Investigation of ion beam techniques for the analysis and exposure of particles encapsulated by silica aerogel: Applicability for Stardust

Abstract— In 2006, the Stardust spacecraft will return to Earth with cometary and perhaps interstellar dust particles embedded in silica aerogel collectors for analysis in terrestrial laboratories. These particles will be the first sample return from a solid planetary body since the Apollo missions. In preparation for the return, analogue particles were implanted into a keystone of silica aerogel that had been extracted from bulk silica aerogel using the optical technique described in Westphal et al. (2004). These particles were subsequently analyzed using analytical techniques associated with the use of a nuclear microprobe. The particles have been analyzed using: a) scanning transmission ion microscopy (STIM) that enables quantitative density imaging; b) proton elastic scattering analysis (PESA) and proton backscattering (PBS) for the detection of light elements including hydrogen; and c) proton‐induced X‐ray emission (PIXE) for elements with Z > 11. These analytical techniques have enabled us to quantify the composition of the encapsulated particles. A significant observation from the study is the variable column density of the silica aerogel. We also observed organic contamination within the silica aerogel. The implanted particles were then subjected to focused ion beam (FIB) milling using a 30 keV gallium ion beam to ablate silica aerogel in site‐specific areas to expose embedded particles. An ion polished flat surface of one of the particles was also prepared using the FIB. Here, we show that ion beam techniques have great potential in assisting with the analysis and exposure of Stardust particles.     

Multistep matched-field inversion for broad-band data from ASIAEX2001

This paper discusses the results of geoacoustic inversion carried out using explosive charge data from the Asian Seas International Acoustic Experiment (ASIAEX) East China Sea (ECS) Experiment. A multifrequency incoherent matched-field inversion processor and a genetic algorithm (GA) are used for the inversion. A multistep matched field inversion approach is presented, which makes use of the varying sensitivities of wave fields at various frequencies to reduce the inversion problem into a sequence of smaller inversions with fewer unknowns to estimate at each stage. Different parameters are estimated using data at different frequencies according to their sensitivities. Inversion results for different areas in the ECS region are summarized and compared with core data.     

Radio spectra of the low-luminosity active galactic nucleus NGC 266 at centimetre-to-submillimetre wavelengths

We report multi-frequency and multi-epoch radio continuum observations with multi-spatial resolution for the low-luminosity active galactic nucleus (LLAGN) NGC 266. In the centimetre regime, we find diffuse components with Very Large Array (VLA) observations, and a variable compact core with a rising spectrum with Very Long Baseline Array (VLBA) observations. Although the spectral index of the rising spectrum is consistent with the prediction of the simple advection-dominated accretion flow (ADAF) model, the observed radio power is slightly high compared with that of the model prediction. A spectral break at centimetre-to-millimetre wavelengths is inferred from the upper limits of flux densities from Nobeyama Millimetre Array (NMA) and James Clerk Maxwell Telescope (JCMT) data at millimetre and submillimetre wavelengths, respectively. More complicated considerations are required for the theoretical model to interpret such observed radio properties.     

Dynamical implications of Jupiter's tropospheric ammonia abundance

Groundbased radio observations indicate that Jupiter's ammonia is globally depleted from 0.6 bars to at least 4-6 bars relative to the deep abundance of ∼3 times solar, a fact that has so far defied explanation. The observations also indicate that (i) the depletion is greater in belts than zones, and (ii) the greatest depletion occurs within Jupiter's local 5-μm hot spots, which have recently been detected at radio wavelengths. Here, we first show that both the global depletion and its belt-zone variation can be explained by a simple model for the interaction of moist convection with Jupiter's cloud-layer circulation. If the global depletion is dynamical in origin, then important endmember models for the belt-zone circulation can be ruled out. Next, we show that the radio observations of Jupiter's 5-μm hot spots imply that the equatorial wave inferred to cause hot spots induces vertical parcel oscillation of a factor of ∼2 in pressure near the 2-bar level, which places important constraints on hot-spot dynamics. Finally, using spatially resolved radio maps, we demonstrate that low-latitude features exceeding ∼4000 km diameter, such as the equatorial plumes and large vortices, are also depleted in ammonia from 0.6 bars to at least 2 bars relative to the deep abundance of 3 times solar. If any low-latitude features exist that contain 3-times-solar ammonia up to the 0.6-bar ammonia condensation level, they must have diameters less than ∼4000 km.     

