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31.
32.
An approach to determination of phenolic compounds in seawater using SPME-GC-MS based on SWCNTs coating 总被引:1,自引:0,他引:1
Phenolic compounds have become one kind of the important pollutants of the marine environment. Single-walled Carbon nanotubes, as one-dimensional nano materials, have light weight and perfect hexagonal structure of connections, with many unusual mechanical, chemical and electrical properties. In recent years, with the research of carbon nanotubes and other nano materials, the application prospect is also constantly discussed. In this paper, homemade single-walled carbon nanotubes(SWCNTs) coating was used for establishing an analytical approach to the determination of five kinds of phenolic compounds in seawater using SPME-GC-MS. Optimal conditions: After saturation was conducted with Na Cl, and p H was adjusted to 2.0 with H_2SO_4, the extract was immersed in a water bath at 40 for GC℃-MS determination through 40-min agitating extraction at 500 rmin~(-1) and 3-min desorption at 280℃. The liniearities ranged between 0.01-100 μg L~(-1), and the determination limits ranged between 1.5-10 ngL~(-1). The relative standard deviation(RSD, n = 5) was less than 6.5%. For the phenolic compounds obtained from the spiked recovery test for actual seawater samples, the rates of recovery were 87.5%-101.7%, and the RSDs were less than 8.8%, which met the requirements of determination. Due to its simplicity, high efficiency and low consumption, this approach is suitable for the analysis of trace amounts of phenolic compounds in marine waters. 相似文献
33.
WU Yanyan CHEN Yufeng LI Laihao YANG Xianqing YANG Shaoling LIN Wanling ZHAO Yongqiang DENG Jianchao 《中国海洋大学学报(英文版)》2016,15(4):681-689
This study was carried out to investigate the biogenic amines(BAs), physicochemical property and microorganisms in dry salted fish, a traditional aquatic food consumed in China. Forty three samples of dry salted fish were gathered from retail and wholesale markets and manufacturers, which had been produced in various regions in China. Cadaverine(CAD) and putrescine(PUT) were quantitatively the most common biogenic amines. About 14% of the samples exceeded the histamine content standards established by the FDA and/or EU. The highest histamine content was found in Silver pomfret(Pampus argenteus)(347.79 mg kg-1). Five of forty three samples exceeded the acceptable content of TYR(100 mg kg-1), and 23.26% of dried-salted fish contained high contents of biogenic amines(above 600 mg kg-1). In addition, species, regions, pickling processes and drying methods made the physicochemical property, microorganisms and biogenic amines in dry salted fish to be different to some extents. The total plate count(TPC) was much higher than that of total halophilic bacteria in all samples. The biogenic amines, physicochemical property and microbiological counts exhibited large variations among samples. Furthermore, no significant correlation between biogenic amines and physicochemical property and TPC was observed. This study indicated that dry salted fish may still present healthy risk for BAs, depending on the processing methods, storage conditions among others. 相似文献
34.
35.
Position-domain integrity risk-based ambiguity validation for the integer bootstrap estimator 总被引:1,自引:0,他引:1
Integrity monitoring for ambiguity resolution is of significance for utilizing the high-precision carrier phase differential positioning for safety–critical navigational applications. The integer bootstrap estimator can provide an analytical probability density function, which enables the precise evaluation of the integrity risk for ambiguity validation. In order to monitor the effect of unknown ambiguity bias on the integer bootstrap estimator, the position-domain integrity risk of the integer bootstrapped baseline is evaluated under the complete failure modes by using the worst-case protection principle. Furthermore, a partial ambiguity resolution method is developed in order to satisfy the predefined integrity risk requirement. Static and kinematic experiments are carried out to test the proposed method by comparing with the traditional ratio test method and the protection level-based method. The static experimental result has shown that the proposed method can achieve a significant global availability improvement by 51% at most. The kinematic result reveals that the proposed method obtains the best balance between the positioning accuracy and the continuity performance. 相似文献
36.
We present an aerosol injection technique (AIT) to accelerate the consolidation of soft soils for ground improvement. We employ high-pressure aerosol injections at different depths to enhance the drainage in soft soils for faster consolidation. The technique is briefly described. A well-instrumented field test is carried out to demonstrate its performance. Compared to the traditional methods, our approach gives rise to faster dissipation of excess pore pressure and larger ground settlement. This method is particularly attractive for the improvement in soft ground in medium depths.
