentially diagnostic tool for estimating local acoustic bottom properties. In numerical simulations, tow-ship noise which bounces off the bottom is processed on a beamformer that shows the arrival angles; the beamformer output is readily interpreted by relating it to the Green's function of the acoustic wave equation. Simple signal processing is shown to be sufficient to extract the propagation angles of the "trapped" (i.e., propagating) modes of the acoustic waveguide. By relating the trapped modes to a basic geophysical model of the bottom, one can predict acoustic-propagation conditions for a particular bottom-interacting ocean acoustic environment. 相似文献
68.
Verónica Oliveros Dania Tristá-Aguilera Gilbert Féraud Diego Morata Luis Aguirre Shoji Kojima Fernando Ferraris 《Mineralium Deposita》2008,43(1):61-78
The Michilla mining district comprises one of the most important stratabound and breccia-style copper deposits of the Coastal
Cordillera of northern Chile, hosted by the Middle Jurassic volcanic rocks of the La Negra Formation. 40Ar/39Ar analyses carried out on igneous and alteration minerals from volcanic and plutonic rocks in the district allow a chronological
sequence of several magmatic and alteration events of the district to be established. The first event was the extrusion of
a thick lava series of the La Negra Formation, dated at 159.9 ± 1.0 Ma (2σ) from the upper part of the series. A contemporaneous intrusion is dated at 159.6 ± 1.1 Ma, and later intrusive events are
dated at 145.5 ± 2.8 and 137.4 ± 1.1 Ma, respectively. Analyzed alteration minerals such as adularia, sericite, and actinolite
apparently give valid 40Ar/39Ar plateau and miniplateau ages. They indicate the occurrence of several alteration events at ca. 160–163, 154–157, 143–148,
and 135–137 Ma. The first alteration event, being partly contemporaneous with volcanic and plutonic rocks, was probably produced
in a high thermal gradient environment. The later events may be related either to a regional low-grade hydrothermal alteration/metamorphism
process or to plutonic intrusions. The Cu mineralization of the Michilla district is robustly bracketed between 163.6 ± 1.9
and 137.4 ± 1.1 Ma, corresponding to dating of actinolite coexisting with early-stage chalcocite and a postmineralization
barren dyke, respectively. More precisely, the association of small intrusives (a dated stock from the Michilla district)
with Cu mineralization in the region strongly suggests that the main Michilla ore deposit is related to a magmatic/hydrothermal
event that occurred between 157.4 ± 3.6 and 163.5 ± 1.9 Ma, contemporaneous or shortly after the extrusion of the volcanic
sequence. This age is in agreement with the Re–Os age of 159 ± 16 Ma obtained from the mineralization itself (Tristá-Aguilera
et al., Miner Depos, 41:99–105,2006). 相似文献
69.
70.
Pb isotope data, major and trace element compositions, fission track and synchrotron X-ray fluorescence analyses are presented
for staurolites from nine pelitic schists in the continental United States to evaluate their potential use in U-Pb geochronology.
Seven U-Pb analyses from Lanzirotti and Hanson (1995) are reexamined with respect to this additional data which was not available
at the time. These data are then compared to 21 new U-Pb analyses of staurolite of varying composition from a variety of localities.
The primary goals of this study are to: (1) evaluate the variability in U and Pb abundance and U/Pb ratio in staurolites of
varying composition; (2) constrain how much of the measured U and Pb is derived from radiogenic solid inclusions such as monazite
and zircon; (3) constrain how much of the measured U and Pb is derived from staurolite itself and evaluate any possible correlation
of U and Pb abundance and U/Pb ratio to major element composition; (4) place preliminary constraints on closure temperature
to Pb diffusion in staurolite; (5) evaluate how meaningful U-Pb ages can better be calculated for the low U/Pb ratio minerals.
In the staurolite fractions analyzed U abundances range from 0.2 to 24.9 ppm, Pb from 0.13 to 2.41 ppm, the 238U/204Pb ratios vary from 135 to 9447, and the 206Pb/204Pb ratios from 23 to 623. For many of the fractions analyzed precise U-Pb ages can be calculated (±10 Ma or better) that appear
to be consistent with available age constraints on the time of peak metamorphism. Mass balance calculations, fission track
analysis, and synchrotron X-ray fluorescence trace element mapping show that although radiogenic inclusions are almost always
present in large staurolite porphyroblasts, it is difficult for inclusions to account for the measured Pb isotopic compositions.
It is also demonstrated that the U-Pb ages calculated for staurolites from Connecticut are at least 20 Ma older than nearby
Rb-Sr muscovite and 40Ar-39Ar hornblende ages. This is consistent with staurolite having a closure temperature to U and Pb diffusion significantly higher
than 500 °C.
Received: 14 July 1995 / Accepted: 16 May 1997 相似文献