Flexure of Europa's lithosphere due to ridge-loading

Using photoclinometry, topographic profiles across europan ridges have been produced. These profiles allow the identification of bulges in the terrain adjacent to the ridges. The bulges are assumed to have been produced by flexure of the elastic lithosphere due to the load of the ridges, which lie along cracks in the crust. The distance from the crack to these “fore-bulges” depends on the thickness of the elastic plate being flexed. Based on a survey of ridges in Galileo images with resolution <300 m/pixel, the thickness of the elastic lithosphere has been determined by this method at a wide variety of sites along the leading and trailing hemispheres of Europa. The average thickness is about 200 m. The elastic lithosphere underneath smooth dilational bands tends to be thicker than plains morphology, an effect that is pronounced at Thynia Linea and Astypalaea Linea. Among the ridges investigated here, more recent loading correlates with a thicker elastic lithosphere, which may either reflect an intrinsically thicker layer, or less viscous relaxation over the shorter time period.     

Ocean-floor hydrothermal metamorphism in the Limousin ophiolites (western French Massif Central): evidence of a rare preserved Variscan oceanic marker

The Limousin ophiolite is located at the suture zone between two major thrust sheets in the western French Massif Central. This ophiolitic section comprises mantle‐harzburgite, mantle‐dunite, wehrlites, troctolites and layered gabbros. It has recorded a static metamorphic event transforming the gabbros into undeformed amphibolites and the magmatic ultramafites into serpentinites and/or pargasite‐bearing chloritites. With various thermobarometric methods, it is possible to show that the different varieties of amphibole have registered low‐P (c. 0.2 GPa) conditions with temperature ranging from high‐T, late‐magmatic conditions to greenschist–zeolite metamorphic facies. The abundance of undeformed metamorphic rocks (which is typical of the lower oceanic crust), the occurrence of Ca–Al (–Mg) metasomatism illustrated by the growth of Ca–Al silicates in veins or replacing the primary magmatic minerals, the P–T conditions of the metamorphism and the numerous similarities with oceanic crustal rocks from Ocean Drilling Program and worldwide ophiolites are the main arguments for an ocean‐floor hydrothermal metamorphism in the vicinity of a palaeo‐ridge. Among the West‐European Variscan ophiolites, the Limousin ophiolites constitute an extremely rare occurrence that has not been involved in any HP (subduction‐related) or MP (orogenic) metamorphism as observed in other ophiolite occurrences (i.e. France, Spain and Germany).     

Observation and preliminary analysis of a recent Jovian satellite phenomenon

The occultation of Io by Ganymede as observed on 10 June 1985 is reported. The middle of the occultation minimum was found to occur at 14h 14m 5.7s UT. In the plane perpendicular to the line of sight the centres of the two satellite disks passed to within ~ 2530 km of each other, at a relative velocity, in this plane, of about 11 kms^–1. The values of these last two quantities, however, depend on what assumptions are made about the light distribution over io's disk.     

Estimation of dispersion in estuaries by a self-consistent method

Longitudinal and transverse dispersion in estuaries may be determined in principle by measuring the change in time of the concentration field of a water soluble dye. In practice, measurements may take the form of several sampling runs crossing the dye patch. The coefficients of dispersion are usually estimated from the second moments of the concentration field; the use of second moments, in particular, introduces errors because measurements at long times or distance are unduly emphasized.A self-consistent method, free of the disadvantages inherent in the use of higher moments, is described in which the distribution of concentration in space is related to the zeroth spatial moment of concentration. In this formulation, based upon sampling runs across the dye patch, the concentration field in the estuary may be directly and simply related to the dispersion coefficients in both the intercept and gradient of a linear graph.The methods are illustrated by the characterization of a series of experiments in the Inner Estuary of Milford Haven.     

A lower limit to the field strength in magnetic reconnection sites in solar flares inferred from hard X-ray bursts

It is shown how the hard X-ray burst count rate and itse-folding ime can be used to estimate the minimum magnetic fieldB _min required in a flare magnetic reconnection site for the burst to be interpreted in terms of a thick target model. Application of the method to data from the Solar Maximum Mission (HXRBS) indicates absolute minimum fields well in excess of 100 G, and impossibly high values for some reconnection geometries.