相似文献37.
LIN Xueyuan LI Tingjun QIU Libo LIN Yu 《地球空间信息科学学报》2006,9(2):89-93
IntroductionDouble-Star is to use two stationary orbit satellitesto locate the target which is located in the overlayarea of the the satellites’wave-beam. The two sat-ellites can only supply two equations. In order toget the three-dimensional position of… 相似文献
38.
立式储液罐地震破坏快速评估方法 总被引:1,自引:0,他引:1
本文采用大型有限元程序ANSYS对立式储液罐的地震反应进行了非线性数值分析,考虑了罐体和内部液体的相互作用,得到了3个不同容积的储罐,在不同峰值的地震动时程输入下的反应结果。结合地震灾害中立式储罐的地震破坏现象和特点,以及现有的立式储罐地震破坏预测方法,提出了立式储罐的地震破坏快速评估方法。 相似文献
39.
MA Lu ZHAO Lin TIAN Li-ming YUAN Li-ming XIAO Yao ZHANG Le-le ZOU De-fu QIAO Yong-ping 《山地科学学报》2019,(7)
The availability of high-resolution satellite precipitation measurement products provides an opportunity to monitor precipitation over large and complex terrain and thus accurately evaluate the climatic, hydrological and ecological conditions in those regions. The Global Precipitation Measurement(GPM) mission is an important new program designed for global satellite precipitation estimation, but little information has been reported on the applicability of the GPM’s products for the Tibetan Plateau(TP). The object of this study is to evaluate the accuracy of the Integrated Multi-Satellite Retrievals for GPM(IMERG) Final Run product under different terrain and climate conditions over the TP by using 78 ground gauges from April 2014 to December 2017. The results showed the following:(1) the 3-year average daily precipitation estimation in the IMERG agrees well with the rain gauge observations(R~2=0.58, P0.01), and IMERG also has a considerable ability to detect precipitation, as indicated by a high probability of detection(78%-98%) and critical success index(65%-85%);(2) IMERG performed better at altitudes from 3000 m to 4000 m with a small relative bias(RB) of 6.4%. Precipitation change was not significantly affected by local relief;(3) the climate system of the TP was divided into four climate groups with a total of 12 climate types based on the K?ppen climate classification system, and IMERG performed well in all climate types with the exception of the arid-desert-cold climate(Bwk) type. Furthermore, although IMERG showed the potential to detect snowfall, it still exhibits deficiencies in identifying light and moderate snow. These results indicate that IMERG could provide more accurate precipitation data if its retrieval algorithm was improved for complex terrain and arid regions. 相似文献
40.
JIANG Tao WANG Longhua ZHANG Fuchong FANG Xiao LU Lin ZHANG Jihong WANG Wei QU Keming CHAI Chao 《中国海洋湖沼学报》2019,(5)
Understanding the feeding selectivity on phytoplankton by shellfish is currently a big challenge.In order to investigate the feeding behavior of bay scallop(Argopecten irradians)on phytoplankton,we compared its compositions of phytopigments in digestive glands with those in the surrounding seawater,and conducted five consecutive investigations between July and November 2016 in a bay scallop culture area along coast of Qinghuangdao City,northwest of the Bohai Sea,China.Phytopigments in four-size fractionated phytoplankton of seawater(micro-(20-200 μm);nano(L)-[10-20 μm];nano(S)-[2.7-10 μm],and pico-[2.7 μm])and digestive glands of A.irradians were examined to investigate the selective feeding of A.irradians.Results show that fucoxanthin and peridinin constituted the major part of taxonomically diagnostic carotenoids(TDCs)in the micro-and nano(L)-phytoplankton in seawater.Compared with total phytoplankton biomass of seawater(TPB,sum of the four sizes),a substantial decrease of fucoxanthin proportion to total DCs in digestive glands was observed while that of peridinin,19'-butanoyloxyfucoxanthin,alloxanthin and 19'-hexanoyloxy-fucoxanthin showed an obvious increase when those pigments were mainly confined to micro-sized phytoplankton(20-200 μm).However,zeaxanthin and prasinoxanthin were mainly confined to nano(s)-and pico-phytoplankton,of which the proportions in digestive glands were usually lower in TPB.The contribution of lutein to total DCs in digestive glands(with an average of 7.23%)increased compared with TPB of seawater(with an average of 0.63%)during all five sampling times. 相似文献