Iron, Cu and Zn stable isotope systems are applied in constraining a variety of geochemical and environmental processes. Secondary reference materials have been developed by the Institute of Geology, Chinese Academy of Geological Sciences (CAGS), in collaboration with other participating laboratories, comprising three solutions (CAGS‐Fe, CAGS‐Cu and CAGS‐Zn) and one basalt (CAGS‐Basalt). These materials exhibit sufficient homogeneity and stability for application in Fe, Cu and Zn isotopic ratio determinations. Reference values were determined by inter‐laboratory analytical comparisons involving up to eight participating laboratories employing MC‐ICP‐MS techniques, based on the unweighted means of submitted results. Isotopic compositions are reported in per mil notation, based on reference materials IRMM‐014 for Fe, NIST SRM 976 for Cu and IRMM‐3702 for Zn. Respective reference values of CAGS‐Fe, CAGS‐Cu and CAGS‐Zn solutions are as follows: δ56Fe = 0.83 ± 0.07 and δ57Fe = 1.20 ± 0.13, δ65Cu = 0.57 ± 0.06, and δ66Zn = ?0.79 ± 0.12 and δ68Zn = ?1.65 ± 0.24, respectively. Those of CAGS‐Basalt are δ56Fe = 0.15 ± 0.07, δ57Fe = 0.22 ± 0.10, δ65Cu = 0.12 ± 0.08, δ66Zn = 0.17 ± 0.13, and δ68Zn = 0.34 ± 0.26 (2s). 相似文献
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The runoff and sediment load of the Loess Plateau have changed significantly due to the implementation of soil and water conservation measures since the 1970s. However, the effects of soil and water conservation measures on hydrological extremes have rarely been considered. In this study, we investigated the variations in hydrological extremes and flood processes during different periods in the Yanhe River Basin (a tributary of the Loess Plateau) based on the daily mean runoff and 117 flood event data from 1956 to 2013. The study periods were divided into reference period (1956–1969), engineering measures period (1970–1995), and biological control measures period (1996–2013) according to the change points of the annual streamflow and the actual human activity in the basin. The results of the hydrological high extremes (HF1max, HF3max, HF7max) exhibit a decreasing trend (P?<?0.01), whereas the hydrological low extremes (HBF1min, HBF3min, HBF7min) show an increasing trend during 1956–2013. Compared with the hydrological extremes during the reference period, the hydrological high extremes increased during the engineering measures period at low (<?15%) and high frequency (>?80%), whereas decreased during the biological control measures period at almost all frequencies. The hydrological low extremes generally increased during both the engineering measures and biological control measures periods, particularly during the latter period. At the flood event scale, most flood event indices in connection with the runoff and sediment during the engineering measures period were significantly higher than those during the biological control measures period. The above results indicate that the ability to withstand hydrological extremes for the biological control measures was greater than that for the engineering measures in the studied basin. This work reveals the effects of different soil and water conservation measures on hydrological extremes in a typical basin of the Loess Plateau and hence can provide a useful reference for regional soil erosion control and disaster prevention policy-making.